乙酸定量

Ee were achieved in the Pd (0)-catalyzed asymmetric reaction of racemic 1, 3-dipheylprop-2-en-1-yl acetate with dimethyl malonate under the optimized reaction conditions.

在钯催化的乙酸1，3-二苯基烯丙基酯与丙二酸二甲酯的不对称反应中，取得了接近定量的收率和较好的对映选择性（71.2％ee）。

He chromatographic conditions for separation and detection of organic acids and inorganic weak acids with ion exclusion chromatography and nonsuppressed conductivity detection are described in this paper.

用非抑制型电导检测的离子排斥色谱法，以对甲苯磺酸为淋洗液，研究了柠檬酸、苹果酸、抗坏血酸、乙醇酸、甲酸、乙酸、丙酸及氢氟酸和碳酸的色谱分离及定量检测条件。

On the condition of the existence of the buffer solution of ammonium acetate (PH5-6) and ammonium thiocyanate, quantitatively reduce Cu2+ into Cu+ by using sodium thiosulphate .

本文在PH5-6的乙酸铵缓冲溶液及硫氰酸铵存在下，用硫代硫酸钠定量还原Cu~(2+)为Cu~+，Cu~+与SCN~-结合，形成稳定的硫氰酸亚铜白色沉淀，反应终点可由全自动电位滴定仪确定。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后，用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质，过滤，用次氯酸钠将样品溶液中的甜蜜素转化为N，N-二氯环己胺经正己烷萃取后，在phenomenex Gemini-C18柱上，以乙腈－水(7+3)或甲醇－水(8+2)为流动相进行分离，HPLC-UV检测器在314 nm测定，外标法定量。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。