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The beheviour of four low-molecule weight organic acid lactic acid,hydroxy-acetic acid,mercapto-acetic acid,glyconic acid as iron-containing silicate-aegirines depressants on the hematite direct flotation is investigated in this paper.The results of flota

本文研究了四种小分子有机酸抑制剂乳酸、羟基乙酸、巯基乙酸、葡糖酸在赤铁矿正浮选中对含铁硅酸盐脉石霓石的抑制行为,纯矿物、人工混合矿与实际矿石浮选实验均证明了它们具有良好的选择性抑制作用,可以成功地实现赤铁矿与霓石的浮选分离。

Six derivatives of 4-phenyl-3-phenoloxymethyl-5-mercapto-1,2,4-triazlyole were synthesized from phenoloxyacetyl hydrazide by two-steps reaction under microwave irradiation, then reacted with 2-chloroacetic acid to give six novel derivatives of 2-(3-phenoxymethyl-4-phenyl-[1,2,4]triazole-5-thio)-acetic acid.

在微波辐射条件下,芳氧乙酰肼经两步反应制得4-苯基-3-芳氧甲基-1,2,4-三唑-5-硫酮衍生物,再与氯乙酸反应得到6种尚未见文献报道的2-(3-芳氧甲基-4-苯基-1,2,4-三唑-5-硫基)乙酸衍生物。

The dimer and isomer of NAA has been found as the main products arised from these radical groups.

这些自由基又进一步反应形成了主要的产物,包括萘乙酸二聚体和萘乙酸的异构体。

The variance of ABA of grape during storage were discussed in this paper.The following results are been drawn:the change of the content of ABA of grapes during storage characterizes by a parabolic shaped curve with obvious peak.Low temperature (0±0.5℃) is conducive to delaying the appearance of the peak of ABA and reduces the peak value.Nine kinds of plant growth regulators and two kinds of chemicals were chosen to treat grape bunches so as to study their mechanisms on ABA of grapes,2,3,5 triiodobenzoic a...

试验研究了葡萄贮期脱落酸的变化,结果表明:葡萄贮期 ABA含量呈抛物线形变化,有明显的高峰出现,低温( 0± 0 。5℃)贮藏具有推迟 ABA峰期和降低峰值的作用,经用 9种植物生长调节剂和 2种化学药品对葡萄果穗处理试验,三碘苯甲酸对 ABA的形成有极强的抑制作用,吲哚- 3-乙酸、赤霉素( GA3)、萘乙酸和 6-苄基氨基嘌呤( 6- BA)对 ABA的形成也具有拮抗作用,矮壮素、比久( B9)、乙烯利和外源脱落酸对 ABA的形成有促进作用。

A novel solvothermal synthesis method for direct preparing of crystals of copper phthalocyanine is presented in this article.

我们使用三种原料合成酞菁铜晶体:一是邻苯二腈、钼酸铵和二水乙酸合铜为起始原料;二是1,3-二亚胺基异吲哚啉和二水乙酸合铜为起始原料;三是邻苯二腈、氧化铜和钼酸铵为起始原料。

Cellulose diacetate and cellulose triacetate, for example, are not attacked by microorganisms because most of the hydroxyl groups have been converted to acetate groups.

比方说由于大部分的羟基已经被转化成了醋酸基,双乙酸纤维素和三乙酸纤维素就不再受微生物的侵蚀。

A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.

魏太保 ;冷艳丽;王永成;张建辉;张有明*摘要:以对甲苯磺酰氯为原料,通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸,再经酯化、肼解得到对甲苯磺酰氨基乙酰肼,然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析, IR, 1H NMR和13C NMR确证。

The results also indicated a low production of acetic acid, acetoin and ethyl acetate, and high amounts of amyl alcohols in all of the ciders.

结果在全部萍果汁也表明了乙酸、乙醛和乙酸乙酯旳低产量和大量产生旳戊基乙醇。

Reaction (1) was examined with different kinds of acetal substrate(1) and vinyl ethyl ether, and the results indicated that the 1, 1,3-triethoxy compounds could be obtained in high yields of 88 and 97% respectively when the R groups of the acetal are phenyl and anisyl, while the yields amounted only to 55-75 % for R=a...

有证据表明这种催化反应也可能是通过正碳离子中间体进行的。本反应的产物1,1,3-三乙氧基化合物经乙酸/乙酸钠溶液水解可得反式α,β-不饱和醛。水解产率:芳香族产物大于90%,脂肪族产物大于75%。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3,3-二甲基-4-戊烯酸-3'-甲基-2'-丁烯酯工艺复杂、异戊烯大量分解问题,研究了MBDP直接返回循环使用工艺,MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺,比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果,筛选出回收MBDP&一锅煮&最佳工艺:按照n:n:n:n=1.0:9.8:9.2:0.05物质的量比投料,74℃~78℃反应21h,MBDP转化为贲亭酸甲酯和异戊烯醇,单程转化率87.7%,用85%的磷酸中和甲醇钠,蒸出甲醇,直接用于合成贲亭酸甲酯。

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