乙酸乙酯

The experimental result showed that three byproducts was formed and the optimal condition was as follows: the molar ratio of ethylene glycol, hydrogen bromide, and acetic acid was 1:1:1.3, when ethylene glycol was 1 mol, refluxed 5 h under the action of 100 mL toluene.

结果表明：较适宜的合成条件为乙二醇1 mol， n：n：n=1：1：1.3，在带水剂甲苯(100 mL)的作用下，回流反应5 h，约4 h后分两次追加0.12×2 mol醋酸酐，合成效果最好，产率可达到95%，反应副产2-溴乙醇及少量的1， 2-二溴乙烷、乙二醇二乙酸酯和二乙二醇二乙酸酯。

The surface hydroxyl group onto magnetic polyvinyl acetate nanoparticles can be obtained by saponification reaction on their surface.

结果表明，磁性聚苯乙烯颗粒与丁二酸酐发生Freidel-Crafts酰基化反应，可以在颗粒表面引入少量羧基；磁性聚甲基丙烯酸甲酯颗粒分别与乙二醇、二缩三乙二醇、聚乙二醇等发生醇-酯交换反应，可以在颗粒表面接枝不同分子链长度的末端羟基；磁性聚醋酸乙烯酯颗粒经过醇解或皂化反应可以获得表面羟基；磁性聚丙烯酸甲酯颗粒通过乙二胺或1，6己二胺的胺解反应可以得到表面氨基，继而与一氯乙酸反应可以引入亚胺二乙酸基团。

Ingredients: water,glycerin,caprylic/capric triglyceride,cetyl alcohol,squalane,glyceryl stearate,panthenol,betaine,dimethicone,lavandula angustifoliaoil,allantoin,carbomer,xanthan gum,parfum,triethanolamine,tocopheryl acetate,hyaluronic acid,methyl paraben,propyl paraben,creatine,tetrasodium edta,phenoxyethanol,caprylyl glycol,sorbic.

成分：去离子水，甘油，辛酸/葵酸三甘油酯，鲸蜡醇，角鲨烷，硬脂酸甘油酯，泛醇，甜菜碱，聚二甲基硅氧烷，薰衣草精油，尿囊素，卡波姆，汉生胶，香精，三乙醇胺，生育酚乙酸酯，透明质酸，对羟基苯甲酸甲酯，对羟基苯甲酸丙酯，肌酸，乙二胺四乙酸四钠，苯氧乙醇，辛二醇，山梨酸。

Ingredients:Water,Glycerin,Caprylic/Capric Triglyceride,Cetearyl Alcohol,Squalane,Glyceryl Stearate,Panthenol,Betaine,Dimethicone,Oiea Europaea Oil,Allantoin,Glyceryl Stearate Se,Carbomer,Xanthan Gum,Parfum,Triethanolamine,Tocopheryl Acetate,Hyaluronic Acid,Methyl Paraben,Propyl Paraben,Creatine,Tetrasodium Edta,Phen-oxyethanol,Caprylyl Glycol,Sorbic.

成分：去离子水，甘油，辛酸/葵酸三甘油酯，鲸蜡硬脂醇，角鲨烷，硬脂酸甘油酯，泛醇，甜菜碱，聚二甲基硅氧烷，橄榄油，尿囊素，自乳化硬脂酸甘油酯，卡波姆，汉生胶，香精，三乙醇胺，生育酚乙酸酯，透明质酸，对羟基苯甲酸甲酯，对羟基苯甲酸丙酯，肌酸，乙二胺四乙酸四钠，苯氧乙醇，辛二醇，山梨酸。

Ingredients:Water,Glycerin,Caprylic/Capric Triglyceride,Myristyl Myristate,Butyrosper-mum Parkii Butter,Glyceryl Stearate,Panthenol,Betaine,Dimethicone,Oiea Europaea Oil,Allantoin,Polysorbate-60,Carbomer,Xanthan Gum,Parfum,Triethanolamine,Tocopheryl Acetate,Hyaluronic Acid,Methyl Paraben,Propyl Paraben,Creatine,Tetrasodium Edta,Phenoxyethanol,Caprylyl Glycol,Sorbic.

成分：去离子水，甘油，辛酸/葵酸三甘油酯，肉豆蔻酸肉豆蔻酯，乳木果油，硬脂酸甘油酯，泛醇，甜菜碱，聚二甲基硅氧烷，橄榄油，尿囊素，聚山梨醇酯-60，卡波姆，汉生胶，香精，三乙醇胺，生育酚乙酸酯，透明质酸，对羟基苯甲酸甲酯，对羟基苯甲酸丙酯，肌酸，乙二胺四乙酸四钠，苯氧乙醇，辛二醇，山梨酸。

Ingredients:water,glycerin,caprylic/capric triglyceride, cetyl alcohol ,propylene glycol,glyceryl stearate,panthenol,betaine dimethicone,simmondsia chinensis, rosa rugosa flower extract,allantoin,carbomer,parfum,triethanolamine,tocopheryl acetate,methyl paraben,propyl paraben,creatine,tetrasodium edta,phenoxyethanol,caprylyl glycol,sorbic.

