二-十进制

The polyesters with terminal hydroxyl groups were prepared by condensation polymerization of adipic acid with 1,4-butanediol or ethylene glycol and, in some cases, a little amount of propylene glycol. The polyurethane thermoplastics were then prepared with the polyester, 4,4'-diphenylmethane diisocyanate and 1,4-butanediol.

采用己二酸、乙二醇(或加入少量1，2-丙二醇)和1，4-丁二醇制备了端羟基聚酯，并用该聚酯和4，4'-二苯基甲烷二异氰酸酯、1，4-丁二醇制备了聚酯型热塑性聚氨酯；考察了NCO/OH值、聚酯分子量等因素对热塑性聚氨酯的物理机械性能的影响。

Copolyesters of sebacic/terephthalic acid series was synthesized by the condensation polymerization of sebacic acid and terephthalic acid with ethanediol and neopentyl glycol.

论文采用癸二酸、对苯二甲酸与乙二醇、新戊二醇进行缩聚反应，合成了癸二酸/对苯二甲酸系共聚酯。

Attempts in part I of the dissertation were to develop microemulsion systems using medium chain triglyceride, Captex 300, deionized water (H2O), and TPGS as surfactant for the oral delivery of protein drugs or poorly water soluble drugs. Pseudo-ternary phase diagrams were constructed to elucidate the phase behavior of systems composed of medium-chain triglyceride and water with TPGS as main surfactant, polysorbates (Tween 20, Tween 40, Tween 60 and Tween 80) as adjuvant surfactants, and polyethylene glycols (PEG 400 and PEG 600) and polyols (ethanediol, 1,2-propanediol, 1,3-propanediol, 1,3-butanediol, 1,4-butanediol and glycerin) as cosurfactants.

藉由拟三相图（Pseudo-ternary Phase Diagrams）的建立来了解中链型三酸甘油酯、去离子水及TPGS为主要界面活性剂配合聚醇山梨酯（如Tween 20、Tween 40、Tween 60及Tween 80）为辅助界面活性剂或聚乙二醇（如PEG 400及PEG 600）及多醇类（如乙二醇、1，2-丙二醇、1，3-丙二醇、1，3-丁二醇、1，4-丁二醇及甘油作为共界面活性剂所形成的微乳基剂之相变化。

In result, formic, acetic, methanesulfonic, oxalic, malonic, succinic and glutaric acids were detected notably. Formic, acetic and oxalic acids were the most abundant organic acids, and the sum of their concentrations averagely accounted for 89% of the total detected organic acids and 13% of the total anions, respectively.

结果表明，甲酸、乙酸、甲磺酸、乙二酸、丙二酸、丁二酸、戊二酸均有不同程度检出，一元有机酸中甲酸和乙酸在每场降水中均有检出；二元有机酸中，乙二酸和丁二酸检出率很高，其他有机酸检出率较低。

In this paper, the glyoxal structure both in reagent and in bulking solution were detected by infrared spectro and mass spectra, the result shows that there is no aldehyde group but only hydrate existing in both solutions. Besides, the mechanism of the ac-tion between glyoxal and waterlogged wood is discussed and some problems like how to prevent the bulk-ing solution from acidification are also mentioned.

此外，还运用红外光谱和质谱法测定了试剂乙二醛和加固液的结构，详细讨论了乙二酯在试剂和加固液中官能团的存在形式和聚合状态的细微变化，指出在二种溶液中并不存在醛基，乙二醛仅以水合物的形式存在并讨论了乙二醛与饱水古木的作用机理，提出用醇溶液能有效控制乙二醛使用中易返酸等问题。

Liu Yakang Lu Jianmin He Jianyun Jin Guantai College of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing, 100029

引言 环氧基型丙烯酸粉末涂料，通常所采用的固化剂主要有：壬二酸、癸二酸、十二二酸及二十二酸等［1］。

The reaction of [60] fullerene with dimethyl malonate and diethyl malonate in the presence of manganese acetate dihydrate for 20 min afforded singly bonded [60] fullerene dimers in a 1, 4-addition pattern.

