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It is existed competitiveness inhibition of 6APA, non-competitiveness inhibition of PAA and substrate inhibition of Penicillin on the hydrolysis of benzylpenicillin to 6APA and PAA by an immobilized penicillin amidase. The heat conductive coefficients were determined on the vacuum elevation liquid membrane concentration. The thermodynamics and kinetics of PAA extraction were studied on the organic solvent extraction of the above solution.

研究证明固定化青霉素酰化酶裂解反应是典型的底物、产物抑制酶反应,其反应动力学数据表明,青霉素、苯乙酸以及6APA对反应分别存在底物抑制、非竞争性抑制和竞争性抑制;真空升膜浓缩适应热敏性以及粘度不大的物系,对于6APA水溶液的真空升膜浓缩过程研究得到了浓缩实验的传热系数;浓缩液萃取主要是提取出其中的苯乙酸,本文测定了不同温度以及溶剂条件下的苯乙酸溶解度,并观测了苯乙酸萃取动力学。

The process is carried out by taking organic acid and sulfoxide chloride as raw materials, acyl chloride synthesizing, reacting ethylenediamine with sodium chloroacetate to synthesize intermediate sodium EDDA, and reacting it with acyl chloride to synthesize the final product.

所述双子烷基羧酸盐表面活性剂是由以下方法制得的,以有机酸和氯化亚砜为原料首先进行酰氯的合成,再用乙二胺与氯乙酸钠反应合成中间体乙二胺二乙酸钠,将中间体乙二胺二乙酸钠与酰氯反应合成终产物。

Results: The 12 kinds of toxicants including methyl acetate, ethyl acetate, benzene, toluene, ethylbenzene, butyl acetate, p-dimethylbenzene, m-dimethylbenzene, o-dimethylbenzene, n-butanol, cinnamene and cyclohexanone were separated well. Good linear relationship sensitivity and reproducibility were obtained and detection limits (S/N=3) of them were 0.2 mg/l respectively. Conclusion: In this paper, a new method for simultaneous determination of 12 kinds of toxicants by using gas chromatography has been described.

结果:对乙酸甲酯、乙酸乙酯、苯、甲苯、乙酸丁酯、乙苯、对二甲苯、间二甲苯、邻二甲苯、正丁醇、苯乙烯、环己酮12种有毒物质的分离效果好,线性和重现性均较好,方法的检测限达到0.2 mg/L。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法,以钛酸丁酯和乙酸锌为前驱物,冰乙酸为催化剂和胶溶剂,水为溶剂,无水乙醇为钛酸丁酯的溶剂,乙醇胺为沉淀剂并提供OH -,经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂,其组分和重量百分比含量如下:钛酸丁酯占1~15%;二水乙酸锌占1~12%;无水乙醇占1%~20%;冰乙酸占5%~15%;乙醇胺占0.1%~5%;水余量,具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点,可实现对对织物的抗紫外、抗菌、抗静电功能整理。

2 It was found that there was clear inhibitory effect on hypha and sporangia during a 7-day period when doses of 200 and 400Gy were used, but little on conidia and chlamydospores.

苹果用 射线辐照后,其乙酸乙酯被分解,但对照乙酸乙酯纯品不受影响。问题:注意纯品乙酸乙酯是作对照的,说明也已被照射。而在译文中没有反映出来,显然是一个无效判断(Null judgement。

Polyester nanofiber can be prepared by electrospinning process from PET chips separately dissolving in three kinds of solvents,namely,the mixture solvent of phenol and tetrachloroethane ,trifluoroacetic acid and the mixture solvent of trifluoroace- tic acid and dichlormethane.

利用静电纺丝法制备聚酯纳米纤维,选择苯酚和四氯乙烷,三氟乙酸,三氟乙酸和二氯甲烷3种溶剂分别溶解PET切片进行静电纺丝,通过扫描电子显微镜对纤维表面形态进行观察,结果表明:三氟乙酸和二氯甲烷混合溶剂溶解PET制备的电纺纤维较好。

Preparation of trifluoroacetaldehyde and trifluoroacetic acid by trifluoroethanol catalytic oxidation;2. Polyester nanofiber can be prepared by electrospinning process from PET chips separately dissolving in three kinds of solvents,namely,the mixture solvent of phenol and tetrachloroethane, trifluoroacetic acid and the mixture solvent of trifluoroace- tic acid and dichlormethane.

利用静电纺丝法制备聚酯纳米纤维,选择苯酚和四氯乙烷,三氟乙酸,三氟乙酸和二氯甲烷3种溶剂分别溶解PET切片进行静电纺丝,通过扫描电子显微镜对纤维表面形态进行观察,结果表明:三氟乙酸和二氯甲烷混合溶剂溶解PET制备的电纺纤维较好。

Nuttallii propagules germinated normally, but the buds was significantly inhibited (p.05) in growth and the recovery in the subsequent culture was slow. Exposures to 4 mmol/L or higher caused death of E. nuttallii. In contrast, at concentration of 4 mmol/L, all P. crispus buds survived with significant growth and had a good recovery in the subsequent culture; P. crispus turions were remarkably reduced in gerimination rate, but all sprouted in the subsequent culture.

在4mmol/L的乙酸影响下,菹草幼芽仍有明显的生长;菹草繁殖体的萌发受到显著抑制(p.05),但在随后的培养中可全部萌发。4mmol/L以上的乙酸暴露3d或6d导致伊乐藻全部死亡,8mmol/L的乙酸处理6d或16mmol/L的乙酸处理3d或6d导致菹草全部死亡。

The effect factors on glycolic acid ratio were studied(reaction temperature,reaction time,and the ratio of catalyst to choloroacetic acid).

以氯乙酸和氢氧化钠为主要原料,碘化钠为催化剂碱性水解法合成羟基乙酸,并采用单因素法对影响因素进行了研究,得到最优化条件:反应温度90℃,反应时间8 h,催化剂NaI用量为氯乙酸质量的0.8%。

At first, the broth was acidified, then centrifuged to get mycelia, which was heated and powdered; finally we use acetic ether to soak the powder. After that, the phase of acetic ether was washed using the solution of ammonium sulfate and the solution of ethanedioic acid, then concentrated to gain pulps. It was crystallized at 4℃.The coarse crystals was decolorized by activated carbons, the pure needle crystal of lovastatin was obtained.

发酵液经酸化处理后,离心得到菌体,烘干后过筛得到菌粉;用乙酸乙酯浸泡,乙酸乙酯相需用(NH_4)_2SO_4溶液和草酸溶液洗涤两次;乙酸乙酯相经薄膜浓缩得到浆状物,于4℃结晶,得到粗晶体;再经粉末活性炭脱色和重结晶后得白色针状结晶,为lovastatin的纯品。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。