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It is found that the sample stained with silver methenamine instead of mercaptoacetic acid-osmium can prevent the false phenomena caused by the inappropriate use of mercaptoacetic acid.

摘 要：本文将六亚甲四胺银染色法作为加工毛发的电子染色剂得到较好的电子显微图像，并系统地比较了用巯基乙酸-锇法染色的羊毛样品和用六亚甲四胺银染色的人发样品的超微结构，认为对深加工过的毛发样品用六亚甲四胺银法替代巯基乙酸-锇法染角蛋白，可以防止巯基乙酸使用不当引起的假象。

To prevent epidemical disease prevalence caused by microorganisms in indoor air, a study was carried out to investigate the effect of ventilation, peracetic acid and ozonization on microorganisms reduction in the indoor air within a campus. The experimental results indicated that ventilation was an effective measure in reducing indoor air microorganisms with economy and simple operation.

为了防止室内空气微生物导致的传染病发生，对某校园室内的空气进行通风、过氧乙酸和臭氧灭菌降低微生物的实验研究结果表明，通风可以有效地降低室内微生物的浓度，是最为经济和易行的措施；过氧乙酸灭菌效果好，持续时间较长，可在不易实施通风情况下采用过氧乙酸灭菌；臭氧具有迅速杀菌的效果，使用时要与人保持一定距离，最好超出 1m。

objective to determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of edaravone, by gas chromatography.methods sample solution was injected on a gdx column (0.18 mm～0.25 mm) with nitrogen as the carrier gas.the residue was calculated by the external standard method.results the linearity was good over the range of 25 μg/ml～400 μg/ml,with the correlation coefficient of acetone being 0.996 and the average recovery 96.8%.conclusions the method was proved to be simple,rapid,practical and highly sensitive.it is an efficient method for the quality control of acetoacetic ester.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。方法：采用固定相为二乙烯苯乙基乙烯苯型高分子多孔小球（直径为0.18 mm～0.25 mm），氮气为载气，用外标法测定乙酰乙酸乙酯中残留丙酮的含量。结果：该方法在丙酮浓度范围在25 μg/ml～400 μg/ml内呈良好的线性关系，响应曲线相关系数为0.996，平均回收率为96.8%。结论：本法简便，快速、实用，灵敏度高，可有效地用于乙酰乙酸乙酯的质量控制。

The results showed that all of the four preservatives can prevent the growth of bacteroidal soft rot, and the effect of sodium diacetate was the best. After 40 or 45 days' storage, all of the untreated asparagus were rotting, but the incidence of disease of the asparagus treated with 1.5% sodium diacetate was 0 and 32% respectively. 0.5% Zhongshengjunsu, 1.5% sodium diacetate and 1% sodium chloride can delay the reduce of chlorophyll.

结果表明，4种防腐保鲜液浸蘸笋尖均可明显地抑制贮藏过程中芦笋软腐病的发生，但以双乙酸钠处理效果最好，贮藏至40d\45d，对照已全部发病，而用1.5%双乙酸钠处理的，发病率为0和32%。0.5%中生菌素、1.5%的双乙酸钠和1%氯化钠处理，均有延缓芦笋叶绿素分解的作用。

With the yield of methyl monochloroacetate as evaluating standard,the synthesized condition of methyl chloroacetate was optimized through orthogonal experiment.

以氯乙酸母液和甲醇为基本原料，固载磷钨酸为催化剂，通过连续酯化的方法制备了氯乙酸甲酯；以氯乙酸甲酯的质量收率为基准，采用三因素三水平正交实验的方法对酯合成的条件进行了优化。

The silk-protein-like polymers could be dissolved in hexafluroisopropanol and strong organic acid (e. g., formic acid, dichloroacetic acid and trifluroacetic acid), while they showed a poor solubility in common solvents.

所合成的模拟聚合物难溶于通常溶剂，但可以溶解在强酸溶剂（甲酸、二氯乙酸及三氟乙酸）和六氟异丙醇中；通过在二氯乙酸中25℃下的特性粘度测定而估算出聚合物的分子量在2～5万之间。

The synthesis of sucrose ester containing ethanoyl and oleoyl was performed by transesterification between sucrose octaacetate and ethyi oleate in organic solvents, using lipases Novo435 as the catalyst.

在有机溶剂中，以脂肪酶Novo435为催化剂，蔗糖八乙酸酯与油酸乙酯通过转酯化反应合成了同时含有油酸酰基和乙酸酰基的混合型蔗糖酯，当蔗糖八乙酸酯与油酸乙酯的物质的量之比为1：1时，油酸乙酯的转化率达95％。

Compared with other antiseptic,SDA can make food have non-harm,fresh,good taste,long stire,low price etc merits.

称双乙酸钠与其它防腐剂相比，经添加SDA的食品，具有无毒、鲜美、口味纯正、储存期长、价格地、低等优点，特别是既没有山梨酸钾的异味，又没有丙酸钙的涩味，更没有苯甲酸钠的怪味，又因为双乙酸钠为钠盐，不会影响食品的绵软。1/3-1/2量的双乙酸钠抑菌效果与丙酸钙相当，与等量的梨酸钾防腐效果相当，但价格极为低廉。

The paper involved two parts: Part 1: A two-chambered microbial fuel cell was constructed with high-concentration sodium acetate as fuel in the anode. The influence of different electron acceptors in the cathode, external resistance value, pH value and concentration of sodium acetate on electricity generation in MFC was investigated. The result showed that the maximum power density of 294.72 mW/m2 and the coulombic efficiency of 25.87% was achieved at sodium acetate concentration of 6.46 g/L, pH 7.0, external resistance 500Ωin the anode and when using potassium permanganate as electron acceptor in the cathode.

全文分为两个部分：第一部分：以乙酸钠为阳极原料构建双室微生物燃料电池，研究不同阴极受体、外接电阻、乙酸钠浓度和pH等因素对电池产电性能的影响，研究结果表明：在500mL的阴阳极反应体系中，选用乙酸钠作为阳极底物，质量浓度为6.46 g/L， pH 7.0，接入500Ω外电阻，阴极电子受体选择高锰酸钾的情况下，微生物燃料电池产电性能最好，最大电功率密度达到294.72 mW/m2，库伦效率能达到25.87%。

Glycidyl benzoate,glycidyl propionate,glycidyl acetate were obtained respectly through a phase-transfer catalytic methodology using sodium benzoate, sodium propionate, sodium acetate and epichlorohydrin as raw materials, and pure products were obtained though vaccum distillation.β-cyclodextrin and glycidyl benzoate, glycidyl propionate, glycidyl acetate, reacted in organic solvent and goal product were

先以苯甲酸钠、乙酸钠、丙酸钠和环氧氯丙烷为原料在相转移催化剂的作用下分别合成了苯甲酸缩水甘油酯、乙酸缩水甘油酯和丙酸缩水酯，经过减压蒸馏，得到相应的纯品；β-环糊精和苯甲酸缩水甘油酯、乙酸缩水甘油酯、丙酸缩水甘油酯在有机溶剂中反应，经过硅胶色谱柱分离，得到了相应的产品，产品经过TLC、IR、1H NMR、MS表征，并研究了温度、反应时间、催化剂等几个因素对反应工艺的影响，结果表明温度和催化剂对反应的快慢有较大影响。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。