二-十进制

Amino-6-nitrobenzodifuroxan was prepared through a three-step reaction from starting material 3, 5-dinitrobenzoic acid:(1)3, 5-dinitroaniline (1) was synthesized from the reaction of DNBA and hydrazoic acid in inert solvent 1, 2-dichioroethane through Schmidt rearrangement with yield of 89.6%;(2) 1 was subjected to nitration to prepare pentanitroaniline (2) with yield of 51.1%;(3) The title compound was prepared from 2 and sodium azide in acetic acid through denitrogenation and then Schmidt rearrangement with yield of 86.8%, m.p.204℃～206℃.

以3，5-二硝基苯甲酸为原料经过3步反应合成了7-氨基6-硝基苯并二氧化吠咱：第1步反应，在二氯乙烷惰性溶剂中，DNBA与叠氮酸反应并发生Schmidt重排反应生成3，5-二硝基苯胺(1)，产率89.6%；第2步反应，1在含100%硫酸的硝硫混酸中硝化生成五硝基苯胺(2)，产率51.1%；第3步反应，2与叠氮酸反应，不经分离直接进行热解脱氮、Schmidt重排反应，得到目标化合物， m.p.204℃~ 206℃，产率86.8%。

In order to achieve a rapid and accurate selection for extractive distillation solvent, and to acquire 1,2,3-trimethylbenzene with high purity from solvent oil via extractive distillation, the UNIFAC model was used to calculate the relative volatility of 1,2,3-trimethylbenzene to indane (the mass ratio of 1,2,3-trimethylbenzene to indane is 4∶1) in five different solvents, acetophenone, di-2-octylhexyl phthalate, glycol, dimethyl sulfoxide,sulfolane at 17.47 kPa.

为了快速准确地选择萃取精馏溶剂，由190#溶剂油萃取精馏获取高纯度连三甲苯，运用UNIFAC模型，计算了质量比为4∶1的连三甲苯-茚满体系在苯乙酮、乙二醇、邻苯二甲酸二辛酯、二甲基亚砜和环丁砜5种溶剂中在17.47 kPa下的相对挥发度。

The wholly aromatic four-component copolyesters were prepared from p-acetoxy-benzoic acid, hydroquinone diacetate, 2,6-naphthalene dicarboxylic acid and isophthalic acid by melting polycondensation.

由对乙酰氧基苯甲酸、对苯二酚二乙酯、2，6-萘二甲酸及间苯二甲酸四种单体通过熔融缩聚反应，合成了全芳香族四组分共聚酯。

Hydrophobic-hydrophilic macroporous polydivinylbenzene/polyacrylethylenediamine interpenetrating polymer networks (PDVB/PAEM IPN) were prepared by the sequential suspension polymerization method. These were composed of two networks, of which one was hydrophobic and the other was hydrophilic. The objective of this work was to study the adsorption thermodynamics and adsorption kinetics of this hydrophobic- hydrophilic IPN. The focus was on adsorption isotherms of vanillin at different temperatures, and these fit well into the Freundlich adsorption isotherm. The isosteric adsorption enthalpy, adsorption Gibbs free energies and the adsorption entropy could be calculated according to thermodynamic functions.

采用分步悬浮聚合法制备了具有疏水性能的聚二乙烯基苯(polydivinylbenzene， PDVB)为第一网，具有亲水性能的聚丙烯酰乙二胺(polyacrylethylenediamine， PAEM)为第二网的疏水／亲水大孔聚二乙烯基苯／聚丙烯酰乙二胺互穿聚合物网络(interpenetrating polymer networks， IPN)，研究这类疏水／亲水IPN组成的树脂对吸附质的吸附热力学和吸附动力学；测定了该树脂对香兰素在不同温度下的吸附等温线，吸附等温线符合Freundlich等温吸附方程，利用热力学函数关系计算出了吸附焓、自由能和熵变。

Spinel lherzolites vary from 850°to 1050℃. The number of spinel lherzolite sample increases at 850℃ and decreases at 1050℃ sharply. The rarity of spinel lherzolite between 900° 950℃ has a particular significance. Spinel-garnet lherzolites have higher temperatures (1050° 1100℃) than the spinel lherzolites.

