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It,s allelchemicals were isolated through extraction, thin-layer chromatography, and column chromatograpathy. After the white clover was infused in ethanol and evaporation, the leavings was dissolved by water. The aqueous extract was extracted by petroleum,chloroform, ethyl acetate and n-Butanol successively, and the bioassay showed that the chloroform phase has obvious inhibitory effect, the inhibitory rate was 44.32%,88.08% on Abutilon theophrasti M., seedling length and root length, 82.08%,92.16% on Echinochloa crusgalli L., seedling length and root length, and the Amaranthus retroflexux L., germination rate is 0, the secondly was ethyl acetate phase.

运用萃取、薄层层析、柱层析等方法对白三叶草地上部分的化感物质进行初步分离,结果表明,白三叶草经乙醇浸提旋转蒸发后用蒸馏水溶解,依次用石油醚、氯仿、乙酸乙酯、正丁醇萃取,生物测定表明氯仿组分对杂草的抑制作用最强,对苘麻芽长和根长抑制率分别为44.32%、88.08%,对稗草芽长和根长的抑制率分别为82.08%、92.16%,反枝苋的发芽率为0;其次是乙酸乙酯相。

Based on the analysis of the chromatogram of flavoring compositions of Taishan Tequ, 13 kinds of flavoring compositions including n-propanol, isoamyl alcohol, ethyl caproate, ethyl lactate, ethyl acetate, ethyl butyrate, caproic acid, acetic acid, butyric acid, acetaldehyde, acetal, total acids and total esters were determined as the chromatogram skeleton compositions of Taishan Tequ. The physiochemical indexes of Taishan Tequ could be under proper control through the stipulation of the content range of the above flavoring compositions, which is an effective way to liquor quality improvement and stability and has greatly improved the blending techniques of Taishan Tequ.

以泰山特曲酒香气成分色谱分析结果为基础,确定了正丙醇、异戊醇、己酸乙酯、乳酸乙酯、乙酸乙酯、丁酸乙酯、己酸、乙酸、丁酸、乙醛、乙缩醛、总酸、总酯这13种香味成分作为泰山特曲的色谱骨架成分来控制成品酒理化指标,并制订了控制范围,使泰山特曲的勾兑技术有了飞跃的发展,成为提高与稳定产品质量的有效方法。

Chapter two 4-Hydroxybenzoic acid is connected with PEG6000 through defoliant DCC at rooom temperature, then the product is refluxed with chloroacetic acid in acetone to afford PEG-bound phenyloxyacetic acid, which is reacted with thionyl chloride, ammonium thiocyanate and arylamines in turn to give PEG-bound disubstituded thioureas. After the cleavage with sodium methoxide in methanol, the eleven disubstituted thioureas are obtained.

第二章 利用PEG6000作载体,通过脱水剂DCC在室温下将对羟基苯甲酸以酯键连接在PEG6000上,再与氯乙酸在较温和的条件下生成PEG6000支载的芳氧乙酸,然后,依次与亚硫酰氯、硫氰酸铵、芳胺反应,生成PEG6000支载的硫脲,最后用甲醇钠的甲醇溶液切割PEG,得到了十一种1,3-二取代硫脲。

In addition, the Gibbs free energy and standard equilibrium constant of the reaction were calculated under the different temperature.

采用基团贡献法估算了反应体系中乙酸、乙醇和乙酸乙酯在298.15K标准状态下的生成焓和标准熵,并且估算了这3种物质的热容随温度变化的关系式,计算了不同温度条件下反应的吉布斯自由能和标准平衡常数。

Methyl α-naphthaleneacetate was synthesized by using α-naphthaleneacetic acid and methanol as raw materials and solid superacid TiO2/SO42- as a catalyst.

以固体超强酸TiO2/SO42-为催化剂,研究了α-萘乙酸与甲醇的酯化反应,探讨了催化剂种类、用量及活化温度等反应条件,发现固体超强酸TiO2/SO42-对α-萘乙酸与甲醇的酯化反应具有较高的催化活性,并使后处理简化。

All dates were analyzed by the principal component analysis through using the SIMCA-P 10.0 software. Result: The PCA demonstrated that the metabolome between treated group and control group had difference in rat urine sample after of 22 days administrated, for treated group 169 kinds of biomarkers were found including oxalacetic acid, malic acid, 2-ketoglutaric acid, NE, arachidonic acid, 5-HIAA and other compounds, the result was consistent with pharmacological effects of R.coptidis , such as antiinflammatory, inhibiting biosynthesis of CA biosynthesis, anti-central nerve and energy metabolism inhibition.

结果:给药22 d,黄连组与对照组大鼠尿样代谢组有较大差异,发现了169个生物标记物,其中可能的化合物为草酰乙酸、苹果酸、2-酮戊二酸、去甲肾上腺素、花生四烯酸、5-羟吲哚乙酸等物质,这与黄连抗炎、阻止儿茶酚胺的生物合成、抑制中枢神经、降低能量代谢的药理作用相一致。

The effect of different ratios of propionic/acetic acid on the metabolism of long-term cultivated GAO was investigated.

在3个SBR反应器(即SBR-A,SBR-C和SBR-E)中,以3种不同比例的丙酸/乙酸中长期驯化活性污泥使之富集聚糖菌,对丙酸/乙酸对聚糖菌的长期和短期代谢的影响进行了研究。

The results of studying the effects of several plant growth regulating substances on pollen germination and tube growth in pear (Pyrus serotina Rhed.) by cultivating pollens in liquid media showed that GA3,TRIA,IAA and 2,4D stimulated pollen germination and tube growth when pollen was cultivated in their lower concentration media.

采用花粉液体培养法研究了植物生长调节物质对梨花粉萌发和花粉管生长的影响,结果表明:较低浓度的赤霉素、三十烷醇、吲哚乙酸及2,4-D均能促进花粉萌发和花粉管生长,而超过一定浓度时却起抑制作用,最适宜于花粉萌发和花粉管生长的赤霉素浓度为50~300mg/L,三十烷醇为3~100mg/L,吲哚乙酸为5~25mg/L,2,4-D为5~10mg/L。

The examination made known, when consistence of acetic acid glacial at the 2%, dairy salt concentration 8%~12%, the best way was to be elected.

研究了采用冰乙酸和食盐的混合液作为汤汁的香菇酸盐渍生产工艺、产品检验等,研究表明,冰乙酸浓度2%、食盐浓度8%~12%是香菇酸盐渍的最佳生产工艺条件。

Nitric oxide produced by cardiomyocytes cultured in media and generated in heart homogenates was detected with this method, the results showed that it is an efficient method to detect low concentration nitric oxide.

利用乙酸乙酯抽提法,我们检测了心脏匀浆和培养的心肌细胞产生的一氧化氮,证明乙酸乙酯抽提法是一种检测低浓度一氧化氮的有效方法。

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