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二乙酰基胺

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The result of the experiment showed that the qualitative medium - speed filter paper can be used as the material of the nitrite - detecting paper: color developing reagent A containing 4 - aminobenzene sulfonamide and N - 1 naphthyl ethylenediamine hydrochloride, and mixtures of 1 : 1 naphthylamine solution and sulfanilic acid solution as color developing reagent.

实验结果表明:定性中速滤纸可以作为亚硝酸根试纸的材料;含有4-氨基苯磺酰胺和N-1-萘基乙二胺盐酸盐的显色剂A及含有1:1的α-萘胺溶液和对氨基苯磺酸溶液的显色剂B,按1:1混合后可以作为显色剂;通过应用实验表明,亚硝酸根试纸具有体积小、便于携带、检测方便、成本低廉等特点。

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下:首先,以磺胺异噁唑和磺胺二甲嘧啶为模板,分别以4-乙烯基吡啶,甲基丙烯酸,丙烯酰胺为功能单体,以二甲基丙烯酸乙二醇酯为交联剂,偶氮二异丁腈为引发剂,采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

N-(1-Naphthyl)ethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-(1-萘基)乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

N-1-Naphthylethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-1-萘基乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

Based on hydrogen peroxide and ammonium persulfate as compounded initiating system,unsaturated vinyl monomers were used to directly copolymerize a new high range polycarboxylate water reducer structurized in carboxyl,esterquat and amido as main chain and in polyethylene glycol ether as side chain.

以过硫酸铵和双氧水为复合引发体系,采用不饱和单体直接共聚,得到一类主链为羧基、酯基、酰胺基,侧链为聚乙二醇醚基的新型聚羧酸高效减水剂,研究了共聚物的结构对分散性能的影响。

For the smelting slags of exhausted automobile catalyst, a method for determination of trace amounts of platinum and palladium by plus-dual-wavelength overlapping spectrophotometry in dibenzyl dithiooxamide-SnCl2 system was developed.

针对失效汽车催化剂火法熔炼渣,研究了采用正峰双波长叠加,二苄基二硫代乙二酰胺-SnCl2体系萃取光度法测定渣中痕量铂钯的方法。

Four new salicylaldehyde derivatives with a glucose or mannose moiety were synthesized with 2-tert-butylphenol or 4-tert-butylphenol as the starting material, followed by the formylation, chloromethylation, nucleophilic substitution reaction with the desired carbohydrate. The salicylaldehyde derivatives condensed with ethylenediamine to give the Schiff bases, which coordinated with Mn to afford four novel sugar-based Salen Mn complexes.

首先,分别以2-叔丁基苯酚和4-叔丁基苯酚为起始原料,经过甲酰化反应、氯甲基化反应、和糖类衍生物的亲核取代反应制得了四种新型并入葡萄糖基或甘露糖基的水杨醛衍生物,将它们与乙二胺缩合生成希夫碱配体,得到的配体与过渡金属Mn~(3+)配位制备出四种新型含糖基的Salen Mn配合物。

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ,N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

Dendrimers with stearyl groups on the periphery are synthesized by amidation using dendrihmers with NH2 on the periphery and stearyl chloride as raw materials.

以乙二胺和丙烯酸甲酯为原料,甲醇为溶剂,通过Michael加成及酰胺化反应,合成端基为胺基的树枝状大分子。

In chapter four, molecular imprinting polymers against amino acid derivatives utilizing 2-VP+AM as combined functional monomer and trimethylolpropane trimethacrylate as tribasic cross-linker were prepared and result was compared with those with the same amino acid derivative as the imprinted molecules utilizing ethyleneglycol dimethacrylate as dibasic cross-linker. It was found that cross-link intensity of the molecular imprinting polymer is higher when TRIM was utilized and baseline separation for the imprinted molecule could be achieved. When TRIM was utilized as cross-linker more molecule is imprinted during the polymerization.

第四章采用2-乙烯基吡啶+丙烯酰胺复合功能单体,考察了三元交联剂三甲氧基丙烷三甲基丙烯酸酯烙印氨基酸衍生物的情况,并与二元交联剂乙二醇二甲基丙烯酸酯烙印相同氨基酸衍生物的情况进行了对比,发现三甲氧基丙烷三甲基丙烯酸酯交联剂在较小的用量下就可使分子烙印聚合物达到足够的交联度,实现烙印分子的基线分离。

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