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乙酸乙酯

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With 1,4-bezenoquinone and ethyl acetoacetate as the starting materials, it had been prepared in a novel six-step procedure in overall yield of 34.6%.

以1,4-苯醌和乙酰乙酸乙酯为起始原料,经新的六步反应过程,合成阿比朵尔,总收率为34.6%。

KF/NaZnPO4 was used as the catalyst for Michael addition reaction of ethyl acetoacetate and acrylonitrile.

以磷酸锌钠负载KF为催化剂,催化乙酰乙酸乙酯与丙烯腈进行Michael 加成反应。

The synthesis of celery ketone from butyl aldehyde and ethyl acetoacetate was improved with higher yield by using solid superbase(K2O/γ-Al2O3) for the first time.

在正丁醛和乙酰乙酸乙酯为原料合成芹菜酮的合成过程中,对其催化方法进行改进。

The influence of reed produced allelopathy material eathyl-2-methyl acetoacetate on respiration action, photosynthesis action and antioxidant enzymes system of Microcystis aeroginosa were studied.

研究了芦苇产生的化感物质2-甲基乙酰乙酸乙酯对铜绿微囊藻呼吸作用、光合作用和抗氧化酶体系的影响。

The method was proved to be simple,rapid,practical and highly sensitive.It is an efficient method for the quality control of acetoacetic ester.

本法简便,快速、实用,灵敏度高,可有效地用于乙酰乙酸乙酯的质量控制。

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.

摘要] 目的:用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。

The emphasis was on chemical properties,application,main production methods,market,and prospects of main deriva- tives of acetaldehyde such as ethyl acetate,pentaerythritol,glyoxal,peracetic acid, crotonaldehyde and pyridine.

介绍了国内外乙醛及其主要衍生物的生产技术发展及其市场供需状况,尤其对乙醛主要衍生物乙酸乙酯、季戊四醇、乙二醛、乙醛酸、丁烯醛、吡啶的化学性质与用途、主要生产方法、市场供需状况及开发前景作详细介绍和分析。

The propanedinitrile is synthesised from ethyl cyanoacetate by amination and elimination reaction.

由氰乙酸乙酯与氨反应生成氰乙酰胺,再经过消除反应制得丙二腈。

The condensation of aromatic aldehydes with active methylene compounds like malononitrile, cyanoacetamide and ethyl cyanoacetate has been found to proceed very efficiently at room temperature giving excellent yields, but the condensation of heteroaromatic,α,β-unsaturated and aliphatic aldehydes with active methylene compounds proceeded smoothly in 50~65℃ with good yields and the reactions of aromatic, aliphatic ketones as well as p-phthalaldehyde with malononitrile also proceeded in 75~85℃ with moderate yields.

芳香醛与活泼亚甲基化合物如丙二腈、氰基乙酸乙酯、氰基乙酰胺的缩合在室温下即能顺利进行,获得了很高的收率;而对于杂环芳醛、α,β-不饱和的醛以及脂肪醛与活泼亚甲基化合物的缩合,需在50~65℃下进行,也取得了很高的收率;对于脂肪酮、芳香酮以及二元醛与丙二腈的缩合在75~85℃下也能顺利地进行,获得中等以上的收率。

Methods A mixture of 10 mol/L potassium dihydrogen phosphate solution and acetonitrile(60 ∶ 40) was used as the mobile phase.

方法以乙腈-10mmol/L磷酸二氢钾(40∶60)为流动相,炔雌醇为内标,血浆样品经乙酸乙酯萃取。

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