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In this dissertation, two derivatives of aniline containing polyoxyethylene substituent m-phenylene diamino formyl alkylenediamine poly acetate and poly-3-aminobenzoate were designed and synthesized. And then, comb-shaped polyaniline grafted by PEO were prepared by chemical oxidation copolymerization. The structure of copolymers were characterized by FTIR, ultraviolet-visible spectrum, elemental analysis and TEM etc..

本文在设计并合成两种含聚氧乙烯取代基的苯胺衍生物——间苯二氨基甲酰己二氨基甲酸聚氧乙烯乙酸酯和3-聚氧化乙烯单甲醚基苯胺的基础上,采用化学氧化法将它们与苯胺进行共聚,制备出了聚氧乙烯接枝聚苯胺的梳型共聚物。

The methanogenic bacteria strains with different growth substance were easily isolated on the media with different chemical composition.

在培养墓中同时加入营养基质甲酸钠、乙酸钠、甲醇以及注入氢和二氧化碳的混合物,使以各种生长基质为底物的产甲烷细菌在一种培养基比较容易被分离出来。

The results showed that molecular weight of malate dehydrogenase was 69 kDa which included two subunits with the molecular weight was about 34 kDa. The optimal pH, temperature and Km were 8.0, 50℃ and 84. 6μmol/L (oxaloacetic acid, pH 8.3), respectively.

结果表明:苹果酸脱氮酶的相对分子质量约为69000,含有2个亚基,每个亚基的相对分子质量约为34000;该酶的最适作用pH为8.0,最适作用温度为50℃;K值为84.6μmol/L(草酰乙酸,pH8.3)。

A series of 3-naphthyl-2--1,3-thiazolidin-4-ones were synthesized by the three-component one-pot cyclocondensation of naphthylamine, aromatic aldehyde and 2-mercaptoacetic acid using a microwave-assisted method in the presence of DMAP/DCC.

利用微波促进的多组分一锅法,在封管条件下,以萘胺、芳醛和巯基乙酸为原料,4-二甲氨基吡啶/N,N'-二环已基碳二亚胺为催化剂,合成了系列新的噻唑烷酮衍生物,该反应具有时间短、操作简便等优点。

The bio-degradation pathways of NP would be that the long branches in nonyl of NP are firstly degraded into short methyl branches, which come into being a series of short chain alkyl phenols with different branch structures. The middle products should be further metabolized into simpler compounds, such as benzene acetic.

污水生物处理过程中壬基酚可能的初级生物代谢途径是壬基上的长支链断裂为短的甲基链,生成一系列带有不同分支结构的短链烷基酚类代谢产物,进一步的代谢产物有苯乙酸。

Some new α,β-unsaturated sulfones were prepared by condensation of 4-nitrophenylsulfonylacetates with aromatic aldehydes in cyclohexane/CH_3CH_2OH in the presence of catalytic amounts of piperidine.

不饱和砜是以对硝基苯磺酰基乙酸酯为原料与芳香醛在六氢吡啶醋酸盐催化下发生缩合反应制得的。

Based on the tissue culture, the effect of N-phenyl-N'-1,2,3-thiadiazol-5-ylurea, 6- benzyla minoprine(6-BA) and 1-Naphthylacetic acid on spore germination, protonema develop- ment and bud differentiation in Entodon challenged was investigated in this paper. The whole process was observed and taken pictures. The results show that TDZ, 6-BA and NAA have no significant effect on the spore germination. During the process of protonema development, 1.0 mg/L NAA can promote the primary development of protonema significantly, and 0.4 mg/L TDZ promotes branches formation in inter- mediate stage of the protonema development.

:研究了3种植物生长调节剂苯基噻二唑基脲、6-苄基腺嘌呤(6-BA)、萘乙酸对密叶绢藓孢子萌发、原丝体发育及芽体发生的影响,并对整个发育过程进行了显微观察和照相,结果表明:(1)3种植物生长调节剂对密叶绢藓孢子萌发影响不显著;(2)在原丝体发育阶段,1.0mg/LNAA对原丝体初期的发育促进效果显著,0.4mg/LTDZ对原丝体发育中期分枝的形成促进效果显著,6。

The mortality of mice from tartar emetic was observed after concomitant injections of 5 testing drugs (procaine-HCl, sodium phenyl acetate, sodium αα'-dimercaptoadipate, sodium mercaptosuccinate and sodium thiosulfate).

二普鲁卡因、苯乙酸钠、aa′-二巯基己二酸钠及巯基丁二酸钠能使小鼠腹腔注射吐酒石急性及亚急性中毒死亡率明显地减低,而硫代硫酸钠则无效。

A novel compound——N-naphthalene acylN′-substituted p-chlorobenzamido thiocarbamide was synthesized by reaction of p-chlorobenzamido hydrazine and α-naphthalene acyl mustard oil,which was obtained by potassium thiocyanate combined with α-naphthalene acyl chloride formed from α-naphthylacetic acid and SOCl2 in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,合成了新型化合物N-萘乙酰基-N′-对氯苯甲酰氨基硫脲,用薄层色谱法跟踪最后一步反应,确定了反应时间。

Naphthalene acetyl chloride was prepared firstly by the reaction between α-naphthylacetic acid and SOCl2 in anhydrous benzene,then reacted with potassium thiocyanate to obtain α-naphthalene acetyl isosulfocyanate,as taking an addition reaction with p-chloro benzoyl hydrazine the novel compound N-naphthalene acetyl-N'-p-chloro benzoylamino thiocarbamide was finally synthesized.

通过α-萘乙酸和SOC l2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,生成新型化合物N-萘乙酰基-N'-对氯苯甲酰氨基硫脲。

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