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The paper adopts some methods such as gas composition, carbon isotope, systematical analyzing and testing of reservoir bitumen biomarker from high evolutional natural gas and quantitative calculation of mixed gas, illustrates that natural gas from the section Ⅱ of Jialingjiang formation is mainly attributed to sapropel type organic matter gas of Permian, comes from carbonatite hydrocarbon rocks Permian which most of them are overmature, its main gas source has nothing to do with carbonatite hydrocarbon rocks of Jialingjiang formation themselves, presents in geochemistry characteristics of oil type cracked gas.

摘要通过对川中-川南过渡带西部的磨溪-潼南地区嘉二段天然气组成、碳同位素组成、高演化天然气储层沥青生物标志化合物的系统分析测试和混合成因气的定量估算,阐明了该区嘉二段天然气主要属于二叠系腐泥型有机质成因气,来源于二叠系过成熟为主的碳酸盐岩烃源,主力气源与嘉陵江组自身的碳酸盐岩烃源无关,并具有油型裂解气的地球化学特征。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下:一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸;蒸馏NMP;干燥增溶剂;二、在氮气气氛下,Py与NMP混匀后加入密封的反应器中,再加入增溶剂,然后加入5-氨基-2-苯并唑,搅拌;三、在氮气气氛下,将步骤二的混合液搅拌并升温至50℃~150℃后加入脂肪族二酸,再加入TPP后缩聚;四、再倾入甲醇析出沉淀,过滤,清洗沉淀,再干燥;即得到含唑环半芳香聚酰胺。

Terpenoids had business with the life of humanbeings. The last twenty years developments of tricyclic diterpenoids were reviewed.Biologic activities of tricyclic diterpenes which had oxygenous guoups on the 1, 2 or 3 position were reviewed. The important applications and some methods of introducing oxygenous groups on these three positions in recent 20 years were also obtained.

萜类化合物与人类生活密切相关,本文简要介绍了近二十年来三环二萜类化合物的最新研究进展,综述了在C-1、C-2、C-3号位上具有含氧官能团的三环二萜类化合物的生物活性、重要应用,并报道了近二十年来在这三个位置上引入含氧官能团的一些常见方法。

The optimum conditions were obtained as follows: the weight ratio of fatty acids and 85%acetic acid is 1:4, ozonolysis temperature is 20-25℃, manganese/copper acetate as catalyst, and the amount of catalyst is 0.15% of fatty acids, oxidation decomposition temperature and oxidation decomposition time are 90-95℃ and 4 hours respectively. the yields of azelaic acid and pelargonic acid are 57.4% and 51.6% respectively.

以菜油酸为原料、85%醋酸水溶液为溶剂,经臭氧化、氧化分解、重结晶等过程制备壬二酸和十三烷二酸的最佳反应条件为:m:m(85%醋酸)=1:4,臭氧化温度20-25℃;氧化分解温度80-85℃,催化剂醋酸锰/醋酸铜用量为原料菜油酸质量的0.12%,氧化分解时间3h,重结晶溶剂壬酸的用量为5倍质量的氧化分解产物时,十三烷二酸的收率为58.3%,壬二酸的收率为57.2%。

Polyethylene glycol ethers of alkyl alcohols having the general formula CH3(CH2)xCH2(OCH2CH2)nOH wherein x is 8 to 20 (of which ceteareth-20, steareth-20 and steareth-100 are preferred), poloxamer 185, poloxamer 407, N,N-dimethyl dodecylamine N-oxide, and mixtures thereof, are employed to increase follicular delivery and/or follicular residence time of certain water soluble ornithine decarboxylase inhibitors of which 2-2,5-diamino pentanoic acid and its pharmaceutically acceptable salts, hydrates, optical enantiomers and racemic mixture are preferred.