Mn作为一类良好的自由基引发剂，能有效地催化C〓与丙二酸二甲酯和丙二酸二乙酯的自由基加成反应，生成C〓的二聚体。在回流的氯苯中随着时间的的延长，二聚体分解成1，4-双加成的C〓衍生物。

Result 16 kinds of fatty acids were separated from Anak chicken muscle and identified. Among them, 7 kinds fatty acids, including lauric acid, myristic acid, pen-tadecanoic acid, palmitic acid, margaric acid, stearic acid and eicosanoic acid, were saturated fatty acids and its content accounted for 38.55% of the total fatty acids; 9 kinds fatty acids, including 11-teteadecenoic acid, 9-hexadecenoic acid, 9-vaccenic acid, 9,12-octadecadienoic acid, 6,9,12-octadeca-trienoic acid, 11-eicosenoic acid, 10, l3-eicosenoic acid, 7,10, 13-eicosatriennoic acid and 5,8,11,14-arachidonic acid, were unsaturated fatty acids, and its content accounted for 61.45% of the total fatty acids.

结果］安卡鸡肌肉中共分离和鉴定出16种脂肪酸，其中饱和脂肪酸7种，包括月桂酸、豆蔻酸、十五烷酸、棕榈酸、十七烷酸、硬脂酸和花生酸，其含量占总脂肪酸的38.55%；不饱和脂肪酸9种，包括11-十四碳烯酸、9-十六碳烯酸、9-十八碳烯酸、9，12-十八碳二烯酸、6，9，12-十八碳三烯酸、11-二十碳烯酸、10，13-二十碳二烯酸、7，10，13-二十碳三烯酸以及5，8，11，14-二十碳四烯酸，共含量占总脂肪酸的61.45%。

Methyl-5-ethyl-2-thiouracil,m.p.211°,was prepared according to the direc- tions of Johnson and Baily.4-Methyl-5-ethyl-uracil,m.p.236°,was formed in a 81% yield from 4-methyl-5-ethyl-2-thiouracil by boiling the latter with an aqueous solution of monochloroacetic acid.4-Methyl-5-ethyl-uracil reacted with phosphorous oxychloride and phosphorous pentachloride,giving 4-methyl-5-ethyl-2,6-dichloropy- rimidine in a 79% yield.

14-甲基5-乙基-2，6-二氯代嘧啶曾用磷醯氯和五氯化磷与其相应的2，6-二羟基嘧啶作用制取。(2)4-甲基-5-乙基-2，6-二氯代嘧啶与醇钠作用，极易转变成4-甲基-5-乙基-2，6-二烷氧基嘧啶。(3)4-甲基-5-乙基-2，6-二甲氧基嘧啶和2-氧代-3，4-二甲基-5-乙基-6-甲氧基嘧啶在高温时重排成其稳定构型的的异构体：1，3，4-三甲基-5-乙基-2，6-二氧代嘧啶。

Based on isotopic ages and the cycle of magamtism, the ages of Yanbian granites can be subdivided into five periods:①late Permian granites (260-245Ma), the typical plutons are Liukesong and Liangbing plutons, and the main rock type include diorite-monzonitic-K syenogranites;②Triassic granites (225-200Ma), the typical plutons are Sandaogou, Chunyang, Qishiergedingzi, Dahuanggou, Naozhi, and Qinglinzi plutons, the main rock type include quartz dioritesgranodiorites-monzonitic-alkali granites;③early Jurassic granites (190-180Ma), which composed of quartz diorites-granodiorites - monzonitic ,and the typical plutons are Shimen, Miantian, Daxinggou and Yushuchuan rock;④Middle-Late Jurassic (170-150Ma), which composed of granodiorites- monzonitic- garnet-bearing muscovite granites, the typical plutons are Huangniling, Weizigou, Loutuoshan and Dongqing rock;⑤early Cretaceous (about 130Ma), the typical pluton is Zhongping pluton, and its rock type is paulite diorite.

另外，根据同位素年龄和岩石组合并考虑到岩浆的旋回性，将延边显生宙花岗岩进一步划分为五个期次：1。晚二叠世(260-245Ma)，代表性岩体为六棵松和亮兵，主体岩性为辉石闪长岩、二长花岗岩和钾长花岗岩；2。三叠世(225-200Ma)，代表性岩体为三道沟、春阳、七十二个顶子、大荒沟、闹枝、青林子，岩石组合为石英闪长岩—花岗闪长岩—二长花岗岩—碱长花岗岩，以花岗闪长岩和二长花岗岩为主；3。早侏罗世(190-180Ma)，石英闪长岩—花岗闪长岩—二长花岗岩组合，主体岩性为花岗闪长岩，代表性岩体有石门、棉田、大兴沟、榆树川等；4。中侏罗世(170-150Ma)，主体岩性为花岗闪长岩和含石榴石花岗岩，代表性岩体有黄泥岭、苇子沟、骆驼山、东清5。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。