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The enzymolytic products identified were:diisopro-pylaminoethanethiol through the breakdown of P-S bond, and its oxidized product, N, N'-dithiodiethylene-bis ; and diisopropyla-minochloroethane through the breakdown of S-C bond.

VS与电鳐乙酰胆碱酯酶作用的主要产物是: P—S键断裂产物二异丙氨基乙硫醇,该化合物在水溶液中不稳定,可进一步氧化为N,N'-双二异丙氨基乙基二硫醚;S—C键断裂产物二异丙氨基氯乙烷。

The results show that:(1) When N-methylethylenediamine and N, N'-methylethylenediamine equatorially coordinated to Cd〓, arenedisulfonates such as 1, 5-naphthalenedisulfonate, 2, 6-naphthalenedisulfonate and 4, 4'-bipenyldisulfonate act as a bridging ligands coordinated to adjacent Cd〓 centers, leading to a one dimensional chain structure.

研究结果表明:(1)N-甲基乙二胺和N,N'-二甲基乙二胺与Cd〓在赤道平面配位后,芳烃二磺酸根离子作为桥联配体与相邻的Cd〓在轴向配位形成了一维链状结构。

It shows that the method is reliable and can be utilized to improve the efficiency of PET equipment. This method can also apply to the esterify reaction process of PBT and PTT.

该反应精馏法亦可应用于生产聚对苯二甲酸丁二醇酯、聚对苯二甲酸丙二醇酯的酯化反应部分。

The effects of ultrasonication and HF washing on SiC nano-particles were analyzed by Zeta potential, particle size distribution and SEM. The stability of suspension of SiC in ethanol, ethanediol and mixture of the two medias with PEG as dispersant at different pH were compared. The optimum ultrasonication time for SiC nano-particles was obtained. The influence of HF washing on SiC nano-particles was discussed; and high stability of SiC nano-particles suspension was achieved at pH=10 in ethanediol with 1wt% PEG as dispersant.

本文中采用Zeta电位、粒度分析、SEM等测试技术分析了超声震荡和HF酸洗对SiC纳米粉体的影响:对比研究了乙醇、乙二醇以及75%乙醇和25%乙二醇混合液作为分散介质,聚乙二醇为分散剂时纳米SiC粉体在不同pH下的分散稳定性,确定了粉体最佳超声震荡的最佳时间;探讨了酸洗的作用;并在乙二醇中,以1% PEG为分散剂,pH=10条件下获得了纳米碳化硅粉体的高稳定分散悬浮液。

RESULTS: All aromatic anesthetics inhibited I at a holding potential which produce half-maximal current V(1/2; inhibition was modest with 1,3,5-trifluorobenzene (8%+/- 2%), pentafluorobenzene (13%+/- 2%), and hexafluorobenzene (13%+/- 2%), but greater with benzene (37%+/- 2%), fluorobenzene (39%+/- 2%), 1,2-difluorobenzene (48%+/- 2%), 1,4-difluorobenzene (31 +/- 3%), and 1,2,4-trifluorobenzene (33%+/- 1%).

结果:在最高电流的一半的控制电压下所有芳香族麻醉药都阻断钠电流;均苯三酚(8%+/- 2%)、戊苯(13%+/- 2%)、戌苯(13%+/- 2%)的抑制是适度的比苯(37%+/- 2%)、氟苯(39%+/- 2%),1.2-二氟二苯(48%+/- 2%),1,4-二氟二苯(31 +/- 3%),和1,2,4三氟苯(33%+/- 1%)明显。

Three new ferrocenylmethyl-substituted indenes and cyclopentadienes were synthesized by the addition of hydrogen anion and carbon anion to fulvene and benzo fulvene respectively, moreover, their structures were characterized by NMR and MS.

本文以二茂铁基富烯和二茂铁基苯并富烯为前体,通过负氢和负碳对双键的加成,合成了3个新型的二茂铁基甲基取代的茚及环戊二烯,并对其结构进行了核磁及质谱表征。

By the numerical analysis of the ultimate bearing capacity of two- and three-dimensional footing under combined loading mode, the results show that the effect of alteration of underground water lever on bearing capacity of three-dimensional foundation is more than on that of two-dimensional foundation, the effect of soil gravity on bearing capacity of three-dimensional foundation is more than that of two-dimensional foundation. At the same time, the numerical calculation process of ABAQUS indicates that whether the geostatic stress is balanced or not has great effect on the numerical convergence. In view of the effect extent of dilation angle of soil on the ultimate bearing capacity and the failure pattern of foundation, the condition of two-dimensional plane strain is higher than that of the three-dimensional foundation.

复合加载模式下,通过对三维矩形基础和二维条形基础进行数值分析,结果表明:黏性土地基中地下水位的变化,对三维矩形基础极限承载力的影响程度高于对二维条形基础的影响;在求解地基极限承载力的过程中,土体重度对三维矩形基础的影响明显高于对二维条形基础的影响,同时ABAQUS数值计算过程表明,地基土体地应力能否合理平衡,对数值求解过程中是否收敛有很大的影响;就土体剪胀角对地基极限承载力的影响程度而言,二维平面应变情况下土体剪胀角对极限承载力的影响比三维情况下的影响更明显,即土体剪胀角对条形基础极限承载力的影响高于三维矩形基础。

Diethyl glutarate was synthesized using glutaric anhydride and ethanol, which were separated from dicarboxylic acid, as raw material, heteropoly acid as catalyst.

以从二羧酸中分离出的戊二酸酐和乙醇为原料,用杂多酸为催化剂,合成了戊二酸二乙酯。

The diisoamyl glutarate in catalysis of silicotungsticacid was preparated by esterification of isoamyl alcohol and glutaric anhydride seperated from dicarboxylic acid.

用硅钨杂多酸为催化剂,以从二羧酸中分离出的戊二酸酐和异戊醇为原料合成了戊二酸二异戊酯。

The standard curves for glyoxal and glyoxalic acid both had good linear relations in the ranges of 2~20 mg/L and 10~100 mg/L, respectively.

乙二醛质量浓度在2~20 mg/L范围内,乙二醛二腙的峰面积与乙二醛的质量浓度之间呈良好的线性关系;乙醛酸质量浓度在10~100 mg/L范围内,乙醛酸腙的峰面积与乙醛酸的质量浓度之间呈良好的线性关系。

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

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