乙酰胺

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ，N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

These products include sodium percarbonate, percarbamide, 4Na 2SO 4·2H 2O 2·NaCl adduct, tertiary amine oxides, hydrazine hydrate, dihydroxy benzene, quaternary ammonium salt hydrogen peroxide and methylethyl ketone oxime.

介绍了近期国外过氧化氢在部分化学品合成中应用研究新进展，产品包括过碳酸钠、过碳酰胺、4Na2 SO4·2H2 O2 ·NaCl加合物、叔胺氧化物、水合肼、二羟基苯、季铵盐过氧化氢和甲乙酮肟。

Inorganic chemistry ; hydrogen peroxide ; review ; sodium percarbonate ; percarbamide ; 4Na 2SO 4·2H 2O 2·NaCl adduct ; tertiary amine oxides ; hydrazine hydrate ; dihydroxy benzene ; quaternary ammonium salts hydrogen peroxide ; methylethyl ketone oxim

无机化学；过氧化氢；综述；过碳酸钠；过碳酰胺； 4Na2SO4·2H2O2·NaCl加合物；叔胺氧化物；水合肼；二羟基苯；季铵盐过氧化氢；甲乙酮肟；合成；催化剂；质量；安定性；收率

A HPLC method for determination of phenylephrine hydrochloride, paracetamol, caffeine anhydrous ,salicylamide and brompheniramine maleate in Liufenkamin tablets was established.

建立了HPLC法测定柳酚咖敏片中盐酸去氧肾上腺素、对乙酰氨基酚、无水咖啡因、水杨酰胺、马来酸溴苯那敏的含量。

Results After screening, 59 subtracted library clones were isolated which were specific for strain VIB72, and the DNA sequences of these clones were determined. Seventeen fragments showed high homology to the genes of known functions in other bacteria. This includes soluble lytic murein transglycosylase, mobilization protein, transposase (IS66), resistance-related protein (metallo-beta-lactamase and acetyltransferase family), toxin protein (DT-201 and alveicin A immunity protein), ATP-dependent endonuclease of OLD family like protein, SocE and GTP-binding protein HflX (high frequency of lysogenization).

通过对差减文库筛选，分离到59个对菌株VIB72的克隆，并对这些克隆的DNA序列进行了测定。17个基因片断与其它细菌的已知功能的基因有较高的同源性，其中包括可溶性溶胞壁质转糖基酶、转移蛋白MobA和MobC、转座子IS66、抑制相关蛋白（金属β-内酰胺酶和乙酰转移酶家族）、毒素蛋白（DT-201和alveicin A免疫蛋白）、与OLD 家族相似的ATP依赖性核酸内切酶以及SocE 和GTP结合蛋白HflX。

Results Eleven compounds were obtained and identified as sarcodonin A, scabronine B, 3β-hydroxy-5α, 8a-epidioxyergosta-6, 22-dien,(22E, 24R)-ergosta-7, 22-diene-3β, 5α, 6β-triol,(22E, 24R)-ergosta-7, 22-diene-3β-ol, benzoic acid, 4-hydroxylben-zaldehyde, 4-monopropanoylbenzenediol, ethy1-β-D-glucopyranoside, thioacetic anhydride,(2S, 2'R, 3S, 4R)-2-(2-hydroxyoctadecanoylamino) docosane-1, 3, 4-triol.

结果共分离鉴定了11个化合物，分别是：sarcodonin A、scabronine B、3β羟－5α，5α-过氧麦角甾－6，22-二烯－3β-醇、(22E，24R)-麦角甾－7，22-二烯－3β，5α，6β三醇、(22E，24R)-麦角甾－7，22-二烯－3β-醇、苯甲酸、对羟基苯甲醛、对羟基苯甲酸乙酯、乙基－β-D-吡喃葡萄糖苷、硫代乙酸酐、（25，2'R，3S，4R）-2-（2-羟基－十八碳酰胺）二十二碳烷－l，3，4-三醇。

A new chelating fiber containing thioamide group is synthesized by cross-linking of polyacrylonitrile fiber with ethylene-dimine and following with chemical modification with sodium sulfide using DMF as solvent.

以腈纶纤维为起始原料，经乙二胺预交联后，以DMF作溶剂与硫化钠反应，合成了一种硫代酰胺功能基可达6.8mmol/g干纤维的螯合功能纤维，其对贵金属金、银离子具有良好的吸附性能。

The results show that 60Co-γ ray radiation has the most remarkable effect on the degradation of organophosphorus pesticides such as fenitrothion, parathion, methyl-parathion, phorate and chlorpyrifos and the maximum degradation rates are over 85%. The degradation rates of methamidophos, acephate, malathion ,dimethoate are slightly inferior to them and the optimum degradation rates is just only 34.70%. At the same time, the contents of soluble total sugars, glucose, fructose, sucrose and total sugars in apple juice decrease unconspicuously, but the total acid content in apple juice and its color value and clarity increase. Based on a comprehensive consideration of the 60Co-γ radiation effect on the actual degradation of organophosphorus pesticides in apple juice and its main chemical and physical indexes, organophosphorous pesticides residue will be decreased to a lower level with radiation dose of about 5 kGy but the main chemical and physical indexes of export apple juice can not be affected.

结果表明： 60Co-γ射线辐照处理对苹果汁中杀螟硫磷、对硫磷、甲基对硫磷、甲拌磷、毒死蜱降解效果最为显著，最高降解率均在85%以上；对苹果汁中甲胺磷、乙酰甲胺磷、马拉硫磷和乐果的降解效果不显著，最高降解率仅为35%；在0～9 kGy辐照剂量范围内降解苹果汁中有机磷农药的同时，会使苹果汁中的可溶性固形物、葡萄糖、果糖、蔗糖及总糖含量轻微降低，苹果汁的总酸度有所增加，苹果汁的色值及透光率提高；综合分析60Co-γ射线辐照对苹果汁中有机磷农药的实际降解效果及对苹果汁主要理化指标的影响，选用5 kGy的辐照剂量已完全使苹果汁中的有机磷农药残留降低到一个很低的水平，又不会对苹果汁出口主要理化指标造成影响。

A series of pH- and temperature-sensitive hydrogels carrying pendant phosphategroups have been synthesized by copolymerizing 2-methacryloyloxyethyl dihydrogenphosphate with N-isopropylacrylamide. The swelling ratio, swelling and deswellingkinetics have been investigated. High loading percentage of lysozyme into hydrogelshas been achieved and the release profile has been studied.

通过N-异丙基丙烯酰胺和含磷酸基团的单体2-甲基丙烯酰乙氧基二氢磷酸酯的共聚合，合成了一类含磷酸基团的既对温度敏感又对pH敏感的水凝胶，研究了它们在不同pH及温度时的溶胀率及溶胀动力学，并初步研究了其对溶菌酶的释放行为。

acetyl chloride, a novel fluorescence derivatization reagent, has been developed for the determination of sterols and stanol .

采用荧光衍生化试剂2-(9-咔唑)乙酰氯，对天然产物谷甾醇、豆甾醇、菜油甾醇及谷甾烷醇的柱前衍生化条件，包括催化剂的种类、反应温度、衍生化时间等进行了考察，结果表明：催化剂选用三乙胺，反应温度80℃，时间20min，衍生产物具有恒定的最大检测响应值。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。