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乙酰胺

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It seemed to have something to do with lysergic acid diethylamide, LSD-25, the substance he had been working on.

这好像与他所致力于合成的一种物质———麦角酸酰二乙胺( LSD-25)有些关系。

Monochloroethylene carbonate is prepared by chlorination of ethylene carbonate with sulfuryl chioride ,a solution of monochloroethylene carbonate in ethylene carbonate is reacted with triethylamine to give vinylene carbonate.A parameter design method was applied to select the optimum synthesis conditions.63.3% and 78% yields superior to the conventional for monochloroethylene carbonate and vinylene carbonate were obtained respectively,and the process was also simplified .

以碳酸乙烯酯为原料,用磺酰氯作为氯化剂生成一氯代碳酸乙烯酯,三乙胺为脱卤化剂在碳酸乙烯酯溶剂中合成碳酸亚乙烯酯,对一氯代碳酸乙烯酯和碳酸亚乙烯酯制备的工艺参数进行优化,收率分别达到63.3%和78%,均超过了传统方法,且简化了工艺,缩短了反应时间,易于工业化生产。

Using stearic acid, hexadecanoic acid,thionyl chloride,triethylamine as raw material, neutral sizing agent AKD was synthesized through three steps of reaction,i.

以硬脂酸、棕榈酸、氯化亚砜、三乙胺为原料,经过酰氯化、缩合和浓缩三步反应合成了中性施胶剂AKD。

Due to their applications in magnetic, optical, electronic and catalyst, polynuclear lanthanide clusters are of importance. In this part, a series of nanowheel-shaped nonanuclear lanthanide clusters,〓〓(Ln=Sm~Tm; BA=benzoylacetone), were prepared and characterized. Each complex can exist in three phases, i. e., cubic, tetragonal and triclinic.

本论文第二部分在醇溶液中以三乙胺调变溶液pH,利用β-二酮配位方式的灵活性成功地构筑了一系列结构稳定、纳米尺度轮状的九核稀土配合物〓〓(Ln=Sm~Tm;BA=苯甲酰丙酮),并在不同溶剂中重结晶分别得到了三斜、四方以及立方三种晶型的晶体。

The final product Rimonbant was then obtained in 64% yield via chlorination of the acid with oxalyl chloride followed by treatment of the resultant acyl chloride with 1-aminoperidine.

酰氯与1-氨哌啶在三乙胺存在下缩合生成目标产物利莫那班,产率64%。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生,用WatersHPLC仪,AccQ-TagTM专用C18柱(3.9mm×15cm),以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A,乙腈为溶剂B,超纯水为溶剂C,进行梯度洗脱,检测波长为248nm,35min测试完毕。

Methods The amino acids in the injections were pretreated with 6-aminoquinolyl-N-hydroxysuccinimdyl separately and their derivatives were analyzed on Waters 2695 HPLC using AccQ-Tag column. Gradient eluents consisted of sodium acetate solution (pH 4.95), acetonitrile and water. The Detection wavelength was 248 nm and column temperature 37℃.

采用AccQ-Tag法,以6-氨基喹啉-N-羟基琥珀酰亚胺基甲酸酯为衍生试剂,与复方氨基酸注射液(18AA-V)中17种氨基酸柱前衍生,用Waters 2695 HPLC仪器,AccQ-Tag柱,以醋酸钠(pH 4.95)缓冲液为流动相A,乙腈为流动相B,水为流动相C进行梯度洗脱,检测波长为248 nm,柱温为37℃,进样量为5μL。

Unsaturated polyester resins are the most widely used resin type for composites, comprising in excess of 80% of all thermoset resins (others being epoxies, phenolics, acrylics, imides, and urethanes).

不饱和聚酯树脂是复合材料使用树脂类型中应用最广泛的一种,也是热固性树脂最常用的一种(其它种类热固性树脂包括环氧树脂、酚醛树脂、丙烯酸树脂、酰亚胺树脂以及氨基甲酸乙酯)。

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