二-十进制

New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene PolymerizationFacile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that:1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.

本工作的新贡献如下：(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2，3-双(2，6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2，6-二[1-(2，4，6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上，研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响，研究表明：1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理，可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体；2、BET，XRD，IR，SEM，GPC和DSC研究表明，脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。

New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene Polymerization Facile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that: 1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.

本工作的新贡献如下：(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2，3-双(2，6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2，6-二[1-(2，4，6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上，研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响，研究表明： 1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理，可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体； 2、BET，XRD，IR，SEM，GPC和DSC研究表明，脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。

Two bispyrazolylimine nickel complexes [bis-N-(phenyl-1,3,5-dimethylpyrazolylmethylene) phenylimine nickel dibromide] (Cat.1) and [bis-4-methoxy-N-(phenyl-1,3,5-dimethylpyrazolylmethylene) phenylimine nickel dibromide] (Cat.2) were synthesized.

合成了两种双吡唑亚胺镍配合物：双－N-（苯基－1-3，5-二甲基吡唑基亚甲基）苯基亚胺二溴化镍Cat.1）和双－4-甲氧基－N-（苯基－1-3，5-二甲基吡唑基亚甲基）苯基亚胺二溴化镍

54 2 Have been synthesized by the reaction of di(p-chlorbenzyl)tin dichloride with sodium dithiocarbamate .

利用二二氯化锡和吗啉氨荒酸钠、N， N-二乙基氨荒酸钠反应，合成了二锡双吗啉氨荒酸酯C24H28Cl2N2O2S4Sn Mr = 694。

The good development prospect of popularizing dimethyl ether vehicle in China is pointed out.

介绍了二甲醚生产工艺，对比了二甲醚与柴油的理化性质，分析了二甲醚作为汽车发动机燃料的可行性和存在的问题，指出了我国推广使用二甲醚汽车的良好发展前景。

Result At the end of dioestrus, the estradiol level was increased gradually, and the peak of estradiol appeared from 1 day before oestrus to 3 days after oestrus (52.50±29.26) pg/mL, then the estradiol decreased rapidly, its lowest value at 6-9 days of oestrus (7.20±5.50) pg/mL. The level of progesterone was low before oestrus, and rose gradually at the peak of estradiol and reached the highest value at 9-15 days of oestrus (35.52±7.87) ng/mL, then it decreased gradually.

结果 发情间期的末期，雌二醇开始升高，在发情前1 d至发情开始后3 d内出现雌二醇高峰(52.50±29.26) pg/mL，峰值后雌二醇急剧下降，到发情第6~9天下降至最低值(7.20±5.50) pg/mL；孕酮水平在发情前期较低，于雌二醇高峰时开始上升，发情第9~15天达到最高值(35.52±7.87) ng/mL，此后逐渐下降。

Effects of 1 2-benzenedicarboxylic acid dibutyl phthalate and diphenylamine on mineral elements absorption of young tomato root system were studied in this paper.

以番茄为试材，研究了邻苯二甲酸、邻苯二甲酸二丁酯和二苯胺3种化感物质对番茄幼苗根系吸收矿质元素的影响。

The inhibitive effect of 1, 2-benzenedicarboxylic acid on the absorption of N, P and K increased with its concentration rising. Low concentration of dibutyl phthalate increased the absorption of N, but decreased the absorption of P and K. Its high concentration restrained the absorption of N, P and K, while the low concentration of diphenylamine could stimulate the absorption of N and K, but restrain the absorption of P.

随着邻苯二甲酸浓度的增加，其对番茄幼苗根系吸收N、P、K的抑制作用增强；低浓度的邻苯二甲酸二丁酯可以促进番茄幼苗根系对N的吸收，抑制对P、K的吸收，高浓度时对N、P、K的吸收均起抑制作用；低浓度的二苯胺可以促进番茄幼苗根系对N、K的吸收，抑制对P的吸收。

The results show that 5% nucleating agent,twelve-hydrated disodium hydrogen phosphate,could reduce the supercooling degree of acetate hydroxide trihydrate to some extent but the supercooling degree was still large.However,the supercooling degree of sodium acetate trihydrate could decrease clearly by adding 3% thickener gelatin and 5% twelve-hydrated disodium hydrogen phosphate.

实验结果表明，质量百分比为5%的成核剂十二水磷酸氢二钠能一定程度上抑制无机水合盐三水醋酸钠的过冷度，但其过冷度仍然较大；使用质量百分比5%的十二水磷酸氢二钠和质量百分比3%的增稠剂明胶做添加剂后，三水醋酸钠的过冷性能得到明显改善。

Sodium hexametaphosphate, sodium acid pyrophosphate, monosodium phosphate,disodium phosphate

六偏磷酸钠，酸式焦磷酸钠，，磷酸二氢钠，磷酸氢二钠，磷酸氢二钾，磷酸二氢钾

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。