乙酰胺基

N-（3-Amino-4-methoxyphenyl）acetamide is an important intermediate for the production of azo disperse dyes,while it is still produced by reduction with iron powder in industry currently.

摘 要： N-（3-氨基-4-甲氧基苯基）乙酰胺是生产偶氮型分散染料的一类重要中间体。现有的工业生产方法仍全部采用铁粉还原。

STUDY ON THE EQUILIBRIUM AND COORDINATION COMPOUND OF IRONEXTRACTION WITH N,N-DI (1-METHYLHEPTYL)ACETAMIDE IN HYDROCHLORIC ACID

N，N-二(1-甲基庚基)乙酰胺在盐酸介质中对铁的萃取平衡及其配合物的研究-中国学术期刊网络出版总库

A novel Pd／C catalyst with high activity,high selectivity and good stability developed by our group was used for the hydrogenation of N-（3-nitro-4-methoxyphenyl）acetamide into N-（3-amino-4-methoxyphenyl）acetamide in methanol and water,respectively.

笔者开发了一种高效的Pd／C催化剂，分别选用甲醇和水作为反应溶剂，实现了高活性、高选择性和高稳定性地催化加氢制备N-（3-氨基-4-甲氧基苯基）乙酰胺。

We provide intermediates of Methylphenidate HCl: 2-Phenyl-2-(2-Piperidyl) Acetamide; 2-Phenyl-2-(2-Piperidyl) Acetic Acid; Series of Benzoic Acid、Benzonitrile; Other pharmaceutical intermediates.

提供盐酸利他林中间体：2-苯基-2-(2-哌啶基)乙酰胺；2-苯基-2-(2-哌啶基)乙酸；苯甲酸、苯甲腈系列及其他医药中间体。

Polyethersulfone with Cardo is a developed engineering thermoplastic and membrane material with high glass transition temperature. PES-C ultrafiltration membranes were prepared by phase inversion method using dimethylacetamide as solvent and PVPK3O as additive.

采用凝胶相转化法，以新型耐高温工程塑料－含酚酞侧基的聚芳醚砜为膜材料，N，N-二甲基乙酰胺为溶剂，通过改变铸膜液中添加剂聚乙烯吡咯烷酮(PVPK30)的含量，在平板刮膜机上制备了一系列超滤膜。

Based on broad information collection, author compared and studied on the old synthesis process, and proposed the better process that started from benzyl chloride, then according to the sequence of " synthesis of benzylamine, synthesis of N-benzyl-N--acetamine, synthesis of 2-chloro-5-methylpridine ,2-chloro-5-trichloromethylpyridine,2-chloro-5-trifluropyridine " five steps to get the final product, CTFP.

本文在查阅大量文献资料和对2-氯-5-三氟甲基吡啶合成路线进行分析比较的基础上，提出了较佳合成路线，即以氯化苄为原料，合成的反应步骤为&苄胺&合成、&N-苄基-N--乙酰胺&合成、&2-氯-5-甲基吡啶&合成、&2-氯-5-三氯甲基吡啶&合成、&2-氯-5-三氟甲基吡啶&合成五步。

Based on hydrogen peroxide and ammonium persulfate as compounded initiating system,unsaturated vinyl monomers were used to directly copolymerize a new high range polycarboxylate water reducer structurized in carboxyl,esterquat and amido as main chain and in polyethylene glycol ether as side chain.

以过硫酸铵和双氧水为复合引发体系，采用不饱和单体直接共聚，得到一类主链为羧基、酯基、酰胺基，侧链为聚乙二醇醚基的新型聚羧酸高效减水剂，研究了共聚物的结构对分散性能的影响。

The condensation of aromatic aldehydes with active methylene compounds like malononitrile, cyanoacetamide and ethyl cyanoacetate has been found to proceed very efficiently at room temperature giving excellent yields, but the condensation of heteroaromatic,α,β-unsaturated and aliphatic aldehydes with active methylene compounds proceeded smoothly in 50~65℃ with good yields and the reactions of aromatic, aliphatic ketones as well as p-phthalaldehyde with malononitrile also proceeded in 75~85℃ with moderate yields.

芳香醛与活泼亚甲基化合物如丙二腈、氰基乙酸乙酯、氰基乙酰胺的缩合在室温下即能顺利进行，获得了很高的收率；而对于杂环芳醛、α，β-不饱和的醛以及脂肪醛与活泼亚甲基化合物的缩合，需在50~65℃下进行，也取得了很高的收率；对于脂肪酮、芳香酮以及二元醛与丙二腈的缩合在75~85℃下也能顺利地进行，获得中等以上的收率。

The structural assignment of Ⅱwas supported by spectral data and was confirmed by the identification of the compound as the product obtained by synthesis from triethyl orthoacetate and 2- cyanot hioacetamide.

结构的指定得到由光谱数据的支持，确认结构是通过原乙酸三乙酯和2-氰基-硫代乙酰胺合成得到的化合物。

The Sm or Yb complexes were tested to be used as a catalyst for the Diels-Alder reaction of cyclopentadiene with methyl acrylate.

用α-亚磺酰基-N，N-二取代乙酰胺同三氯化钐和三氯化镱反应得到了相应的稀土配合物，用元素分析、红外光谱进行了结构表征。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。