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二-十进制

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Thus, a stable, homogeneous melt solution is obtained from a solid mixture comprising 4,4'-biphenol(mp 282-284 DEG C) at a temperature of about 200 DEG C using either diphenyl carbonate or bis carbonate as the diaryl carbonate component.

因而,在约200℃的温度下使用碳酸二苯酯或碳酸二酯作为碳酸二芳基酯组分,由含有4,4′-二酚(mp282-284℃)的固体混合物获得稳定、均质熔体溶液。

Four kinds of aromatic ether-linked dinitriles with low melting temperatures were obtained via the nucleophilic substitution of hydroquinone, resorcinol, biphenol and bisphenol A with CBN. They were polymerized to afford a series of poly(pheny-s-triazine)s under the optimized conditions.

以对苯二酚、间苯二酚和联苯二酚为原料,分别与对氯苯腈进行亲核取代反应,合成了三种较低熔点的含醚键二腈,并分别研究了其在优化条件下的聚合反应。

Sulfonated poly are prepared by direct polymerization of biphenol A, disodium 4, 4"-difluoro-3, 3"-disulfonate-1, 1-diphenylketone and 2, 6-difluorobezonitrile. The polymers are characterized with ~1H-NMR, FT-IR.

以双酚A,2,6-二氟苯腈和4,4′-二氟-3,3′-二磺酸钠-1,1′-二苯酮采用直接缩合法合成了不同磺化度的磺酸型聚芳醚腈酮,通过FT-IR和~1H-NMR对聚合物进行了表征,证明其结构正确。

Sulfonated poly are prepared by direct polymerization of biphenol A, disodium 4, 4"-difluoro-3, 3"-disulfonate-1, 1-diphenylsulfone and 1, 3-(4-difluorophenyl)benzene. The polymers are characterized with ~1H-NMR, FT-IR.

以双酚A,1,3-二(4-氟苯基)苯和4,4′-二氟-3,3′-二磺酸钠-1,1′-二苯砜采用直接缩合法合成了不同磺化度的磺酸型聚芳醚酮砜,通过FT-IR和~1H-NMR对聚合物进行了表征,证明其结构正确。

Poly with sulfonic acid groups were readily synthesized with biphenol and 1,3-bis(4-fluorobenzoyl)benzene in the presence of excess potassium carbonate followed by sulfonation with chlorosulfonic acid.

以二氯二苯甲烷和2,6-二甲基苯酚为原料合成了含有阻碍基团的双酚单体,用此双酚单体和1,3-二(4-氟苯甲酰基苯)在无水碳酸钾存在的条件下反应制得聚芳醚酮,然后用氯磺酸磺化,控制反应条件,使磺酸基团恰好进入苯环对位,制得新型结构的磺化聚芳醚酮。

The best survuval rate of each stage thawed-embryos existed in groups of Zygote EDT3O-two-step method with I mm equilibration(66%), of Morulae EDT3O-two-step method with I mm equilibration(94%) and EDT4O-two--step method with 0.5 mm equilibration(94%), of Blastocyte EDT3O-two-step method with I mm equilibration(91%) and EDT4O-one-step method with I mm equilibration(91%).

总之,我们的研究表明,DET玻璃液冷冻方法是简单、经济而又高效的,冷冻小鼠各阶段胚胎都能获得较高的存活率,其中受精卵的EDT30二步法1分钟平衡组(66%)、桑椹胚的EDT30二步法1分钟平衡组(94%)和EDT40二步法0.5分钟平衡组(94%)、囊胚的EDT30二步法1分钟平衡组(91%)和EDT40一步法1分钟平衡组(91%)冷冻效果最好。

Our idea of easy dimensional driving includes mainiy:(1) a driving mechanism of construction constraints and dimensional constraints,(2) automatic graphic recognition of constraints,(3) a bothway cross dimensional linked list for storing dimension sparse matrices and for recalling them,(4) a reasonable method of constraint consistence checking,(5) the linking of movement of 2D views,(6) a method for creating a sequence graphic library.

随着二维与三维设计技术的交叉发展,目前的参数化设计主要有两个分支:①面向纯二维的图形参数化,其特点是二维图形为多拓扑环的复杂图形;②面向三维的基于CSG特征造型的参数化,用于拉伸扫描的单拓扑环的二维图形参数化及空间任意曲面的参数化是其特点。

Optically active cyclophane s, such as helical molecules and three-dimensional, cagelike cyclophanes have been the subject of extensive investigation from the standpoints of structural chemistry and material science.

本论文在大量的文献调研和本实验室过去研究结果的基础上,设计了由2,2'-二取代-1,1'-联萘和2,6-二取代吡啶,1,4-二取代苯,4,4'-二取代联苯三种不同连接桥通过炔键链接构筑的拓扑有趣的光学活性环芳化合物-四联萘笼状分子。

Ingredients:water,glycerin,caprylic/capric triglyceride, cetyl alcohol ,propylene glycol,glyceryl stearate,panthenol,betaine dimethicone,simmondsia chinensis, rosa rugosa flower extract,allantoin,carbomer,parfum,triethanolamine,tocopheryl acetate,methyl paraben,propyl paraben,creatine,tetrasodium edta,phenoxyethanol,caprylyl glycol,sorbic.

成分:去离子水,甘油,辛酸/葵酸三甘油酯,鲸蜡醇,丙二醇,硬脂酸甘油酯,泛醇,甜菜碱,聚二甲基硅氧烷,霍霍巴油,玫瑰花提取液,尿囊素,卡波姆,香精,三乙醇胺,生育酚乙酸酯,对羟基苯甲酸甲酯,对羟基苯甲酸丙酯,肌酸,乙二胺四乙酸四钠,苯氧乙醇,辛二醇,山梨酸。

A series of 2-oxocyclododecyl sulfonylurea s have been synthesized from 2-oxocyclododecylsulfonamide via acylation of phenyl chloroformate and amination.

以环十二酮为起始原料,经磺化反应制备得到2-氧代环十二烷基磺酸盐B,B经过氯化和胺解反应制备得到2-氧代环十二烷基磺酰胺C,C经过苯氧酰化与胺解反应后合成了10个新的2-氧代环十二烷基磺酰脲类化合物D,它们的结构通过了1HNMR和IR的确证。

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