成分：去离子水，甘油，辛酸/葵酸三甘油酯，鲸蜡醇，丙二醇，硬脂酸甘油酯，泛醇，甜菜碱，聚二甲基硅氧烷，霍霍巴油，玫瑰花提取液，尿囊素，卡波姆，香精，三乙醇胺，生育酚乙酸酯，对羟基苯甲酸甲酯，对羟基苯甲酸丙酯，肌酸，乙二胺四乙酸四钠，苯氧乙醇，辛二醇，山梨酸。

Ingredients: Water,Glycerin,Caprylic/Capric Triglyceride,Myristyl Myristate,Butyrospermum Parkii Butter,Glyceryl Stearate,Panthenol,Betaine,Dimethicone,Hydrolyzed Collagen,Allantoin,Polysorbate-60,Carbomer,Xa-nthan Gum,Parfum,Triethanolamine,Tocopheryl Acetate,Hyaluronic Acid,Methyl Paraben,Propyl Paraben,Creatine,Tetrasodium Edta,Phenoxyethanol,Caprylyl Glycol,Sorbic.

成分： 去离子水，甘油，辛酸/葵酸三甘油酯，肉豆蔻酸肉豆蔻酯，乳木果油，硬脂酸甘油酯，泛醇，甜菜碱，聚二甲基硅氧烷，水解胶原蛋白，尿囊素，聚山梨醇酯-60，卡波姆，汉生胶，香精，三乙醇胺，生育酚乙酸酯，透明质酸，对羟基苯甲酸甲酯，对羟基苯甲酸丙酯，肌酸，乙二胺四乙酸四钠，苯氧乙醇，辛二醇，山梨酸。

Chapter 2 has analysized the conversly synthetic means of solanesol and designed novelly synthetic routes of solanesol and key intermediate Chapter 3 has summarized the preparation of trans-3-methyl-4-hydroxy (bromo-2-butenyl oxy methyl benzene In chapter 4 ,a novel technology of important intermediate(all trans-8-bromo geranyl acetate),which is suitable for industrial procedure , was found .meanwhile,an another new way has been invented ,of which the key intermediate (all trans-8-hydroxy geranyl acetate) has been produced.

第二部分分析了茄尼醇的逆合成方法，设计了一条适合于合成茄尼醇的合成路线及其重要中间体的合成路线。第三部分研究了重要中间体[Trans-3-甲基-4-羟基-2-丁烯基乙酰基(苄基，2，3-二氢吡喃基)醚]的合成新方法，找到了一条适合于工业化生产的制备反式-3-甲基-4-羟基-2-丁烯基苄基醚的新方法。第四部分研究了重要中间体[-3，7-二甲基-8-羟基-2，6-辛二烯-1-醇乙酸酯、-3，7-二甲基-8-溴-2，6-辛二烯-1-醇乙酸酯]的合成新方法，找到了一条适合于工业化生产的制备它们的新方法；同时研究了一条制备-3，7-二甲基-8-羟基-2，6-辛二烯-1-醇乙酸酯的另一新方法。

In order to supply basic thermodynamic data for the separation design of acetyl acetone from the isomerization reaction of isopropenyl acetate,vapor-liquid equilibrium data of isopropenyl acetate-acetyl acetone system under 101.3 kPa was measured using Ellis equilibrium still.

为了给乙酸异丙烯酯异构化生产乙酰丙酮工艺的产物分离设计提供基础热力学数据，用埃利斯平衡蒸馏器测定了101.3 kPa下乙酸异丙烯酯-乙酰丙酮体系的汽液平衡数据，结果表明，该二元体系未形成共沸物，实验数据通过了Herrington面积法的热力学一致性检验。

A series of novel polyethylene glycol derivates was synthesized by esterification of chloroacetic acid with polyethylene glycol. Because of the good reactive activity of α-chlorin in the esters it can react with 5-fluorouracil, thus the conjugate can be obtained .

采用氯乙酸与不同分子量的聚乙二醇进行酯化反应得到氯乙酸聚乙二醇酯，由于酯中的α-氯具有良好的反应活性，将它再与抗癌药物5-氟尿嘧啶结合制备了不同分子量的高分子前药。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

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