二-十进制

Diethylene gly- col butylmethyl ether was synthesized through the Williamson reaction between butyl bro- mide (n-C_4 H_9 Br) and CH_3 OCH_2 CH_2OCH_2 CH_2 ONa.

通过正溴丁烷与二乙二醇单甲醚钠的Williamson反应合成了二乙二醇甲基丁基醚。

Furthermore, influences of different phosphate salts at various concentrations on the ionization efficiency of phosphopeptide were investigated systematically, finding that the signal intensity for phosphopeptide 48FQEEQQQTEDELQDK63 digested from β-casein were 5 to 8 times increased in an optimized condition with 10 mmol/L ammonium monobasic phosphate or 3 to 4 times increased with 10 mmol/L ammonium dibasic phosphate as additive to matrix 2,5-dihydroxybenzoic acid, respectively.

考察了两种适合于磷酸化肽离子化的基质类型2，5-二羟基苯甲酸和2，4，6-三羟基苯乙酮。用2，5-二羟基苯甲酸作为基质时，当加入10 mM 磷酸氢二铵时，磷酸化蛋白质β-casein的磷酸肽 48FQEEQQQTEDELQDK63的离子化效率可以增强5-8倍，当加入10 mM磷酸二氢胺时，磷酸肽的离子化效率可以增强3-4倍。

Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.

用甲苯作溶剂，使三乙烯四胺和N，N-二甲基甲酰胺二甲基缩醛在85℃反应2 h，得到中间体双咪唑啉，产率90.4%，在乙腈溶剂中，碳酸钾存在下，双咪唑啉和1，2-二溴乙烷进行扩环反应，得到环状中间体一溴盐，产率78.7%，一溴盐经碱性水解2 h，得到1，4，7，10-四氮杂十二烷，产率74.2%。

The experimental results showed that, monochloroacetic acid and dichloroacetic acid enhanced photocatalytic hydrogen generation activity, but trichloroacetic acid did not improve it. The amount of produced H_2 increases almost proportionally to the irradiation time within 5 h irradiation. The photocatalytic oxidation of monochloroacetic acid and dichloroacetic acid mainly produced CO_2, HC1 and CH_2O, the photocatalytic oxidation of trichloroacetic acid mainly produced CO_2 and HCl.

实验表明，一氯乙酸、二氯乙酸的存在明显地提高了制氢反应效率，而三氯乙酸的存在却不能起到促进作用；反应5h内，反应生成氢的量与反应时间成线性关系；一氯乙酸、二氯乙酸光降解产物主要是CO_2、HCl和CH_2O，三氯乙酸光降解产物主要是CO_2和HCl；研究了溶液pH值对放氢反应的影响；在实验浓度范围内，一氯乙酸、二氯乙酸浓度对放氢反应的影响，表观上符合Langmuir-Hinshelwood关系式；考察了一氯乙酸、二氯乙酸在光催化剂表面的吸附。

Detailed geology- petrology-mineralogy study shows that late Triassic-early Jurassic granites can be divided into 4 groups: granodiorites, monzonitic-K syenogranites mainly, alkali feldspar-alkali granites and syenite, Middle Jurassic granites is composed of quartz diorites-granodiorites and monzonitic granites, the main rock type includes granodiorites and monzogranites; Early Cretaceous granites include alkali gabbro, alkali granites and granodiorites, and these rocks composed bimodal igneous rock group.

详细的地质-岩石矿物学研究表明，晚三叠-早侏罗世花岗岩可以划分成四种岩石组合，即花岗闪长岩组合、二长花岗岩—正长花岗岩组合、碱长花岗岩—碱性花岗岩组合和正长岩组合，其中以二长花岗岩—正长花岗岩组合为主；中侏罗世花岗岩由石英闪长岩-花岗闪长岩组合和二长花岗岩组合构成，岩石类型以花岗闪长岩和二长花岗岩为主；早白垩世出现了碱性辉长岩、碱性花岗岩和花岗闪长岩，构成双峰式火成岩组合。

The selective linear dimerization of isoprene to formate myrcene in a single phase catalyst solution prepared by mixing two metals, amine, solvent and a small content of isoprene was studied.

摘 要：研究了异戊二烯在两种金属催化作用下均相线性二聚生成月桂烯的影响因素，得到优惠工艺条件：反应温度 13℃，催化剂∶异戊二烯=0 。0 5∶1 0 ，胺∶异戊二烯=0 。0 7∶1.0。

Dimethylnaphthalene is an ideal raw material of the production of polyethylene naphthalate. It is an important task to obtain 2,6-dimethyinaphthalene in low cost.

2，6-二甲基萘是制备高性能聚酯-聚对萘二甲酸乙二醇酯最理想的原料，如何低成本地获得2，6-二甲基萘已成为一项重要的课题。

Poly(ethylene-2,6,-naphthalate) is a newly developed polyester. The chemical structure of PEN can be described by replacing the benzene ring in poly with the stiffer naphthalene ring.

聚萘二甲酸乙二酯是一种近年来获得较大发展的高性能聚酯材料，其分子结构与聚对苯二甲酸乙二酯相类似，可看作是由PET链中苯环由刚性更大的萘环所替代的产物。

Results11 separated constituents were identified, the contents of 3 compounds were over 20%. The main constituents in extracts were Bis(2-ethylhexyl) phthalate (21.51%), Nonacosane (25.73%), Stigmastan-3,5-dien (25.73%).

结果从海南裂叶山龙眼叶超临界二氧化碳20 MPa压力提取物中共分离出11个组分，全部进行了鉴定，其中含量高于20%的有3个，为邻苯二甲酸二(2-乙基己基)酯（21.51%）；二十九碳烷（25.73%）；3，5-二烯豆甾烷（25.73%）。

Research group of these samples after determination found that even children of all brands of edible oil in plastic barrels, all containing "phthalate ester" and "octyl phthalate", these two plasticizers in the plastics industry are frequently used phthalate type plasticizers, without the use of plastic containers containing the bulk oil and solid shortenings, almost non-plasticizer.

科研小组对这些样品进行测定后发现，儿乎所有品牌的塑料桶装食用油中，都含有&邻苯二甲酸二酯&和&邻苯二甲酸二辛酯&，这两种增塑剂是塑料工业中经常使用的酞酸酯类增塑剂，而未使用塑料容器盛装的散装豆油和固体起酥油中，几乎不含增塑剂。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