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乙醇酸

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Phenoxyethanol,Caprylyl Glycol,Sorbic.

胺四乙酸四钠,香精,苯氧乙醇,辛二醇,山梨酸。

With the observation of the outward appearances, it can be known roughly that if the sample was added with adulterations. Since the beeswax dissolves in the benzene but the adulterations, such as gypsum, starch and so on do not, these can be determined. By the verification of acid value and alcohol dissolve ability, the acid or non acid added can be determined. By the change of saponification value, the ester or non ester added can be determined. By the carbonification degree in the concentrated sulphuric acid, the mineral wax, such as paraffin wax added can be determined.

通过样品外观的观察初步定性是否掺有杂质;利用纯蜂蜡在苯中溶解,而掺入的石膏、面粉和淀粉等杂质在苯中不溶而定量鉴定这类杂质;由酸值变化和乙醇溶解物的量,测定掺入的硬脂酸等酸性物质或其它的非酸性物质;由皂化值变化,定量测定掺入的动物脂等酯类物质或其它的非酯类物质;根据蜂蜡中的烃类在浓硫酸中可被炭化,加入的石蜡等矿物蜡不被炭化来测定此类掺杂物。

In addition, the activties of different catalyst were compered. The test proved the chloroplatinic acid– ethanol catalyst provides high yields of addition products without the formation of undesirable by-products, to provide the possibility of using less rigorous reaction condition, to provide a catalyst material, which is effective at low concentrations.

实验过程中特别对不同催化剂进行了比较,其中氯铂酸—乙醇催化剂提高了加成反应的产率,没有副产物生成,不需要苛刻的反应条件,在低浓度时有很好的催化效果。

Polyether modified polysiloxane was synthesized by the hydrosilation reaction of hydrogen containing silicone fluidand allyl polyether, using chloroplatinic acid as the catalyst.

以氯铂酸为催化剂,利用含氢硅油与烯丙基聚醚的硅氢加成反应,合成出聚醚改性硅油;然后用乙醇胺进行胺化反应,制成纸张用氨基改性聚醚硅油柔软剂。

And cinnamic aldehyde and cinnamic acid were extracted from cinnamon by MAE using water and ethanol as solvents and were analyzed by HPLC method.

利用聚焦式微波辅助萃取系统,结合HPLC分析,对肉桂中的肉桂醛和肉桂酸进行微波萃取分离和分析,并比较了水及乙醇等溶剂作为萃取溶剂的效果。

Densities and viscosities of the binary mixture of ethyl crotonate with ethanol at different compositions were determined at the temperature range from 293.15K to 343.15K and under atmospheric pressure by using a vibrating U-shaped tube densimeter and Ubbelohde suspended-level viscometer.

在常压下采用U形振动管密度计测定了巴豆酸乙酯与乙醇的混合液在293.15~343.15K下的密度。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂,用粉末K2CO3代替常规使用的乙醇钠,在季铵盐和聚乙二醇混合相转移催化剂的存在下,含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应,得到相应的环化物。

The ethanol extract was dissolved with HCl, the acidic extract was basified to pH9-10 with NH_3-water and extracted with CHCl_3 to give total alkaloids. five alkaloids were isolated with column chromatography and preparative thin-layer chromatography, and three of them were identified as dehydrocorydaline、 corynoline and dihydrosanguinarine on the basis of spectral analysis MS,~1H-NMR,~(13C-NMR and physicochemical properties. All of them were found for the first time from this plant.

为研究灰绿黄堇的化学成分,本文将灰绿黄堇乙醇提取物采取酸提取、碱游离后萃取的方法得到总生物碱,然后利用柱色谱、制备薄层色谱等方法分离、纯化了灰绿黄堇中5种生物碱,并利用IR、MS、~1H-NMR、~(13)C-NMR等方法鉴定了其中的3种,分别为去氢紫堇碱、紫堇灵、二氢血根碱,均为首次在此植物中发现。

After analyzing the reaction mechanism through literature, we think the reaction from diethanolamine to iminodiatic salt is composed of two steps—reaction from alcohol to aldehyde and the disproportionation reaction of the aldehyde. The selectivity, conversion, rate of this reaction are mainly attributed to the capability of this catalyst.

通过查阅文献资料,分析了反应机理,认为二乙醇胺脱氢生成酸是由两步反应组成─醇脱氢生成醛与醛的歧化,催化剂的性能是影响反应转化率、选择性及反应速度的主要因素,确定了采用沉淀法制备Cu/ZrO2做催化剂。

In order to carry out the separation of the azeotropic mixture dipropyl ether + 1-propyl alcohol by extractive distillation, we are studied the influence on the phase equilibria behavior four different solvent: 1-pentanol [2], butyl propionate [3], N,Ndimethylformamide [4] and 2-ethoxyethanol.

为了用萃取性蒸馏法分离二丙醚和1-丙醇组成的共沸混合物,我们正在研究4种不同溶剂对相平衡行为的影响:1-戊醇[2]、丙酸丁酯[3]、N,N-二甲基甲酰胺[4]和2-乙氧基乙醇。

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