乙酸

The results showed as follows: 1 Extraction of gelsemium total alkaloids. Total alkaloids were extracted with 95 per cent ethanol. The extract rate was 0.519 per cent and the extract purity were 88.02 per cent and 87.38 per cent; Total alkaloids were extracted with chloroform .The extract rate was 0.416 per cent and the extract purity were 89.02 per cent and 94.52 per cent. 2 Isolation of gelsemium total alkaloids with TLC. Total alkaloids contained five or more alkaloids. The optimal developing agent was chloroform :methanol :ethyl acetate(9:l:0.3),the optimal eluent was methylene chloride:methanol(92:8). 3 Isolation of total alkaloids with column chromatography. Alkaloid A and alkaloid B were obtained, alkaloid B was identified as koumine.

研究结果如下：1、钩吻总碱的提取：用95％的乙醇提取钩吻生物碱提取率为0.519％，其提取物纯度为88.02％、87.35％；用氯仿提取钩吻生物碱提取率为0.416％，其提取物纯度为89.02％、94.52％。2、钩吻总碱的薄层层析分离：总碱中含有5种或5种已上的生物碱；氯仿：甲醇：乙酸乙酯(9：1：0.3)是最佳薄层层析的展开剂；二氯甲烷：甲醇(92：8)是柱层析的最佳洗脱剂。3、钩吻总碱的柱层析分离：共得到两种钩吻生物碱单体成分碱A和碱B，碱B为钩吻素子，碱A可能是钩吻素甲。4、钩吻总碱的急性毒性试验：钩吻总碱小鼠腹腔注射的半数致死量LD_(50是：7.38mg／kg，95％的可信限范围为：6.67mg／kg～7.94mg／kg。

Our country ethylene diamine mainly uses in producing the agricultural chemicals (woods manganese zinc, dithane Z-78, generation of woods amine and pesticide, weed killer, disinfectant), the surface active agent (lives geminate stearic acid amide, alkyl imidazole lin, double amide, with oxirane, epoxypropane synthesizes non-ionic surface active agent), the epoxy resin firming agent (polyamide resins, epoxy firming agent, hydroxyethyl ethylene diamine and so on), the wash assistant (ethylene diamine four ethanoic acid and sodium salt series chelating agents), medicine raw material (aminophylline, washes must be peaceful, nose eye only, deinsectization spirit and so on), water treatment medicinal preparation (ethylene diamine four methylene phosphonates, second grade trunk base ethylidene two phosphine acids), corrosion inhibitor dye fixing agent, photography materialFixing bath and oil dope and so on.

我国乙二胺主要用于生产农药（森锰锌、代森锌、代森胺及杀虫剂、除草剂、杀菌剂），表面活性剂（生成双硬脂酸酰胺，烷基咪唑啉、双酰胺，与环氧乙烷，环氧丙烷合成非离子表面活性剂），环氧树脂固化剂（聚酰胺树脂，环氧固化剂，羟乙基乙二胺等），洗涤助剂（乙二胺四乙酸及其钠盐系列螯合剂），医药原料（氨茶碱，洗必泰，鼻眼净，灭虫灵等），水处理剂（乙二胺四甲叉膦酸盐，乙脒基乙叉二膦酸），缓蚀剂染料固色剂，照相材料定影液及润滑油添加剂等。

Sinopodohyllum hexandrum seeds were treated with different concentration NaHCO3, Na2CO3, KT, GA3, NAA, 6-BA and 2, 4-D. The effects of different chemicals on Sinopodohyllum hexandrum seeds were measured, and seed germination rate, germinability, germination index and germination speed were determined.

方法］用不同浓度的碳酸氢钠、碳酸钠、细胞激动素、赤霉素、萘乙酸、6-苄基－嘌呤和2，4-D等7种药剂处理桃儿七种子，通过测定种子发芽率、发芽势、发芽指数和发芽速度等活力指标研究药剂对桃儿七种子萌发的促进作用。

Glyceraldehyde, glycoladehyde, glycolic acid, and formaldehyde were identified as the intermediate products.

