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The optimum reaction conditions are as follows: diphenylmethanethiol : methyl chloroacetate is 1:1.5, and the reaction carried out at 100℃ for 4 h, 2- acetamide can be carried out in the room temperature for 20 h, the yield of 2- acetamide was 76%, hydrogen dioxide: 2- acetamide is 1:1, and the reaction carried out at 60℃ for 3 h, the yield of modafinil was 79%, the total yield of reaction can be reached 48%.

研究表明,采用氯乙酸甲酯作为醚化试剂,反应时间4h,反应温度100℃,二苯甲硫醇:氯乙酸甲酯=1:1.5,室温下氨解反应20h,二苯甲硫乙酰胺收率76%;采用过氧化氢作为氧化试剂,反应时间3h,反应温度60℃,过氧化氢:二苯甲硫乙酰胺=1:l,莫达非尼收率79%,反应总收率可达48%。

To study the corrosion of dehydration column in acetic acid plant,a mathematical model of separation process was developed.

为解决乙酸装置脱水塔的腐蚀问题,建立了乙酸生产分离过程的数学模型,对脱水塔的操作工况进行了模拟分析。

The yields of peracetic acid is studied from two different preparation methods using hydrogen peroxide and acetic acid or acetic anhydride .

比较了用乙酸乙酸酐分别与过氧化氢反应制备所得的过氧乙酸的浓度。

The synthesis of sucrose octaacetate from sucrose with acetic anhydride in the presence of anhydrous sodium acetate is reported.

报道了在无水乙酸钠存在下,蔗糖和乙酸酐反应合成蔗糖八乙酸酯。

However, when the target organic was acetic acid (an inhibitor of radical reaction),Fe2+/O3 and O3 had similar degradation efficiencies.

当目标有机物是对自由基链反应具有抑制剂作用的乙酸时,O3和Fe2+/O3对乙酸有着相似的降解效率。

In particular, when the Knoevenagel condensation of 2-hydroxybenzaldehyde was conducted with ethyl 2-cyanoacetate, 3-ethoxycarbonylcoumarin was obtained by simultaneous cyclization and alcoholysis of cyanide.

当反应底物为水杨醛与氰基乙酸乙酯的时候,产物为3-乙氧基羰基香豆素,这是水杨醛和氰基乙酸乙酯缩合关环,再发生氰基醇解的产物。

The route include three steps: etherification, ammoniation and then oxidation. Factors such as chloracetate, reaction temperature on process were studied. And discussed the ionic liquid was recovered.

讨论了不同的氯乙酸酯和反应温度对醚化反应收率的影响,讨论了不同的二苯甲硫乙酸酯对氨解反应收率的影响,及离子液体的回收使用。

This paper introduces in detail the factors influencing the yield of the amino acetic acid with the chloroacetic acid ammonolysis process, and connecting with the production procedures, makes deep analysis, and puts forward some corresponding methods for increasing the yield.

详细介绍了氯乙酸氨解法氨基乙酸生产过程中影响收率的因素,并结合生产过程进行了深入分析,有针对性地提出了提高收率的办法。

The synthesis of i amyl acetate from i amylic alcohol and acetic acid using silica gel carrier acid as catalyst is reported.

乙酸和异戊醇为原料,采用硅胶载体酸为催化剂合成乙酸异戊酯。

The results also indicated a low production of acetic acid, acetoin and ethyl acetate, and high amounts of amyl alcohols in all of the ciders.

结果在所有萍果汁也表明了乙酸、乙醛和乙酸乙酯的低产量和大量产生的戊基乙醇。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力