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乙醇钠

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Influened the synthesis of ferrocene by the sodium ethylate method were researched in this paper.

研究了乙醇钠法合成二茂铁的影响因素:不同原料、原料配比、温度、时间、反应体系的氛围等,在选定的较优条件下,三茂铁的产率达到81.3%,并对二茂铁在柴油中的助燃、消烟作用进行了初步考察。

Under the conditions of homogeneous liquation, the reaction of ester exchange is completed.

以蔗糖、植物油为原料,乙醇钠为催化剂,脂肪酸皂及SE为促进剂,在均相熔融状态下进行酯交换反应合成蔗糖酯。

A new compound of merocyanine dye based on fullerene unit (2) was designed, synthesized and characterized by MALDI-TOF, FT-IR, NMR and UV-vis spectra and the allochroic processes were also studied.

并对化合物 2的变色过程进行了研究,发现该化合物对极性溶剂如甲醇、N ,N 二甲基甲酰胺和酸或碱如乙酸、乙醇钠等具有良好的变色过程。

Compound 2 had allochroic processes in polar solvents such as methanol or DMF. Acids or alkali such as acetic acid or NaOC_2H_5 also showed apparent influence on the allochroic process.

并对化合物2的变色过程进行了研究,发现该化合物对极性溶剂如甲醇、N,N-二甲基甲酰胺和酸或碱如乙酸、乙醇钠等具有良好的变色过程。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂,用粉末K2CO3代替常规使用的乙醇钠,在季铵盐和聚乙二醇混合相转移催化剂的存在下,含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应,得到相应的环化物。

In the fourth chapter, 5-phenyl-1,2,4-triazine(3) was synthesized from(5-phenyl-1,2,4-trizin-3-yl)hydrazine in the presence of sodium ethoxide firstly. Themerit of this process was simplification of operation and good yield (more than 90%),which to our knowledge has not been reported so far in literature.

第四章首先以(5-苯基-1,2,4-三嗪-3-基)肼为原料,在乙醇钠作用下经一步反应,合成了化合物5-苯基-1,2,4-三嗪(3);该法操作简单,产率高(>90%),迄今未见文献报道。

Ethyl 4,4,4-trifluoroacetoacetate was synthesized from ethyl acetate and 4,4,4-trifluoroacetate(mole ratio 3:1) with sodium ethoxide.

乙酸乙酯与三氟乙酸乙酯(摩尔比为3∶1)在乙醇钠作用下进行克莱森酯缩合反应,得到三氟乙酰乙酸乙酯。

Then sodium ethoxide was used as base,the nucleophilic substitution of 2-pyrrolidone with the intermediate provided nefiracetam.

以碳酸钠为缚酸剂,摩尔比为1︰1的2,6-二甲基苯胺与氯乙酰氯反应合成了中间体2-氯-N-(2,6-二甲基苯基)乙酰胺;在强碱乙醇钠作用下,2-吡咯烷酮再与2-氯-N-(2,6-二甲基苯基)乙酰胺经亲核取代合成了目标化合物奈非西坦。

The long wave ultraviolet grass green fluorescence function material is synthesized with the p-toluensulfonyl chloride and o-amino benzoic acid as raw materials,pyridine as solvent,and sodium ethoxide as activator.

缑卫军,刘新奇,紫外长波草绿荧光功能材料的合成研究以对甲苯磺酰氯和邻氨基苯甲酸为原料,吡啶为溶剂,乙醇钠为催化剂,合成紫外长波草绿荧光功能材料。

Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5:1)中和-2,6-二羟基甲苯环合得1,3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

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