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On the basis of above results, the reaction rectification tower to synthesize benzyl chloride was established.

目前,国内均采用间歇釜式生产,一氯乙酸生成的同时也生成了副产物二氯乙酸,反应终点二氯乙酸浓度在12-25%。

Uranium solution is obtained electrolytically by reducing uranyl ion on mercury cathode. The effect of the addition of various aminopolycarboxylic acids (such as EDTA, DTPA, CyDTA and TTHA) and organic water-miscible solvents (such as CH3OH, C2H5OH and CH3COCH3) on the stability of ura-nium in air has been investigated. The absorption spectra of uraniumand uraniumin 1 mol/l and 9mol/l hydrochloric acid solutions are examined.

本文采用汞阴极电解还原法制备了铀溶液,研究了在盐酸介质中各种氨羧络合剂乙二胺四乙酸二钠、二乙三胺五乙酸、1,2-环已烷二胺四乙酸、三乙基四胺六乙酸和水溶性有机溶剂甲醇、乙醇和丙酮的存在对铀稳定性影响,测定了在不同盐酸浓度中铀和铀的吸收光谱。

In this method, EDTA was used as complexant which can form 1∶1 complex with Cr〓, this complex carried negative charge and can be detected directly by UV absorbance at 200nm, therefore, the CrO〓 and Cr〓 can be separated and determined in one run.

采用乙酸钠-乙二胺四乙酸钠-CTAB-乙酸缓冲液体系,加入EDTA使Cr〓与其生成的1∶1络合物,带负电荷且具有紫外吸收,在200nm处可用直接紫外法检测。

Solani. The extract was further separated into two parts and one part separated by ethyl acetate while the other was separated by petroleum ether. Based on the inhibition experiment against R. solani, ethly acetate extract has a rather strong effect on R. solani with 89.70% inhibition rate and 15.52 mgmL^(-1) EC 50.The effect of petroleum ether extract on R. solani is relatively weak. The former was again divided into five parts in silica gel column, of which the second part significantly inhibits R. solani. During the periods of 24 and 48 hrs, the inhibition rate of the second part on R. solan is respectively 89.58% and 80.36%.

结果表明:鸭粪乙醇提取物对水稻纹枯病菌有抑制作用,24h内最高菌丝生长抑制率和EC50分别为88.64%、26.11mgmL^(-1);鸭粪乙醇提取物经萃取分离得到石油醚和乙酸乙酯两种组分,其中石油醚组分抑菌效果较弱,乙酸乙酯组分抑菌能力较强,其对水稻纹枯病菌抑制率为89.70%,EC50为15.52mgmL^(-1);对乙酸乙酯组分进行硅胶柱层析分离得到5种流份,其中第2流份有显著抑菌活性,在24h和48h内对水稻纹枯病菌的抑制率分别为89.58%和80.36%。

Zinc acetate, cobaltous Acetate, zirconium oxychloride and manganese acetate are used as typical experimental materials.

实验以乙酸锌、乙酸钴、氧氯化锆和乙酸锰为典型材料,进行了超临界水热合成制备金属氧化物微粒的研究。

The result of study on the apparent kinetics of photochlorination of acetic acid showed that the reaction rate is comparatively slow and the byproduct of dichloroacetic acid is created during the reaction. In order to put the technology of photochlorination of acetic acid into industrialization, the new technology about distillation column with a single reactor having a large reactive potency must be adapted.

由乙酸光氯化反应宏观动力学研究结果可见,反应速度相对较慢,且生成二氯乙酸副产品,为了乙酸光氯化工艺实现工业化,必须采用具有较大反应能力的反应与精馏耦合工艺。

The advantages of α-hydroxyacetic acid biosynthesis over traditional chemical conversion are wide range of reaction condition,high conversion ratio and green process.

化学法生产羟基乙酸存在原料消耗大、产品收率低、环境污染严重等缺点;生物法合成羟基乙酸条件温和、底物转化率高,为绿色合成羟基乙酸提供强有力的技术支持。

The ionization enthalpies of acetic acid, chloro-, bromo- and iodo- acetic acids were measured at 5℃ intervals between 20℃ and 45℃ in aqueous solution by LKB-2277 Bioactivity Monitor.

本文用LKB-2277BioActivityMonitor以5℃的间隔测量了20-45℃温度区间乙酸、氯乙酸、溴乙酸和碘乙酸在水溶液中的电离焓。

Monochloroacetic acid is a rather important chemical raw material and organic intermediate product, which is mainly manufactured by chloride of acetic acid using sulfur and anhydride acetic acid as catalyst.

氯乙酸是一种及其重要的化工原料和有机中间体,目前氯乙酸主要以硫磺或醋酐为催化剂进行乙酸氯化生产而得。

All animals were individually fed with a constant concentration and hay for 8 weeks. Results showed that VB12 production from cobalt in lambs was similar when using cobalt sulphate and cobalt chloride, and was significantly higher (P.05) in cobalt sulphate than in cobalt acetate. However, VB12 production significantly decreased in cobalt oxide treatment compared with other forms of cobalt sources. The relative bioavailability of cobalt sulphate, cobalt chloride, cobalt acetate and cobalt oxide was 100%, 95.66%, 89.50% and 22.56% respectively.

结果表明:1硫酸钴、氯化钴、乙酸钴、氧化钴的相对生物学有效率分别为100%、95.66%、89.50%和22.56%(P.01);2硫酸钴、氯化钴、乙酸钴和氧化钴组血浆VB12的含量分别为1666.9、1594.5、1493.3和376.1pmol/L,硫酸钴、氯化钴组相近,乙酸钴组稍低,而氧化钴组明显下降,血浆甲基丙二酸含量为2.94、3.01、3.49和3.99μmol/L;同型半胱胺含量为8.91、9.23、9.97和10.78μmol/L,硫酸钴与氯化钴组相近,乙酸钴组稍有增加,而氧化钴组明显升高,3个指标反映了一致的钴营养状况。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。