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In this paper the antitumour action of 17 phosphoramide nitrogen mustard compounds were studied.

本文研究了17种磷酰胺氮芥类化合物,发現N-双(2-氯乙基)-N'-N-二乙撐基磷酰胺(以下均簡称AT-222)具有較强的抗癌作用。

Two compounds were synthesized with two methods. The two compounds can be synthesized by two steps with triethylamine as catalyst.

分别用氢氧化钠、三乙胺为缚酸剂,3-氨基-2-丁醇、2-氨基-3-戊醇、环己酮和二氯乙酰氯为原料,采用一步法和分步法合成了两种潜在除草剂安全剂。

The poly grafted starch copolymer was synthesized by the reaction of glycolide and starch in dimethyl sulfoxide with triethylamine as catalyst.

摘要以乙交酯和淀粉为原料,三乙胺为催化剂,在二甲基亚砜介质中合成了聚羟基乙酸接枝淀粉共聚物。

In this paper several methods including acylamide dehydration, metal cyanide replacement, etherification and isoxazole method for synthesis of 3,3-diethoxyethylcyanide were reviewed.

综述了3,3-二乙氧基丙腈的合成方法,包括酰胺脱水、金属氰化物取代、醚化和异恶唑法,用于工业化生产较为满意的合成路线是以1,1,3,3-四乙氧基丙烷为原料的异恶唑法。

Hypersil of ODS-C18 was used with acetonitrile-0.01mol/L monobasic potassium phosphate-triethylamine phosphoric acid8:92:0.4:0.3) as mobile phase.

色谱柱:依利特 Hypersil ODS柱4.6 mm×250mm,5μm),流动相:乙腈-0.01mol/L磷酸二氢钾溶液-三乙胺-磷酸(8 : 92 : 0.4 : 0.3)。

Methods The HPLC System consisted of Agilent Plus C18 column, acetonitrile-buffer(0.01mol · L-1 monobasic potassium phosphate, contained 0.1% triethyl amine, pH 6.8 )(70∶30) as mobile phase with detection wavelength 282nm.

采用 Agilent Plus C18柱;以0.01mol · L-1磷酸二氢钾溶液(含0.1%三乙胺,用磷酸调节 pH 值至6.8)-乙腈(30∶70)为流动相;检测波长:282nm 。

In application of modified phenol-formaldehyde resin in OCC pulp, firstly the application effictiveness of phenol-formaldehyde resin modified by triethylamine and diethylene triamine in OCC pulp was researched, and the optimum application effictiveness was gotten through mon- factor trial.

通过对改性酚醛树脂在OCC废纸浆中的应用研究,考察了二乙烯三胺和三乙胺改性酚醛树脂在OCC废纸浆中的应用效果,并通过单因素实验得到了改性酚醛树脂的最佳应用效果。

The thermal property studies indicate that the mass loss of compound B was 54.39% at 242.2~750℃, and when the temperature was 1000℃, there was 25.11% char residue left, which showed that the title compound has a good thermal stability and char forming capability. Using acetonitrile as the solvent instead of trichloromethane or 1, 2-dichloethane gave higher yield. During the synthesis, the yield was very low when triethylamine was used as acid acceptor alone, and when a little amount of 4-dimethylaminopyridine was added at the same time, the yield could be 81%.

结果表明,所合成的化合物B的结构与预期的结构一致;热性能研究表明,化合物B在242.2~750℃质量损失为54.39%,1000℃时仍有25.11%的炭残渣,显示出优异的热稳定性和成炭性;在相同反应条件下,用乙腈作为溶剂的反应产率比使用氯仿和二氯乙烷为溶剂的高,并且在合成过程中,单独使用三乙胺作为缚酸剂时产率很低,而当同时加入少量4-二甲氨基吡啶时,产率可达81%。

It was found that the titled amine in which although dimethyl aniline and triethyl amine both were contained, possesses less efficiency of photoinitiation while it was composed with ketone as an initiated system.

发现该特殊的胺类化合物虽包括二甲基苯胺和三乙胺两个部分,但它和酮类相组合形成的光引发体系只有较低的尤引发速率。

Department of Chemical Pharmacology, Capital University of Medical Science, Beijing 100054, ChinaAbstract: A reversedphase high performance liquid chromatographic method was developed for the simultaneous quantitative determination of caffeine, dapsone and chlorzoxazone. The operation was carried out on a C18 column (250 mmX4.6 mm i.d., 5.0 μm) with the mobile phase of acetonitrilephosphate buffer including 0.02 mol/L KH2PO4 and 0.02 mol/L (C2H53N, pH 6.5(25:75 in volume ratio).

用反相高效液相色谱同时测定血清中咖啡因、氨苯砜、氯唑沙宗探针药物的质量浓度,以乙腈磷酸盐缓冲体系(含 0.02 mol/L的磷酸二氢钾和0.02 mol/L的三乙胺,pH 6.5)(体积比为25:75)为流动相,以安替比林为内标,经C18柱(250 mmX4.6 mm i.d。, 5.0 μm)分离,紫外检测器检测,使3种探针药物得到较好的分离,并且在有效血药浓度范围内线性良好。

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