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乙酸乙酯

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Phenetole ;α-oxo-p-ethoxyphenylacetic acid ethyl ester ; ethyl-2-(p-ethoxyphenyl) propenoate ; synthesis

苯乙醚;α-羰基-对乙氧基-苯乙酸乙酯; 2-对乙氧基苯基丙烯酸乙酯;合成

The strongly acidic cation exchange resin catalyzed synthesis of fructone-B by the reaction of ethyl acetoacetate and 1,2-propanediol was studied.

以硫酸高铈铵为催化剂,通过乙酰乙酸乙酯分别与乙二醇和1,2-丙二醇反应合成了苹果酯-A和苹果酯-B,研究了催化剂等有关因素对产品收率的影响。

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果:从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物,分别为绿原酸甲酯,5-O-咖啡酰基-奎宁酸丁酯,奎宁酸丁酯,5-羟甲基-2-糠醛,三十烷酸,-表儿茶素,7,8-二羟基香豆素,3,4-二羟基苯甲酸乙酯,原儿茶酸。

Water samples were extracted and purified and collected by solid-phase extraction LC-18 column. Soil samples were extracted by ethyl acetate/petroleum ether (2:1, by vol) and purified by sulphonation. Wheat sample was extracted by acetonitrile/water (4:1, by vol) and purified and collected by SPE- Florisil column.

水样直接用LC-18固相萃取小柱分离、净化和富集;采用乙酸乙酯/石油醚(体积比2:1)振荡提取,磺化法净化,测定土壤中氯氟吡氧乙酸残留量;以乙腈/水(体积比4:1)为提取剂,氟罗里硅土固相萃取小柱分离、净化,测定小麦样品中氯氟吡氧乙酸的残留量。

Result: The anticancer active component includes: taxol 9.45%、cephalomanine: 9.63%、10- deacetylbaccatinⅢ: 22.64%、total flavonoids: 19.15%. 3. The preparation of Seiadopitysin control Methods: Take dry Ginkgo leaves and extracted three times by sonication with 95% EtOH, solutions were concentrated under vacuum, after defatting by petroleum benzin, the sample was extracted with EtOAc and the solutions were concentrated under vacuum.

金松双黄酮对照品的制备方法:取干燥银杏叶以95%乙醇超声提取3次,提取液合并,减压浓缩,石油醚脱脂后,用乙酸乙酯萃取,萃取液减压浓缩,经硅胶柱(6cm×80cm)层析,石油醚-乙酸乙酯(9∶1~5∶5)梯度洗脱,产物用甲醇多次冲淋,再以二甲基甲酰氨溶解,反复重结晶,得黄色粉末结晶。

The extracts from evening primrose flower could significantly enhance the cellular immune function in immunosuppressed mice. Effects of ethylacetate extract was better than those of water extract.

月见草花乙酸乙酯提取物和水提取物均可明显增强环磷酰胺免疫抑制小鼠的细胞免疫功能,其中乙酸乙酯提取物的作用优于水提取物。

In order to improve the thermal stability of yellow iron oxide pigments, a new balance precipitant coating silicon method with ethyl acetate as potential acid by controlling the dehydrolysis velocity of ethyl acetate was used.

为了改善铁黄颜料的耐热性,运用乙酸乙酯作为潜伏性酸试剂,研究了一种新的铁黄表面均匀包覆二氧化硅的方法,即通过控制乙酸乙酯的水解速率来实现在铁黄表面均匀包覆二氧化硅。

The major occupational hazards factors in printing ink were benzene, toluene, xylene, ethylbenzene, solvent gasoline, methanol, alcohol, isopropyl alcohol, ethyl acetate, butyl acetate, butyl acetate, dichloromethane, etc. 10 of 1224 samples (0.82%) exceeded the national occupational health standards.

印刷油墨中存在的职业病危害因素种类主要有苯、甲苯、二甲苯、乙苯、溶剂汽油、甲醇、乙醇、异丙醇、乙酸乙酯、乙酸丁酯、二氯甲烷等,检测样品总数1224件,超标样品数10件,超标率为0.82%。

In these components, 2-methyl-1-propanol, ethyl acetate, 3-methyl-1- propanol, 2,3-butanediol, phenylethyl alcohol, butanedioic acid diethyl ester, ethyl hydrogen succinate, 2-hydroxy-ethyl propanoic acid and 4-hydroxy-benzeneethanol were main aroma components, these volatile componds provided the typical sensory style of wine.

其中,2-甲基-1-丙醇、乙酸乙酯、3-甲基-1-丙醇、2,3-丁二醇、2-羟基丙酸乙酯、苯乙醇、丁二酸二乙酯、乙基-氢化琥珀酸和4-羟基苯甲醇等成分构成了葡萄酒的主体香气,这些主体香气与其他风味成分一起构成葡萄酒的典型风味特征。

Nitric oxide produced by cardiomyocytes cultured in media and generated in heart homogenates was detected with this method, the results showed that it is an efficient method to detect low concentration nitric oxide.

利用乙酸乙酯抽提法,我们检测了心脏匀浆和培养的心肌细胞产生的一氧化氮,证明乙酸乙酯抽提法是一种检测低浓度一氧化氮的有效方法。

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