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乙酰胺基

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It was obtained with ethylenediamine and ethenesulfonic sodium as primary material through addition.

它是一种易降解的新型Gemini表面活性剂-N, N'-双癸酰基乙二胺二乙磺酸钠的中间体。

N-(1-Naphthyl)ethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-(1-萘基)乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

N-1-Naphthylethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-1-萘基乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

Results After screening, 59 subtracted library clones were isolated which were specific for strain VIB72, and the DNA sequences of these clones were determined. Seventeen fragments showed high homology to the genes of known functions in other bacteria. This includes soluble lytic murein transglycosylase, mobilization protein, transposase (IS66), resistance-related protein (metallo-beta-lactamase and acetyltransferase family), toxin protein (DT-201 and alveicin A immunity protein), ATP-dependent endonuclease of OLD family like protein, SocE and GTP-binding protein HflX (high frequency of lysogenization).

通过对差减文库筛选,分离到59个对菌株VIB72的克隆,并对这些克隆的DNA序列进行了测定。17个基因片断与其它细菌的已知功能的基因有较高的同源性,其中包括可溶性溶胞壁质转糖基酶、转移蛋白MobA和MobC、转座子IS66、抑制相关蛋白(金属β-内酰胺酶和乙酰转移酶家族)、毒素蛋白(DT-201和alveicin A免疫蛋白)、与OLD 家族相似的ATP依赖性核酸内切酶以及SocE 和GTP结合蛋白HflX。

Ten novel derivatives of 1-phenyl-5-[5-(substituted anilinocarbonylmethylthio)-4-phenyl-1,2,4- triazol-3-ylmethylthio]-tetrazole were synthesized rapidly in high yields by the reaction of N--2-chloryacetanilide (3) with 1-phenyl-5-(5-mercapto-4-phenyl-1,2,4-triazol-3-ylmethylthio)-tetrazo- le (2) under microwave irradiation and phase transfer catalysis conditions.

采用微波和相转移催化法通过1-苯基-5-(4-苯基-1,2,4-三唑-5-巯基-3-甲硫基)四唑(2)与2-氯乙酰芳胺(3)反应高效、快速地合成了10种尚未见文献报道的1-苯基-5-[5--4-苯基-1,2,4-三唑-3-甲硫基]四唑。其结构经IR,1HNMR,13CNMR和元素分析表征。生物活性实验结果表明,该类化合物在较低浓度下部分化合物对小麦芽有很好的促进作用

In chapter four, molecular imprinting polymers against amino acid derivatives utilizing 2-VP+AM as combined functional monomer and trimethylolpropane trimethacrylate as tribasic cross-linker were prepared and result was compared with those with the same amino acid derivative as the imprinted molecules utilizing ethyleneglycol dimethacrylate as dibasic cross-linker. It was found that cross-link intensity of the molecular imprinting polymer is higher when TRIM was utilized and baseline separation for the imprinted molecule could be achieved. When TRIM was utilized as cross-linker more molecule is imprinted during the polymerization.

第四章采用2-乙烯基吡啶+丙烯酰胺复合功能单体,考察了三元交联剂三甲氧基丙烷三甲基丙烯酸酯烙印氨基酸衍生物的情况,并与二元交联剂乙二醇二甲基丙烯酸酯烙印相同氨基酸衍生物的情况进行了对比,发现三甲氧基丙烷三甲基丙烯酸酯交联剂在较小的用量下就可使分子烙印聚合物达到足够的交联度,实现烙印分子的基线分离。

Comb-shaped copolymer of polycarboxylate containing carboxyl,sulfonic groups(-SO3M),polyethylene glycol(-OC2H4-) was synthesized by monomers of sodium 2-acrylamido-2-methylpropane sulphonate,acrylic acid,polyethylene glycol monoester acrylate under certain conditions.

本文通过2-丙烯酰胺-2甲基丙基磺酸钠与丙烯酸、聚乙二醇单丙烯酸酯在一定条件下发生聚合反应合成含有羧基、磺酸基(—SO3M)、聚氧乙烯链(—OC2H4—)等侧链的高性能减水剂PC。

Our method featured employing the glycosyl donor with Bz as the protectivegroups and 0.05 equiv of TMSOTf as the promoter.

即:用苯甲酰基保护的三氯乙酰亚胺酯作给体,用5%当量的TMSOTf作促进剂,在室温下反应5min至15min。

Our method featured employing the glycosyl donor with Bz as the protective groups and 0.05 equiv of TMSOTF as the promoter.

即:用苯甲酰基保护的三氯乙酰亚胺酯作给体,用 5%当量的 TMSOTf 作促进剂,在室温下反应 5 min 至 15 min。

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