使用通式为CH3(CH2)xCH2(OCH2CH2)nOH的烷基醇的聚乙二醇醚,其中x为8-20(其中鲸蜡硬脂醇醚-20、硬脂醇醚-20和硬脂醇醚-100是优选的)、poloxamer 185、poloxamer 407、N,N-二甲基十二烷胺N-氧化物及其混合物来提高某些水溶性的鸟氨酸脱羧酶抑制剂的毛囊传输和/或毛囊停留时间,优选的抑制剂是2--2,5-二氨基戊酸及其药学上可接受的盐、水合物、光学对映异构体及外消旋混合物。

With industrial monomer solution of dimethyldiallylammonium chloride as raw material, ammonium persulphate as initiator and Na_4EDTA as chelating agent,using the methods of adding initiator all at once,graduated increasing of temperature and stepwise initiation and polymerization,the polymerization process of preparing poly-dimethyldiallylammonium chloride was researched.

以一步法工业单体二甲基二烯丙基氯化铵为原料,以过硫酸铵为引发剂,采用一次性加入引发剂,梯度升温,分步引发水溶液聚合反应的方法,对制备聚二甲基二烯丙基氯化铵的聚合反应的工艺进行了优化研究。

Phenylenediamines, aminophenols, methoxyanil ines, and 1,4- hydroquinone, 1-naphthylamine were polymerized via the catalysis of horseradish peroxidase in mixed solvents of l,4-dioxane and water at amibient conditions by using hydrogen peroxide as the oxidant. Several factors influencing the polymer yield, such as the concentration of the substrate, pH value and oxidant amount were examined using a- phenylenediamine as substrate.

本文选择了苯二胺、氨基苯酚、甲氧基苯胺三个系列,以及对苯二酚、1-萘胺等单体,在二氧六环-水混合介质中以辣根过氧化物酶为催化剂,以双氧水为氧化剂进行了不同底物的室温酶促聚合,并以邻苯二胺为底物考察了溶剂用量、pH值、作为氧化剂的双氧水用量等条件对聚合物收率的影响。

Mol〓. As the result, some sensitizers have obviously sensitive effect, the ratio of / in photostationary state was change, We designed two methods, One of them is that isomers were synthesized, then we obtained the mixtures of isomers via photoisomerization.

本论文试图由两种方法获得-O-烃基-α-氧代环十二酮肟,一种是由体的肟通过化学合成得到体的O-烃基-α-氧代环十二酮肟,再通过光化学反应得到其体;另一种是由-α-氧代环十二酮肟,通过光化学异构合成体,再由体肟化学合成得到-O-烃基-α-氧代环十二酮肟。

The liquid absorption value and growth of the bacillus was measured after 24, 48 and 72 hour. It was showed that the most effective level of maltose in the medium is 5%. The media with pimelic acid was centrifugated 30min at 10000r/min, room temperature

本研究还将添加5%的麦芽糖的生物素培养基分组,分别加入0、0.2、0.4、0.6、0.8、1.0、1.2、1.4、1.6、1.8、2.0g/L的庚二酸,接种,在37℃,220r/min条件下进行振荡培养,然后测定24、48和72h时菌液的吸收值、pH值、生物素和庚二酸含量,确定庚二酸添加量为1.0g/L时,培养液中的生物素产量最大,庚二酸利用率最高。

Reparation of PBO was begun with the polymerization process in which composite salts that contained 4,6-diaminoresorcinol and terephthalic acid were dissolved in polyphosphoric acid and phosphorus pentoxide.

BO纤维制备:以4,6-二氨基间苯二酚的盐酸盐为单体原料,与对苯二甲酸混合,经过中和反应、脱色处理、干燥后制成复合盐;再以多聚磷酸为溶剂,添加五氧化二磷和抗氧化剂,经过预聚合反应制备出PBO聚合物;聚合物通过双螺杆挤出机进一步进行聚合,然后通过喷丝板挤出,在磷酸水溶液中凝固成型,经过洗涤、干燥等过程,最终卷绕成型。

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