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A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ,N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

An ester or a salt of perchloric acid .Indocin is the trade name of this nonsteroidal anti-inflammatory drug.

氯苯基甲氧基甲基吲哚乙酸是一种非固醇抗炎药物的商标名称。

Deoxybenzoin(3) was prepareded by using the resorcinol and substituted phenylacetic as starting meterials in microwave-mediated.Then the compound(3) was reacted with acetic anhydride to produce(4).The compound(4) was hydrolyzed to convert compound(5) in the acid-mediated. The compound(5) was reacted with the 1,2-dibromo-ethane and 1,3-dibromo-propane in refluxed condition with acetone as solvent to give(6) or(7),respectively.Lastly,the title compounds were synthesized by refluxing(6) or(7) with 2-methyl-benzimidazole and potassium carbonate in acetone solution.

以取代苯乙酸和间苯二酚为起始原料,用微波辐射法合成脱氧安息香(3),(3)与乙酸酐缩合生成2-甲基-7-乙酰氧基异黄酮(4),(4)在酸性条件下水解生成相应的异黄酮(5),化合物(5)分别与1,2-二溴乙烷和1,3-二溴丙烷反应生成(6)和(7),化合物(6)和(7)再分别与2-甲基苯并咪唑偶合生成目标化合物。

4Production of chemical products from which narcotics are easily made ephedrine, 3, 4-idene dihydro phenyl-2-acctonc, phenylacetic acid, 1-phenyl-2-acetone, heliotropin, safrole, isosafrole, acetic oxide

易制毒化学品生产(麻黄素、3,4-亚基二氧苯基-2-丙酮、苯乙酸、1-苯基-2-丙酮、胡椒醛、黄樟脑、异黄樟脑、醋酸酐

The extraction of Pr3+was studied by using heptane containing bis(2-ethylhexyl)phosphinic acid in sodium perchlorate,chloroacetic acid and citric acid medium ,respectively.

研究了二(2-乙基己基)膦酸(PIA-8)的庚烷溶液分别在高氯酸钠、氯乙酸、柠檬酸介质中对Pr3+的萃取。

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为:以青霉素G钾盐为原料,选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂,氧化得青霉素亚砜;采用对硝基溴苄为酯化试剂,制备青霉素亚砜酯;以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂,酞酰亚胺钾和4A型分子筛为酸清除剂,顺利开环;再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯,最终产率在60%以上。

The high sulfur coal from Jiexiu in Shanxi is used in this experiment and the influence of removing pyritic sulfur by adding different pyrites depressors on the process of agglomeration was explored in this study,The experiment result shows that adding pyrites depressors on the process of oil agglomeration can improve the sulfur-removing rate.

油团聚是以脱除煤中灰分为主的团聚技术,脱硫的效率很低,采用山西介休的高硫煤,探索在油团聚过程中加入不同的黄铁矿抑制剂(巯基乙酸、重铬酸钾、高锰酸钾)对脱除煤中黄铁矿硫的影响。结果表明加入黄铁矿抑制剂对脱硫效率有一定程度的影响

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果:从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物,分别为绿原酸甲酯,5-O-咖啡酰基-奎宁酸丁酯,奎宁酸丁酯,5-羟甲基-2-糠醛,三十烷酸,-表儿茶素,7,8-二羟基香豆素,3,4-二羟基苯甲酸乙酯,原儿茶酸。

Continuous flow experiment was carried out using acidogenic-desulfate bioreactor and it is suggested that on quality,SRBis the hydrogen consumer and the remaker of the end products of AB;and maintains the typical characteristic of"acetate-type" metabolism of its population. On quantity, SRB maintains dynamic balance between"substrate chain"and"bio-chain",describing the dynamic of its population.

采用产酸脱硫反应器进行连续流试验,提出在&质&的方面,SRB是产酸脱硫生态系统中氢的&消费者&和产酸菌酸性末端产物的&改造者&,并维持着群落&乙酸型代谢&的典型特征;在&量&的方面,SRB种群通过数量波动维持着&基质链&与&生物链&的动态平衡,并以种群动态为表征。

Continuous flow experiment was carried out using acidogenic-desulfate bioreactor and it is suggested that on quality,SRBis the hydrogen consumer and the remaker of the end products of AB;and maintains the typical characteristic of"acetate-type" metabolism of its population. On quantity, SRB maintains dynamic balance between"substrate chain"and"bio-chain",describing the dynamic of its population.

摘 要:采用产酸脱硫反应器进行连续流试验,提出在&质&的方面,SRB是产酸脱硫生态系统中氢的&消费者&和产酸菌酸性末端产物的&改造者&,并维持着群落&乙酸型代谢&的典型特征;在&量&的方面,SRB种群通过数量波动维持着&基质链&与&生物链&的动态平衡,并以种群动态为表征。

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