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The variance of ABA of grape during storage were discussed in this paper.The following results are been drawn:the change of the content of ABA of grapes during storage characterizes by a parabolic shaped curve with obvious peak.Low temperature (0±0.5℃) is conducive to delaying the appearance of the peak of ABA and reduces the peak value.Nine kinds of plant growth regulators and two kinds of chemicals were chosen to treat grape bunches so as to study their mechanisms on ABA of grapes,2,3,5 triiodobenzoic a...

试验研究了葡萄贮期脱落酸的变化,结果表明:葡萄贮期 ABA含量呈抛物线形变化,有明显的高峰出现,低温( 0± 0 。5℃)贮藏具有推迟 ABA峰期和降低峰值的作用,经用 9种植物生长调节剂和 2种化学药品对葡萄果穗处理试验,三碘苯甲酸对 ABA的形成有极强的抑制作用,吲哚- 3-乙酸、赤霉素( GA3)、萘乙酸和 6-苄基氨基嘌呤( 6- BA)对 ABA的形成也具有拮抗作用,矮壮素、比久( B9)、乙烯利和外源脱落酸对 ABA的形成有促进作用。

The use of benzazepin-N-acetic acid derivatives which contain an oxo group in the a position to the nitrogen atom and are substituted in the 3 position by a 1--cyclopentyl-carbonyl-amino radical, and of their salts and biolabile esters, for the prophylaxis and/or treatment of heart damage caused by cardiotoxic doses of medicaments or chemicals, in larger mammals and in particular humans.

本发明涉及苯并氮杂∴-N-乙酸衍生物及其盐和生物不稳定的酯的应用,其中苯并氮杂∴-N-乙酸衍生物在氮原子的α位置含有氧代基,且在3-位置上被1--环戊基-羰基-氨基残基取代,用于预防和/或治疗大的哺乳动物和特别是人体的心脏损伤,其中心脏损伤是由心脏中毒剂量的药物或化学品引起的。

Toxicity and repellent activity of several plant-based compounds on Blattella germanica were studied, results showed that rotenone, toosendanin and azadirachtin had stomach toxic effect on Blattella germanica, rotenone showed high stomach toxicity and all insects died after 8 hours, matrine also has deformative effect on Blattella germanica , matrine and toosendanin can affect oviposition of Blattella germanica; repellent activity of these botanicals was further studied, results showed that bering hydrochloridum, azadirachtin and sparteinehave had repellent activity against Blattella germanica, observation also showed that rotenone and bering hydrochloridum had high contact toxicity against Blattella germanica, the time of all insects knocked down were 8 and 48 hours.

选取了7种植物源化合物,测定了它们对德国小蠊的毒性和驱避性,结果表明,鱼藤酮、川楝素和印楝素对德国小蠊具有不同程度的胃毒作用,其中鱼藤酮乙酸乙酯溶液作用较强,8小时死亡率已达100%,川楝素和印楝素对德国小蠊也表现出一定的毒杀作用,观察还发现印楝素和苦参碱对德国小蠊的发育有致畸作用,苦参碱和川楝素影响其卵鞘形成;进一步对这几种化合物的驱避性进行研究,结果表明盐酸黄连素、鱼藤酮乳油和印楝素乳油对德国小蠊有不同程度的驱避作用,其驱避率分别为96.7%、51.3%和50.1%,另外观察到鱼藤酮乙酸乙酯溶液和盐酸黄连素对德国小蠊具有较强的触杀活性,供试虫全部被击倒的时间分别为8小时和48小时。

Qualitative and quantitative analysis of chemical constituents.(1) Based on the GC spectrum of 2 species, Whitmania pigra and Poecilobdella manillensis shows little difference between them. 24 kinds of fatty acid in Whitmania pigra was firstly separated and determined by GC/MS. Among them, phenylacetic acid is a component which has active of anticancer. The existence of many unsaturated fatty acid provides chemical evidence for ShuiZhi's functions of invigorate the circulation of blood.

六首次对两种水蛭的脂肪酸类化合物进行了GC定性分析,发现其脂肪酸组成未见明显差异,后又对宽体金线蛭的脂肪酸类化合物进行了GC-MS分析,初步鉴定出24个化合物,包括苯乙酸、龙脑和22种脂肪酸,其中所含的苯乙酸具有抗肿瘤活性,大量不饱和脂肪酸的存在为水蛭在血液流变学方面的药理作用提供了一定的化学依据。

The distillation column with a single photochlorination reactor was built in this paper, which is used in the laboratory study. In light initiation, the semi-continuous operation was applied to study the influence of the chlorine flow, the reflux and the height of the packing on photochlorination of acetic acid. Crude MCA with a purity of 90% or more was attained and the feasibility of this technology was proved.

