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A new type of difunctional initiator (benzyl dibromide, ethyl dibromoacetate) was proposed in this paper and used to synthesize poly based triblock copolymers such as PSt-PBA-PSt, PMMA-PBA-PMMA.

本论文提出一种新型ATRP双官能团引发剂(如α,α-二溴化苄、α,α-二溴乙酸乙酯),并用聚合反应速度法、GPC法、核磁分析法进行双官能度的验证,并通过两步聚合合成以聚丙烯酸酯为中间嵌段、苯乙烯或甲基丙烯酸甲酯为两端嵌段的ABA型三嵌段共聚物。

The effect of the addition of trisaminomethane on the separation of diethylstilbestrol and its cleavage product wasstudied.

该方法中以甲醇作为溶剂,以乙酸钠作为电解质,研究了三羟甲基氨基甲烷的加入对分离己烯雌酚及其分解产物的影响。

The velocities of reaction of ethyl acetate with sodium hydroxide in dioxane- water mixture have been determined in seven different temperatures(5°,10°, 15°,20°,25°,30°and 35°).

作者在7具不同温度(5°,10°,15°,20°,25°,30°,35°)下,研究了乙酸乙酯和氢氧化钠在二氧六圜和水的混合溶剂中的反应速度。

Dioxane was selected as solvent. The linear range for methanol was 6-54mg/L for ethanol and ethyl acetate both were 10-90mg/L. The average recovery of them was 99, 36, 101.26% and 101.57% respectively.

在上述色谱条件下,甲醇的线性范围为6-54mg/L,乙醇和乙酸乙酯的线性范围为10-90mg/L;平均加样回收率分别为99.36、10l.26%和101.57%。

A porous lanthanum-doped hydroxyapatite coating on commercially pure titanium was prepared by micro-arc oxidation in electrolytic solution containing calcium acetate,β-glycerol phosphate disodium salt pentahydrate and lanthanum nitrate.

采用微弧氧化法在含有乙酸钙、β-甘油磷酸钙、硝酸镧的电解液中在纯钛金属表面原位生成了多孔含La羟基磷灰石的生物涂层。

The mechanism was supposed as follows: polyfluoroalkyl iodides were initiated by sodium dithionite to give R〓 which was added to one double bond of diallylacetic acid, after the sequential radical cyclization and nucleophilic substitution to form bicyclo-lactones.

这是因为:多氟烷基碘化物在连二亚硫酸钠的引发下,得到自由基R〓,后者加成到二烯丙基乙酸中的一个—C=C—双键上,然后在碱性介质中进行分子内亲核反应得到双环内酯类产物。

The experimental data also shows that the energy gap for electron transition of acetic acid molecules does not change in various molecular associations.

实验数据还表明:不同的分子缔合结构并不改变乙酸分子中的电子跃迁能级间隔。

Object: The antimicrobial effects of the water, 60% alcohol, 90% alcohol extract and petroleum ether, ethyl acetate, n-butanol components from Pomegranate rind against 3 kind of pathogenesis bacterial and 14 kind of epiphyte were accomplished.

目的:对石榴皮的水、60%乙醇、90%乙醇提取物以及石油醚、乙酸乙酯、正丁醇萃取物对3种细菌和14种真菌的体外抗菌试验进行了研究。

Its catalytic activity in the esterification to form ethylacetate was investigated with the highest yield of 96.2%.

在乙酸乙酯的合成反应中考察了该催化剂的催化活性。

It is the first time that the petroleum ether extract and ethyl acetate extract of Nerviliafoadii.

首次确定了青天葵的石油醚和乙酸乙酯部位是体内抗肿瘤作用的有效部位。

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