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Methods Cyclohexane, ethyl acetate and glacial acetic acid (8∶8∶0.8) were used as the developing solvent. Samples were analyzed on a layer plate of silica gel G thin by using 20% phosphomolybdic acid as chromogenic agent.

以环己烷乙酸乙酯冰醋酸(体积比8∶8∶0.8)为展开剂,以羧甲基纤维素钠为黏合剂自制硅胶G薄层板,20%磷钼酸溶液为显色剂,进行薄层色谱分析。

The results show that the resulting product can be separated by the mixture of petroleum ether, aether and acetic acid (10:10:1, V/V). Among them, the oleic acid component can be eluted by the mixed solvent of ethanol and carbon tetrachloride (35:15, V/V), and then productivity of sodium oleoyl sarcosine can be obtained.

结果表明:用石油醚:无水乙醚:冰乙酸=10:10:1分离产物中的组分,再用无水乙醇:四氯化碳=35:15混合溶剂洗脱制备油酸组分,进而计算油酰肌氨酸钠的产率是可行的。

2 The analysis step by 125mL separatory funnel, a fartoo 0.1mL cadmiun forcultivation added liquid (equivalent 1 μ g cadmiun) and 50mL acetate (4%), and the other one is to join the 50.0mL sample lixivium, separatory funnel and 2mL in the seignette solution,-amoxycillin sodium hydroxide solution and potassium cyanide-2mL hydroxylammonium hydrochloride solution, each adding a reagent shake after.

9.2.2 分析步骤取125mL分液漏斗两只,一只加入0.1mL镉标准使用液(相当1μg镉)及50mL乙酸(4%),另一只加入50.0mL样品浸泡液,分别向分液漏斗中各加2mL酒石酸钾钠溶液,10mL氢氧化钠-氰化钾溶液及2mL盐酸羟胺溶液,每加入一种试剂后均须摇匀。

A method for simultaneously determining sorbic acid, benzoic acid and saccharin sodium in processed fishery product was established.

采用高效液相色谱法同时测定水产品中的山梨酸、苯甲酸、糖精钠,实验采用铁氰化钾和乙酸锌作沉淀剂,取得了良好的净化效果。

In addition, we used a modified MTT 3-(4,5-dimethylthiazol-2-yl-2,5-diphenyltetrazolium bromide assay to examine cell proliferation by dissociating the cell/alginate constructs using trisodium citrate and trypsin/EDTA.

此外,我们用改良的MMT测定被枸橼酸钠-胰蛋白酶-乙二胺四乙酸分离细胞结构的细胞增殖情况。

Results: Solution concentration range depended on 0.5~50 mg/L lineaity, relation fine, the relevance modulus amounted to 0.999 without exception. The soursulfan acet ophenetidin ilamide potassium, benzoic acid, dehydro aectic acid, sorbic acid, saccharin sodium minium inspects up out tickness being 0.062, 0.074, 0.066, 0.370, 0.105mg/L The standard deviation was smaller than 5.0%. The additive hit hack rate was 96.8% in drink pickle and the nature bean product fermenting 101.6%.

结果:本方法测定食品中5种添加剂,溶液浓度范围在0.5~50mg/L线性关系良好,相关系数均达0.999;乙酰磺胺酸钾、苯甲酸、脱氢乙酸、山梨酸、糖精钠最小检出浓度分别为0.062,0.074,0.066,0.037,0.105mg/L;标准偏差均小于5.0%;饮料、酱菜和发酵性豆制品中添加剂的回收率为

The concentration of calcium ion in the decalcifying solution was measured by Inductively Coupled Plasma Optical Emission Spectrometer.

分别应用微波、超声波、联合波和常规方法,在室温下用10%乙二胺四乙酸二钠脱钙。

The similar nicotinoyltrifluoroacetones are synthesized from acetylpyridine and ethyl trifluoroacetate through Claisen reaction.The influnences of alcoholic natrium,reaction temperature and solvent on reaction yield is studied.The subliming method is improved.

本文以乙酰吡啶和三氟乙酸乙酯为主要原料,利用克莱森酯缩合反应,合成了三种相似结构的吡啶甲酰三氟丙酮化合物,考察了碱性试剂醇钠、反应温度和溶剂等因素对反应产率的影响,改进了纯化产物的方法。

Producing Creatin monohydrate, Ctreatine anhydrous, Taurine, Tri-Craetine citrate, Tricreatine Malate, Creatine Ethyl ester Glycocyamine, Guanidino propionic acid, etc.

生产一水肌酸,无水肌酸,肌酸乙酯,牛磺酸,三肌酸苹果酸,三肌酸柠檬酸,胍基乙酸,胍基丙酸,肌氨酸钠,面粉增白剂等食品添加剂等。

Using phosphorus trichloride as the base raw material, we try out the water dosage on hydrolysts, drop quomodo of phosphorus trichloride, the ratio of phosphorus trichloride and MSIDA, other trial operate, and find out the best synthesis method.

用三氯化磷为基本原料,研究了水解用水量、三氯化磷滴加方式、三氯化磷与亚氨基二乙酸一钠盐的配比和工艺操作条件等因素的影响情况。

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