二乙胺

The compositon and structure of two complexes differed from the complex ZnS (en 〓 synthesized in ethylenediamine. The precursors were pyrolysed in nitrogen stream at 400℃.

实验结果表明这种配合物结构、组成都不同于在纯乙二胺溶液中得到的中间体配合物。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后，用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质，过滤，用次氯酸钠将样品溶液中的甜蜜素转化为N，N-二氯环己胺经正己烷萃取后，在phenomenex Gemini-C18柱上，以乙腈－水(7+3)或甲醇－水(8+2)为流动相进行分离，HPLC-UV检测器在314 nm测定，外标法定量。

X 6.36(3)? is formed.Liquid-liquid extraction experiments, between twelve heterocyclic thioalkoxycalix[4]arene on the lower rim, fifteen heterocyclic thioacetamidecalix[4]arene on the upper rim and Na~+、K~+、Cs~+、Mg~(2+)、Cu~(2+)、Co~(2+)、Cd~(2+)、Ni~(2+)、Pb~(2+)、Hg~(2+) and Ag~+ picrates, have been carried out and their results are compared.

分别将十二个下沿含有杂环硫烷氧基杯芳烃衍生物和十五个上沿含有杂环硫乙酰胺基的杯芳烃衍生物与Na~+、K~+、Cs~+、Mg~(2+)、Cu~(2+)、Co~(2+)、Cd~(2+)、Ni~(2+)、Pb~(2+)、Hg~(2+)和Ag~+的十一种苦味酸盐进行了离子萃取实验，并对两类衍生物与不用金属离子的萃取能力进行了分析和比较。

Under mild hydrothermal synthesis conditions, we first successfully prepared threeindium phosphites with different organic amine molecules as template agents.

在水热条件下，以乙二胺为模板首次合成出1个具有一维正六边形孔道结构的亚磷酸镉微孔化合物。

Based on the solid phase/liquid deposition CdSe quantum dots were synthesized using selenium and cadmium-salt as precursor at room temperature. The TEM graph showed that the average size of CdSe QDs was ca.

以硒粉及镉盐为反应前体，通过固相/液相沉淀反应及室温乙二胺溶剂体系两种方法合成了平均粒径为8～10nm的CdSe量子点，以巯基乙酸修饰量子点使之可溶，并标记生物大分子－胃蛋白酶。

The invention adopts halogen acetylized crosslinked polystyrene resin and hydroxybenzyl alcohol as the raw material, and the solid phase synthesis carrier with hydroxymethyl as the active group is synthesized through the joint catalysis of N, N-dimethyl formamide used as the reaction solvent, inorganic base and phase-transfer catalyst.

本发明采用卤乙酰化交联聚苯乙烯树脂和对羟基苯甲醇为原料，在以N，N-二甲基甲酰胺为反应溶剂、无机碱及相转移催化剂的共同催化下合成了一种以羟甲基为活性基团的固相合成载体。

SiO2 aerogel was prepared by using waterglass as the Si source, formamide as the catalyst and glycol as the drying chemical controlling additive via sol-gel method and ambient pressure drying.

以水玻璃为硅源，甲酰胺为催化剂，乙二醇为干燥控制化学添加剂，采用溶胶－凝胶法常压下干燥制备了硅石气凝胶粉体。

The results showed that ZSM-5 zeolite sieve could be synthesized using aqueous ammonia and EDA as template agent.

以离子交换的方式制备了Ni-ZSM-5和Pb-ZSM-5等催化剂，同时以XRD和IR为手段，对分别以氨水和乙二胺为模板剂合成的ZSM-5沸石分子筛的结构进行了比较。

The ZSM-5 zeolite sieve was synthesized using aqueous ammonia and EDA as template agent.

利用氨水和乙二胺等为模板剂合成了ZSM-5沸石分子筛，研究了合成温度和时间对分子筛合成的影响。

The Sm or Yb complexes were tested to be used as a catalyst for the Diels-Alder reaction of cyclopentadiene with methyl acrylate.

用α-亚磺酰基-N，N-二取代乙酰胺同三氯化钐和三氯化镱反应得到了相应的稀土配合物，用元素分析、红外光谱进行了结构表征。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。