乙醇钠

Optimized conditions are as follows:using ethanol solution of sodium ethylate as catalyst, themole ratio of ester to ketone is 1.2:1; the temperature is 90℃; the dosage of solvent is 10mLwith reaction time 5h.

通过正交试验得到了优化实验条件：以乙醇钠的乙醇溶液为催化剂，酯酮摩尔比为1.2：1，反应温度90℃，溶剂用量10mL，反应时间5小时。

The process of diethyl carbonate synthesis by transesterification reaction of ethanol with ethylene carbonate,coproducing useful ethylene glycol was investigated using catalyst of sodium ethylate .

研究了以乙醇钠为均相催化剂，碳酸乙烯酯和乙醇酯交换合成碳酸二乙酯同时联产乙二醇的过程。

The optimun technological conditions were studied on the synthesis of 9-flourenylmethanal by the reaction of flouren and ethyl formate , and the synthesis of 9-flourenylmethanol by the reaction of 9-flourenylmethanal and methanal with sodium ethylate as catalyst.

研究了乙醇钠为催化剂，由芴与甲酸乙酯合成芴甲醛，再由芴甲醛与甲醛合成苯甲醇的工艺条件，结果表明：合成芴甲醛时，当芴为 16g时，催化剂乙醇钠 4 。

From 3-chloropropene bycondensation with sodium ethylate in ethanol to form 3-ethoxypropene followed by anti-Markovnikov addition with HBr inthe presence of benzoyl peroxide.

3-氯丙烯与乙醇钠在乙醇中回流制得3-乙氧基丙烯，继而在过氧苯甲酰存在下，与溴化氢经反马氏加成制得1-溴-3-乙氧基丙烷，总收率89。

After esterification, the ethyl-2-chloro-3-phenylpropionate reacts with diethyl malonate under the catalysis of sodium ethylate, and we obtain the corresponding triethyl ester. The-benzylsuccinic acid is formed by the triethyl ester reacting with concentrate hydrochloric acid and taking place hydrolyzation and decarboxylation reaction at the same time. In order to avoid the formation of cinnamic acid, the sodium ethylate and diethyl malonate must be react sufficiently. The course has simple operation, inexpensive materials and better yield.

具体制备工艺为：首先以L-苯丙氨酸为原料采用重氮化方法得到-2-氯-3-苯基丙酸，再经酯化得到-2-氯-3-苯基丙酸乙酯后在乙醇钠催化作用下和丙二酸二乙酯缩合，发生SN2反应，得到相应的三乙酯，然后经水解和脱羧，得到-苄基丁二酸；在实验中乙醇钠要和丙二酸二乙酯充分反应，避免生成肉桂酸乙酯；该过程操作简单，原料便宜，产率较高，总收率可达到26.8%。

Michael addition reaction must be carried out in the base of the catalyst, the alkali used are: sodium, sodium ethoxide, sodium hydride, sodium amide ...

迈克尔加成反应必须在碱的催化下进行，常用的碱有：金属钠、乙醇钠、氢化钠、氨基钠。。。

The main products are as follows: Pharmaceutical Intermediate, Trimethyl Orthoformate , Triethyl Orthoformate, Sodium Methoxide, Power and solution Ethoxide,α-Chloropropionyl Chloride, Acetyl Chloride. Shandong Xinhua Junli Chemical Co.,Ltd.

公司主要产品为医药中间体，原甲酸三甲酯、原甲酸三乙酯、甲醇钠、乙醇钠、α-氯代丙酰氯、乙酰氯，其中原甲酸三甲酯、原甲酸三乙酯是国内唯一采用金属钠法工艺生产的企业。

Is located in Yellow River Delta, located in West Liuqiao Guangrao County Economic Development Zone, the brink of East Green high-speed, convenient transportation and strategic location, covers an area of 350,000 square meters, is a professional Companies are now built with an annual output of 3,000 tons glyoxylic acid, Allantoin 300 tons, 5,000 tons of sodium methanol, ethanol production of 5,000 tons of sodium scale.

广饶县弘达精细化工有限责任公司座落于黄河三角洲，位于广饶县西刘桥经济开发区，濒临东青高速，交通便利，地理位置优越，占地面积达350000平方米，是一家专业化公司，现已建成年产乙醛酸3000吨、尿囊素300吨、甲醇钠5000吨、乙醇钠5000吨的生产规模。

Compounds 3a-3d, 4a-4d, 5a-5d, 6a-6e and 7a-7e were prepared with a new efficient method, in which the aromatic amines were diazotized with isoamyl nitrite in EtONa/EtOH under refluxing condition, and mono -, bis -and tetrakis -substituted calix [4] arenes were obtained respectively as main product by diazo-coupling in different molar ratio to calix [4] arene.

一，提出了一个有效的新方法合成含有芳香偶氮基团的杯[4]芳烃衍生物3a-3d；4a-4d；5a-5d；6a-6e和7a-7e：即在非水溶剂乙醇中用亚硝酸异戊酯，在强碱乙醇钠存在下对芳香胺进行重氮化，得到芳香重氮酸盐沉淀，过滤，然后加入杯[4]芳烃的四氢呋喃溶液，通入CO〓气体调节溶液的pH值为7-9，使其发生偶联反应。

The optimun technological conditions were studied on the synthesis of 9-flourenylmethanal by the reaction of flouren and ethyl formate , and the synthesis of 9-flourenylmethanol by the reaction of 9-flourenylmethanal and methanal with sodium ethylate as catalyst.

研究了乙醇钠为催化剂，由芴与甲酸乙酯合成芴甲醛，再由芴甲醛与甲醛合成苯甲醇的工艺条件，结果表明：合成芴甲醛时，当芴为 16g时，催化剂乙醇钠 4 。5g ，甲酸乙酯 66ml，反应时间为 36h ，收率 75 %：合成芴甲醇时，当芴甲醛为 19g时，甲醛 7.0ml，10 %NaOH溶液 70ml，反应时间 2 。0h ，收率：63

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。