甘油光催化降解最终产物是H_2O和CO_2，检测到了甘油醛、羟基乙醛、羟基乙酸、甲醛等中间产物。

As a kind of widely used fine chemical, glyceryl triacetate was synthesized by esterification of glycerin with acetic acid.

三乙酸甘油酯是一种用途广泛的精细化工产品。

The effect of different reaction conditions,such as catalyst concentration,molar ratio of reactants,reaction temperature,reaction time,on the coupling reaction of trioxane and methyl formate synthesizing methyl glycolate and methyl methoxy acetate using sulfuric acid as catalyst has been studied.Through the analysis for the yield of products and system pressure,and comparison with other different acidity catalysts,we considered that the activation of formaldehyde was the control step of reaction rate to the...

以硫酸为催化剂，研究了三聚甲醛与甲酸甲酯偶联合成乙醇酸甲酯和甲氧基乙酸甲酯的反应中，催化剂浓度、原料配比、反应温度、反应时间等条件对反应过程的影响，通过对产物收率和系统压力变化的分析，并结合与其它不同酸强度催化剂的对比，得到甲醛的活化是偶联反应的速率控制步骤，催化剂的酸强度决定其对甲醛的活化能力，是影响偶联反应的主要因素。

Acid catalyst and H + catalysis in the acid catalysts were studied for synthesis of methyl glycolate via coupling of methyl formate and trioxane in a microform high-pressure autoclave(120mL).

在微型高压反应釜中(12 0ml)，考察了酸催化三聚甲醛和甲酸甲酯制备羟基乙酸甲酯的偶联反应，并对酸催化剂中H+的作用进行了研究。

During photorespiration the enzyme glycolate oxidase catalyzes the oxidation,by molecular oxygen,of glycolic acid to glyoxylic acid and hydrogen peroxide in the peroxisomes.

乙醛酸在转氨酶作用下转化成氨基乙酸。

SODIUM GLYCOLATE— Transfer about 500 mg of it, accurately weighed, into a 100-mL beaker, moisten thoroughly with 5 mL of glacial acetic acid, followed by 5 mL of water, and stir with a glass rod to ensure proper hydration (usually about 15 minutes). Slowly add 50 mL of acetone while stirring, then add 1 g of sodium chloride, and stir for several minutes to ensure complete precipitation of the carboxymethylcellulose.

乙醇酸钠—取本品500mg，精密称定，置于100mL烧杯中，用5mL冰乙酸完全润湿，接着加5mL水，并用玻棒搅拌使水合作用完全（搅拌时间一般为15分钟），边振摇边缓缓加入50mL丙酮，再加入1g氯化钠，振摇几分钟以确保羧甲基纤维素沉淀完全。

Cephalotaxine ester of 2-oxo-6-methylheptanoic acid was treated with lithium diisopropylamide and Me O-(1-methoxyisopropyl)glycolate to give a mixture of homoisoharringtonine and its stereoisomers with 56% yield. The four stereoisomers separated by TLC showed identical mass spectra and almost superimposed IR but with different 1H NMR spectra. The configuration of the 2'-C and 3'-C of the four isomers were postulated based upon their 1H NMR spectra as compared with the 1H NMR spectra of isoharringtonine and its stereoisomers.

2-氧代-6-甲基庚酰基三尖杉碱(3)与0-(1-甲氧基异丙基)羟基乙酸甲酯(4)在强碱性试剂二异丙胺锂存在下，起亲核加成反应，反应中间体5在室温用酸性丙酮水解，得到一种新的三尖杉酯类生物碱一一高异三尖杉酯碱(6c)及其立体异构体(6a、6b、6d)的混合物，产率56%、通过制备薄层层析分得这四个立体异构体，它们的1H NMR和异三尖杉酯碱及其立体异构体的1H NMR类似，推定了它们的绝对构型。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新