乙酸甲酯

Ee were achieved in the Pd (0)-catalyzed asymmetric reaction of racemic 1, 3-dipheylprop-2-en-1-yl acetate with dimethyl malonate under the optimized reaction conditions.

在钯催化的乙酸1，3-二苯基烯丙基酯与丙二酸二甲酯的不对称反应中，取得了接近定量的收率和较好的对映选择性（71.2％ee）。

The process was methanolysis ed alkyl inino-acetic acid ester hydrogen chloride salt from methyl-cyanide.

研究了由乙腈为原料经烷基亚氨基醋酸酯盐酸盐醇解制备原乙酸三甲酯的工艺方法，对投料比、反应温度、反应时间及中和指示剂等工艺条件进行了研究，得出较优惠的工艺条件。

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

At the initial isolation to the extract from ethyl acetate, tow kinds of crystal a and b with higher purity were found, and the primary components were 98.45%. Quinic acid and 69.34% L-Proline, 5-oxo-, methyl ester.

在乙酸乙酯部分进行初次分离时，还得到了两种纯度较高的晶体a和b，经GC-MS分析可知其主要成份分别为98.45%奎宁酸和69.34%的5-脯氨酸甲酯。

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果：从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物，分别为绿原酸甲酯，5-O-咖啡酰基－奎宁酸丁酯，奎宁酸丁酯，5-羟甲基－2-糠醛，三十烷酸，-表儿茶素，7，8-二羟基香豆素，3，4-二羟基苯甲酸乙酯，原儿茶酸。

For further understanding the effect of the strain on K-bearing silicate mineral, an experiment with KO2 strain cultured in nitrogen-containing and nitrogen-free medium was conducted. By putting mineral powders into the medium and measuring the concentration of capsular polysaccharides, we concluded that the strain can accelerate the weathering rate of silicate minerals. The results showed that the polysaccharides secreted by the strain in the growth process could help the bacterial to adhere to the mineral surface effectively, and created the bacterium-mineral complex, which formed a mircro-enviorment avail the release of potassium. Another result was that there was higher level of Carbonic Anhydrase activity, which revealed that some exo-protein or enzyme produced by the bacterial had postive impact on the process of releasing potassium ion. We carried out the bacterial fermentation for larger scale production of the bacterial secretion, which was used to sperate, and identify the small molecules related to the mineral-bacterial interaction. After the analysis, it was found that the strain can produce many kinds of small molecules, such as 2-Hydroxybenzoic acid, 4-Hydroxyphenylacetic acid, methyl-4-hydroxybenzoate, etc.

分别将菌株接入含有不同矿粉的培养基中培养，检测其在有氮、无氮培养基中荚膜多糖含量的变化，并在以钾长石和黑云母为矿源的情况下，比较研究了菌株在有氮、无氮培养基中对矿物的风化能力，通过一系列的实验，证实胶质芽孢杆菌在生长过程中所分泌的粘稠胞外聚糖可帮助细菌有效黏附在矿物表面，形成细菌-矿物复合体，并改变及维持该复合体内部的微环境，有助于该菌的解钾作用，而且细菌分泌的胞外蛋白质在该菌对含钾硅酸盐矿物的解钾作用过程中发挥重要作用；将胶质芽孢杆菌接入以钾长石和黑云母为矿源的有氮、无氮培养基中培养，检测到该菌碳酸酐酶活性的变化，并进行批量发酵后小分子酸性分泌产物的提取、分离、纯化与鉴定等方面的研究，结果表明，该菌可产生2-羟基苯甲酸，4-羟基苯乙酸，4-羟基苯甲酸甲酯等小分子物质。

This article uses the tetramethyl ammonium hydroxide∕methyl iodide for methyl esterification and the method of temperature program ,determine the content of lactic acid, ethanoic acid, propionic acid, butyric acid.

使用四甲基氢氧化铵/碘甲烷对青贮料浸出液进行甲酯化反应，采用程序升温的方法，同时测定青贮料中乳酸、乙酸、丙酸、丁酸的含量。

Typically,0.2 mmol of cd solution, and 0.4 mmol of mpa solution were mixed in a 40 ml solution and the ph of the solution was 二氰基丙酸乙酯 to 10.0 by solution was palced in a three-necked flask and was deaerated.

通常情况下， 0.2浓度的镉环硫乙烷，和0.4浓度的mpa的混合溶液中40巯基丙酸甲酯溶液和ph值的溶液是调整，以10.0的溶液放置在是在三制作乙酸钙中，并除去溶液中的气体。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。