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Methods Star anise were extracted from Illicium verum Hook.f. using ethanol and ethyl acetate as solvents. After macron absorption resin layer separation, a kind of white fine powder shikimic acid were obtained. The extracted shikimic acid were determined for chemical qualitative analysis. Writhing test and warm bathing test were performed and observed the mice pain threshold latency and writhing reaction times after giving peritoneal shikimic acid extraction solutions.

采用乙醇提取、乙酸乙酯等有机溶剂萃取八角茴香,经大孔吸附树脂柱分离,得到白色精细粉末的莽草酸,并对莽草酸进行化学定性分析,镇痛实验采用扭体法和温浴法,观察腹腔注射莽草酸溶液后小鼠痛阈潜伏期和扭体反应的次数,设阿司匹林和生理盐水为对照组。

After macron absorption resin layer separation, a kind of white fine powder shikimic acid were obtained. The extracted shikimic acid were determined for chemical qualitative analysis. Writhing test and warm bathing test were performed and observed the mice pain threshold latency and writhing reaction times after giving peritoneal shikimic acid extraction solutions. Aspirin and normal saline were used as controls.

采用乙醇提取、乙酸乙酯等有机溶剂萃取八角茴香,经大孔吸附树脂柱分离,得到白色精细粉末的莽草酸,并对莽草酸进行化学定性分析,镇痛实验采用扭体法和温浴法,观察腹腔注射莽草酸溶液后小鼠痛阈潜伏期和扭体反应的次数,设阿司匹林和生理盐水为对照组。

Why did the addition of oxaloacetate or malate stimulate oxygen consumption?

为什么草酰乙酸或苹果酸的加入促进了氧的消耗?

RESULTS: After 3 days of operation, the BMP positive cells were found in the matrix of experimental group I.

将自体成骨样细胞即刻种植在胶原包埋的聚羟基乙酸基质材料上,然后将该复合体或单纯基质材料移植到兔颅骨的一侧全层骨缺损区,作为实验侧或实验侧。

Both of the thermophiles were motile by means of lophotrichous flagella and had high growth rate on medium containing cellulose. Optimal growth occured at 60℃ for the two thermophiles and at PH 7. 5 for Y, PH 7. 37. 5 for W strain. Y strain produced yellow pigment in cellulose medium and had yellow-colored, round or watery colonies in cellulose agar. The colonies of W strain were white -colored and similar in form to that of Y strain. The mesophile, Clostridium sp. B, was motile with peritrichous flagella. The colonies grown on cellulose agar were white and round with slightly undulate margins. The optimal growth temperature and PH of B strain were 40℃ and 7. 0-7. 2, respectively. All of the three Clostridia fermented varieties of carbohydrates and in cellulose media produced the similar end-products: CO〓H〓, ethanol and acetic acid. The DNA compositions were 34 mol% for Y and B, 35 mol% for W strain.

嗜热菌y与w在含纤维素的培养基中生长迅速,其最适生长温度均为60℃;最适PHy为7.5,w为7.3-7.5.y菌在纤维素培养基中产生黄色,在纤维素琼脂中菌落为黄色并呈圆形或流动粥样。w菌落为白色,但形状与y菌类似,嗜温菌B在纤维素琼脂上菌落为白色,圆形,边缘呈微小波状,最适PH与温度分别为7.0-7.2和40℃,三支菌都可发酵多种碳水化合物,且在纤维素培养基中产生同样的产物:CO〓H〓,乙醇和乙酸,三者DNA组成分别是y为34mol%,w 35mol%,B 34mol%。

This invention publishes a preparation method for methyl acetate and a reaction distillation column with combined trapezoid spray trays.

本发明公开了一种乙酸甲酯的制备方法和具有立体传质塔板的反应精馏塔。

The results showed that the optimal parameters of transesterification reaction were: molar ratio of methyl acetate to oil 14:1, 30% enzyme added based on oil weight, temperature 40℃ and reaction time 14 h.

研究结果表明,最佳酯交换条件为:脂肪酶Novozym 435加入量为棉籽油质量的30%,乙酸甲酯和棉籽油的摩尔比14:1,反应温度40℃,反应时间14 h。

In order to test the validity of this method, the saponification of methyl acetate, ethyl formate and methyl formate in aqueous solution at 25℃ has been studied.

研究了25℃下乙酸甲酯、甲酸乙酯和甲酸甲酯在水溶液中的皂化反应,其计算结果与文献值相吻合,从而验证了热弛豫法的正确性。

The Monpac Straight Batons are another innovation from Monadnock to provide a cost effective baton that won't bend, warp or splinter.

乙酸乙酯系列单体防暴棍是莫纳德诺克公司的另一款高性能的新品,不会弯曲、凹陷和碎裂。

A series of 3-naphthyl-2--1,3-thiazolidin-4-ones were synthesized by the three-component one-pot cyclocondensation of naphthylamine, aromatic aldehyde and 2-mercaptoacetic acid using a microwave-assisted method in the presence of DMAP/DCC.

利用微波促进的多组分一锅法,在封管条件下,以萘胺、芳醛和巯基乙酸为原料,4-二甲氨基吡啶/N,N'-二环已基碳二亚胺为催化剂,合成了系列新的噻唑烷酮衍生物,该反应具有时间短、操作简便等优点。

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