本文建立了适合实验室研究的背包式光氯化反应精馏耦合装置,采用半连续操作的方法,在光引发条件下,考察了氯气流量、回流量和填料高度对乙酸光氯化反应的影响,得到了含量达90%以上的氯乙酸粗品,证实了工艺的可行性。

M treatment materials, and also tartaric acid and no maleic acid detected in G. v treatment materials. Inoculation also increased the content of organic acid secretion (increased by 19.80~56.87 mg/kg) of trifoliate root, and the application of AlPO4 greatly increased organic acid content (increased by 20.06~21.84 mg/kg); uninoculated plant root secreted a bit of organic acid; Mycorrhizal poncirus trifoliata seedlings excreted malic acid (42.87%), citric acid (39.22%) and oxalic acid (12.06%).

接种AM真菌的根系分泌的有机酸种类与对照有所不同,未接种处理枳分泌的有机酸有草酸、苹果酸、乳酸、乙酸、顺丁烯二酸和柠檬酸等6种,而接种G.m的则检测到草酸、酒石酸、苹果酸、乳酸、乙酸、柠檬酸、丁二酸等7种,G.v处理的检测到酒石酸,接种处理均未检测到顺丁烯二酸;接种丛枝菌根真菌增加了枳根系分泌有机酸的量比未接种处理增加19.80~56.87 mg/kg,且施用AlPO4后有机酸含量显著增加(增加20.06~21.84 mg/kg;未接种植株根系仅分泌少量有机酸;接种植株根系分泌的有机酸以苹果酸(42.87%)、柠檬酸(39.22%)和草酸(12.06%)为主。

Accordingly a further feature of the invention is a combined process wherein a dialkyl phenylethylmalonate is made from an alkyl phenylacetate and a dialkyl carbonate by a process comprising adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C, at least a chemically equivalent proportion of a lower aliphatic alcohol, subsequently adding an approximately equivalent proportion of a dialkyl carbonate and of an alkyl phenylacetate, heating the mixture to induce reaction and continuously distilling out the alcohol formed from the reaction zone and finally causing the sodio diethyl phenylmalonate so obtained to interact with an ethylating agent, such as ethyl halide, diethyl sulphate of ethyl p-toluene-sulphonate.

因此,本发明的另一个应用是一个组合工艺过程:二烷基苯基乙基丙二酸酯由烷基乙酸苯酯和二烷基碳酸酯得到,具体工艺过程是:向覆盖有沸点超过一百摄氏度的团庆化合物溶剂的金属钠中添加至少化学平衡的低级脂肪族醇,然后加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯,加热混合物引导反应进行,持续蒸馏把形成的醇类从反应区域移出,最后使获得的二乙基苯基丙二酸酯和乙基化试剂如卤代乙烷,二乙基硫酸酯形成乙基p-甲苯磺酸酯。

A combination analysis of SIP and in situ microbiological methods was applied on the anaerobic digestion of biomass organics suffering from severe acids inhibition. The studies found that accumulated acids were degraded mainly by Methanosarcina firstly with acetoclastic pathway and then with hydrogenotrophic pathway under mesophilic condition, whereas acids were mainly degraded to methane by the tandem reactions of syntrophic acetate oxidation and hydrogenotrophic methanogenesis under thermophilic condition.

联合应用稳定同位素表征技术和微生态原位表征方法,对高浓度有机酸胁迫条件下的生物质类有机物厌氧发酵甲烷化途径的研究结果表明,面临高浓度有机酸迅速累积的环境,中温发酵条件下,优势菌种为甲烷八叠球菌,依时间次序,通过乙酸发酵和氢营养型途径利用累积的有机酸产生甲烷;而在高温条件下,有机酸则通过乙酸氧化和氢营养型甲烷化途径的串联反应被降解。

According to the results of the former study in our laboratory, trans-1, 2-cyclohexanediol is produced with a lot of acids and water, for extraction of trans-1, 2-cyclohexanediol from the solution, ethyl acetate and butyl acetate were used as extraction reagents, the solubility data of the trans-1, 2-cyclohexanediol in corresponding mixed solvents of some sorts of acetates and water are needed.

根据本实验室前期研究结果可知,反式-1,2-环己二醇是在酸性和大量水存在的条件下得到的,为了把反式-1,2-环己二醇从反应液中萃取出来,本工艺所采用的萃取剂是乙酸乙酯和乙酸丁酯,需要获得反式-1,2-环己二醇在这些酯类与水混合溶剂中的溶解度数据,因而对反式-1,2-环己二醇进行相关固液相平衡的研究是非常迫切和必要的。

The dissociation constants and the reaction rate constants of inclusion complexes formed between α、β—cyclodextrin and several naphthyl esters (α—naphthyl acetate,β—naphthyl acetate,β—naphthyl caproate) were obtained by kinetics of hydrolyses of naphthyl esters.

通过几种脂肪酸萘酯(乙酸-α-萘酯、乙酸-β-萘酯、己酸-β-萘酯)的环糊精催化水解研究得到了它们同环糊精所形成的包接络合物的分解平衡常数和反应速度常数,进而提出了它们同环糊精所形成的包接络合物的结构模型。

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