乙酸乙酯

Their specific surface area and acid strength were measured, and their catalyt and SBA-15 were ic performance was evaluated in the synthesis of fructone by acetalization of ethyl acetoacetate with ethylene glycol.

用浸渍法制备了一系列负载型磷钨酸及其铯盐催化剂，载体包括超稳Y沸石、脱铝超稳Y沸石、SiO2和SBA-15，测定了催化剂的比表面积和酸强度，并在乙酰乙酸乙酯与乙二醇液相缩合制取苹果酯反应中考察了催化剂的性能。

The synthesis of fructone from ethyl acetoacetate and ethylene glycol using sulfonated activated carbon as solid acid catalyst was investigated.

以活性炭磺化制得新型固体磺酸磺化炭为催化剂，对乙酰乙酸乙酯和乙二醇合成苹果酯的催化工艺进行了系统研究。

Various reaction parameters such as ratio of ethyl acetoacetate to ethylene glycol,catalyst amount,reaction time and water-carrying reagent amount were studied.

讨论了酯醇比、催化剂用量、反应时间、带水剂用量对酯化率的影响。最佳反应条件为：n：n=1：1.8，催化剂用量为乙酰乙酸乙酯质量的2%，带水剂用量为20mL，反应时间3h。

Sodium diethyl oxalacetate ; \ Claisen condensation ; \ 1 phenyl 3 carbethoxy 5 pyrazolone

钠代草酰乙酸乙酯； Claisen酯缩合； 1苯基3羧酸乙酯5吡唑啉酮

Analyse and compare what adopt a variety of pair of methods, the Michael addition reaction of ester of acerbity second of second of hydroxyl of protection of benzyl of the response of close nucleus addition that uses second nitrile and ester of formic acid second certainly, chloridize, cyanogen, reaction that take off carboxyl generates 3- benzyl oxygen radical the fifth of the ten Heavenly Stem the method of 2 nitrile, detailed discussion the action that wait and the by-product that arise possibly reach the reactant in each pace reaction, activator, dissolvent avoid a method.

通过对多种方法的分析和比较，确定采用乙腈和甲酸乙酯的亲核加成反应、氯化苄保护羟基、氰乙酸乙酯的Michael加成反应、脱羧反应生成3-苄氧基戊二腈的方法，并具体的讨论了每一步反应中反应物、催化剂、溶剂等的功能和可能产生的副产物及避免方法。

In this paper, the applications of the environmental friendly solid acid catalysts for esterification were studied and the activities of these catalysts were discussed, by which the solid acid ferric sulfate x-hydrate was used first as catalyst in the synthesis of dimethyl fumarate and ethyl chloroacetate and solid super acid SO42-/Fe2O3 was used first as catalyst in the synthesis of ethyl p-nitrobenzoate.

本文研究了对环境友好的固体酸催化剂在酯化反应中的应用，首次以固体酸Fe_2(SO_4)_3·xH_2O为催化剂合成了新型防霉剂富马酸二甲酯和化工原料氯乙酸乙酯，以固体超强酸5O_4~(2-)／Fe_2O_3为催化剂合成了医药中间体对硝基苯甲酸乙酯，并探讨了这些催化剂的催化活性。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂，用粉末K2CO3代替常规使用的乙醇钠，在季铵盐和聚乙二醇混合相转移催化剂的存在下，含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应，得到相应的环化物。

By using gas chromatography technique nine kinds of fragrance components(acetic aldehyde,ethyl acetate,ethanol,propyl acetate,3-hydroxy-2-butanone,acetic acid,furfural,metacetonic acid,2,3-butylene glycol)were measured quantitatively in different kinds of Shanxi overmature vinegar and the other kinds of vinegar.

应用气相色谱方法对山西老陈醋和其他种类醋的9种香气成分(乙醛、乙酸乙酯、乙醇、乙酸丙酯、3-羟基-2-丁酮、乙酸、糖醛、丙酸、2，3-丁二醇)进行了定性、定量测定，并用聚类分析、模糊综合评判、方差分析、回归分析的方法对实验结果进行了数理分析。

RESULTS: 12 compounds were isolated and identified as aurantiamide acetate (1), aurantiamide benzoate (2), physcion (3), scopoletin (4), vanillin (5), coniferyl aldehyde (6), syringaldehyde (7), syringic acid (8), luteolin (9), apigenin (10), azelaic acid (11), dotriacontanic acid (12), respectively.

结果：从羊耳菊全草的氯仿和乙酸乙酯部分共分离得到12个化合物，分别鉴定为橙黄胡椒酰胺乙酸酯(1)，橙黄胡椒酰胺苯甲酸酯(2)，大黄素甲醚(3)，东莨菪亭(4)，香草醛(5)，松柏醛(6)，丁香醛(7)，丁香酸(8)，木犀草素(9)，芹菜素(10)，壬二酸(11)，三十二烷酸(12)。

According to the results of the former study in our laboratory, trans-1, 2-cyclohexanediol is produced with a lot of acids and water, for extraction of trans-1, 2-cyclohexanediol from the solution, ethyl acetate and butyl acetate were used as extraction reagents, the solubility data of the trans-1, 2-cyclohexanediol in corresponding mixed solvents of some sorts of acetates and water are needed.

根据本实验室前期研究结果可知，反式-1，2-环己二醇是在酸性和大量水存在的条件下得到的，为了把反式-1，2-环己二醇从反应液中萃取出来，本工艺所采用的萃取剂是乙酸乙酯和乙酸丁酯，需要获得反式-1，2-环己二醇在这些酯类与水混合溶剂中的溶解度数据，因而对反式-1，2-环己二醇进行相关固液相平衡的研究是非常迫切和必要的。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。