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乙酰苯

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Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5:1)中和-2,6-二羟基甲苯环合得1,3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

In order to study the mechanism of the biotype of Galium aparine resistant to tribenuron-methyl, the differences on ALS, GSTs, SOD and POD of the resistant and susceptible biotypes to tribenuron-methyl were preliminarily determined.

为探讨猪殃殃Galium aparine抗药性生物型对苯磺隆的抗性机制,测定了苯磺隆对猪殃殃抗性、敏感生物型体内靶标酶[乙酰乳酸合成酶]、代谢酶[谷胱甘肽-S-转移酶]及抗氧化酶影响的差异。

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e,7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟醚类氨基甲酸甲酯3a-e,进一步胺解之后得到了肟醚类氨基甲酰甲胺3f-j。

With the in-situ single-stage self-metallization protocol,surface-silvered polyimide film has been prepared using pyromellitic dianhydride/ 4,4\'-oxydianiline-based polyimide as the matrix and (1,1,1-trifluoro-2,4-pentadionato)silveras the silver precursor.

在原位一步自金属化法中,以均苯四甲酸酐/4,4\'-二胺基二苯醚基聚酰亚胺为基体,以三氟乙酰丙酮银作为银的母体制备出了表面金属化的聚酰亚胺银复合薄膜。

A HPLC method for determination of phenylephrine hydrochloride, paracetamol, caffeine anhydrous ,salicylamide and brompheniramine maleate in Liufenkamin tablets was established.

建立了HPLC法测定柳酚咖敏片中盐酸去氧肾上腺素、对乙酰氨基酚、无水咖啡因、水杨酰胺、马来酸溴苯那敏的含量。

Benzoylated phenyl a - and B - 2 - thio - D - fructofuranosides were synthesized and coupled with protected sucrose acceptor to synthesize a - D - fructofuranoside - linkage stereospecifically by employing NIS/AgOTf as catalysts.

在果糖的合成研究中,合成了四苯甲酰基苯基果糖硫苷,并首次将其用作糖苷化反应的给体,在NIS/AgOTf的促进之下,与乙酰化保护的蔗糖受体反应,从而以高产率立体专一地合成了α构型的呋喃果糖苷。

They are insoluble in water, ethanol, methanol, acetone, chloroform and benzene, but soluble in DMA, DMF and DMSO.

它们溶于N,N-二甲基甲酰胺、N,N-二甲基乙酰胺和二甲基亚矾等溶剂,但不溶于水、乙醇、甲醇、丙酮、氯仿和苯。

A plausible process of this reaction is as following: Aldehyde was in equilibrium with the enol form, aldehyde reacted with aniline catalyzed by 2,2,2-trichloroacetic acid to afford imine, the generated imine immediately reacted with enol to form intermediate via intramolecular cyclization.

我们发现一分子芳基叠氮和一分子三苯基磷反应生成一分子磷亚胺,后者与由两分子取代的苯氧乙酰氯原位生成的烯酮反应生成4-亚烷基-β-烷基-内酰胺,其串联过程涉及烯酮亚胺的形成及其与烯酮的[2+2]的环加成反应。

Our method featured employing the glycosyl donor with Bz as the protectivegroups and 0.05 equiv of TMSOTf as the promoter.

即:用苯甲酰基保护的三氯乙酰亚胺酯作给体,用5%当量的TMSOTf作促进剂,在室温下反应5min至15min。

Our method featured employing the glycosyl donor with Bz as the protective groups and 0.05 equiv of TMSOTF as the promoter.

即:用苯甲酰基保护的三氯乙酰亚胺酯作给体,用 5%当量的 TMSOTf 作促进剂,在室温下反应 5 min 至 15 min。

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