尖晶石二辉橄榄岩的平衡温度主要介于850°-1050℃之间，850℃和1050℃分别代表了尖晶石二辉橄榄岩的数量剧增和锐减的两个温度界线，900°-950℃之间的尖晶石二辉橄榄岩的缺乏具有特殊的意义；尖晶石-石榴子石二辉橄榄岩的平衡温度介于1050°-1100℃之间。

LREE depleted spinel lherzolite xenoliths are the 2%～15% partial melting residues of spinel lherzolite with 2 times REE concentration of chondrite. LREE enriched spinel lherzolite xenoliths are the prodiuct that 1% partial melting of garnet lherzolite derived melts mix in ratio of 2% with most LREE depleted spinel lherzolite.

轻稀土亏损的尖晶石二辉橄榄岩包体，是2倍球粒陨石稀土元素丰度的尖晶石二辉橄榄岩地幔经过2％～15％部分熔融后的残留体；而富集型尖晶石二辉橄榄岩包体可能为，来自深部石榴石二辉橄榄岩源区1％熔融形成的熔体以约2％的比例隐交代轻稀土元素最亏损的包体代表的幔源区后形成的。

To assess the sensitivity of local species to toxic chemicals relative to those from other jurisdictions reported in the literature, ecotoxicological testing was also performed on three local marine species, Dunaliella salina, Brachionus plicatilis, and Lutjanus malabaricus, using 12 representative PPTSL chemicals including metals, pesticides (endosulfan, diazinon, permethrin, atrazine, tributyltin), and industrial chemicals (di-n-octyl phthalate, nonylphenol, acenaphthene).

为了评估与其他相关成文规定的当地有毒化学品种类，生态毒性测试也在三个地方的海洋物种上进行，杜氏盐藻，轮虫和红鳍笛石斑鱼，使用了十二种pptsl代表的化学元素，包括金属，杀虫剂（硫丹，二嗪磷，氯菊酯，莠去津，三丁基锡），和工业化学品（苯二甲酸二正辛酯，壬基酚，苊）。

A series of 3 - aryl - 3 -( 5,5 - dimethyl - 3 - hydroxy - 2 - cyclohexene - 1 - one - 2 - yl) propanoic ester s were synthesized by reaction between aromatic aldehydes ,5,5- dimethyl -1,3-cyclohexanedione and isopropylidene malonate catalyzed by KF - Al2O3 in alcohols.

在KF-Al_2O_3催化下，将芳香醛3，5-二甲基-1，3-环己二酮及丙二酸亚异丙酯在醇中反应，一锅式合成了一系列的3-芳基-3-(5，5-二甲基-3-羟基-2-环己烯-1-酮-2-基)丙酸酯。

N-(6-methyl-2-pyridine)-amino-methylene-diethyl malonate was produced by condensation reaction of 2-amino-6-methyl pyridine with ethoxymethylene diethyl malonate under optimal conditions that n(2-amino-6-methyl pyridine)∶n(ethoxymethylene diethyl malonate) is 1∶1.3, reacting time 45 min and temperature 130 ℃,the yield of this reaction was 96%,which was 6% higher than that of literature.

在250℃的反应温度下，分别以二苯醚、石蜡油和邻苯二甲酸二乙酯为热载体进行成环反应，得到4-氧-7-甲基-1，8-萘啶-3-羧酸乙酯的收率分别为88.6%、56.3%和61.2%，确定二苯醚为最佳热载体，并发现反应温度对产率的影响最大，原料配比次之，反应时间基本无影响。

Silver nanoparticles with average particle size ranging from 2 to 131nm were manipulatively synthesized starting from silver nitrate using 10 kinds of different functional group-containing organic modifiers, such as polyvinylpyrrolidone, tween-80, sodium dodecyl sulfate, sodium polyacrylate, polyethylene glycol, D-sorbitol, sodium dodecyl sulfonate, sodium dodecylbenzene sulfonate, polyvinyl alcohol, cetyltrimethylammonium bromide, at room temperature.

摘 要：选择10种含有不同官能团的有机物为表面修饰剂，如聚乙烯吡咯烷酮、吐温-80、十二烷基硫酸钠、聚丙烯酸钠、聚乙二醇、山梨醇、十二烷基磺酸钠、聚乙烯醇、十二烷基苯磺酸钠和十六烷基三甲基溴化铵等，在室温下进行了平均粒径在2～131nm范围内纳米银颗粒的控制合成研究。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。