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乙醇酸

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Optimization of the extracting method of Chlorogenic Acid from Flos Lonicerae was studied by three different methods of ultrasonic extraction, sorbitic extraction, and improved method of sorbitic extraction.

采用超声波法、索氏法、改良索氏法3种方法分别从金银花中提取绿原酸,用紫外光谱法和高效液相色谱法对其进行定性定量分析。同时用金银花乙醇提取物及纯化的绿原酸对乳房炎主要致病菌进行抑菌试验。

Both of adsorption of VB〓 on sulphonic resin in Zn〓form from ethanol and caffeine on sulphonic resin in Cu〓 form from ethyl acetate is considerable, with saturation adsorption capacity 60 and 76mg/g respectively.

磺酸锌型树脂对乙醇中VB〓、磺酸铜型树脂对乙酸乙脂中咖啡因和丙烯酸铁型树脂对甲醇中的鞣酸均具较好的吸附性能,其静态饱和吸附量分别为60、76和34mg/g。

Six crystalline substances were isolated from the stem and root of Syzygium buxifoli um and identified as friedelin,βsitosterol,ursolic acid,pomolic acid,oleanolic acid and βdaucosterol..

摘要从赤楠的茎和根部的乙醇提出物中,分离和鉴定了6个化学成分,分别为木栓酮,β谷甾醇,乌苏酸,19α羟基乌苏酸,齐墩果酸和胡萝卜甙。

In addition, a further study was made of the technique of extraction, isolation and purification of GLA. The factional extraction used in the laboratory with n-hexane and ethanol was changed into the whole extraction of 6〓 solvent, which simplified production technique and reduced cost of production. The fungal lipid extracted from the fermentation in the medium-scale test was concentrated by the urea adducting method with methanol as solvent, at 75~80℃ for 3 hours. After GLA had been adducted twice, the content of GLA came up to 84. 25%, around a twelfth as much as the original concentration.

并对γ—亚麻酸的提取和分离纯化工艺进行了研究,将实验室中用正己烷和乙醇分步抽提的工艺改为用6〓溶剂一步抽提技术,从而简化了生产工艺,降低了生产成本;采用脲素包合法,以甲醇作为溶剂,温度控制在75~80℃,包合时间为3h,对中试发酵所提取的菌油进行了浓缩,γ—亚麻酸两次包合后,GLA含量达到84.25%,比原浓度浓缩了近十二倍。

During the preparation, when the water was used as solvent, the sodium stearate is dispersed by the acid-base neutralization reaction between sodium silicate and stearic acid in water solution, and is encapsuled by the reverse reaction; while when the alcohol/water mixed solution was used, the dispersion and encapsulation of the stearic acid is accomplished via esterification and hydrolysis in alcohol/water solvent.

具体为:以水为溶剂时,利用十八烷酸与水玻璃间发生的酸碱正反应解决其分散问题,而利用其逆反应完成相变材料的包裹,以乙醇/水为混合溶剂时,则利用其酯化、水解双向反应分别完成十八烷酸的分散、包裹过程。

METHODS:Ceftizoxime acid was prepared with 7-Amino-3-norcephem-4-carboxylic acid(7-ANCA)and AE-ester ceftizoxime acid as raw material;then ceftizoxime sodium was obtained through the reaction between ceftizoxime acid and sodium carbonate.

以粗品7-氨基-3-烷基头孢烷酸和AE活性酯为原料合成头孢唑肟酸,再与无水碳酸钠反应制得头孢唑肟钠;同时研究反应时间、乙醇用量和滴加时间、无水碳酸钠的用量以及pH值对产品质量的影响。

Micro/nanorods water-soluble copper glycine were synthesized by the reaction of glycine and copper acetate on a large scale via organic solvent-induced crystallization.

以甘氨酸和醋酸铜作为反应物,通过乙醇溶剂析出法大量制备水溶性甘氨酸铜微/纳米棒。

Thinking of presenting problems, this research mainly studied some solid base catalysts which own higher catalysis ability and longer lifetime. Then, the phase diagram and equilibrium data of oil-alcohol-biodiesel-glycerol multiphase system were measured because the biodiesel producing process lacks of thermodynamic data.Based on a double-membranes theory and the thermodynamic data, a kinetic model was proposed. In addition, a mult-step extraction process was proposed to dispose the jatropha curcas l oil with high acid value in order to decrease the acid value. Then, a new technology of biodiesel producing using solid base as a catalyst was developed. The study objects and results are as follows.

本研究针对负载型固体碱催化剂活性组分易流失、使用寿命短的缺点,制备了高效、稳定的固体碱催化剂;针对生物柴油制备体系热力学数据缺乏的问题,测定了大豆油-醇-生物柴油-甘油体系的相图和平衡特性,在此基础上基于双膜理论,建立了固体碱制备生物柴油的动力学模型;同时针对酸价较高的麻疯果油,提出了先用甲醇或乙醇多级萃取降低酸价,再用固体碱催化制备的新工艺。

This thesis put that, although ETF and BATF had the same biogas yield, their hydrogen yields were remarkably different in the same testing condition because the hydrogen content in their produced biogases were different due to the difference of their metabolic pathways.

本研究先后从连续流反应系统的乙醇型发酵阶段和丁酸型发酵阶段分别7次采集分离样品,从中分离到215株产酸发酵细菌,其中有36株具有产氢能力。

In this experiment, some strains of yeast were separated from koumiss in 4 regions of 3 nations, 3 strains of which were chosen to make the koumiss by the mixed fermentation under the experimental condition with the lactic acid bacteria. In fermentative process the alcohol content variation was measured.

从3个国家4个地区的酸马奶中共分离筛选出多株酵母菌,并筛选出3株酵母菌在实验室条件下与乳酸菌进行混合发酵制成酸马奶,测定发酵过程中的乙醇含量变化。

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