乙酰甲醇

A novel Pd／C catalyst with high activity,high selectivity and good stability developed by our group was used for the hydrogenation of N-（3-nitro-4-methoxyphenyl）acetamide into N-（3-amino-4-methoxyphenyl）acetamide in methanol and water,respectively.

笔者开发了一种高效的Pd／C催化剂，分别选用甲醇和水作为反应溶剂，实现了高活性、高选择性和高稳定性地催化加氢制备N-（3-氨基-4-甲氧基苯基）乙酰胺。

The main contents are:(1) The polarized laser Raman spectra of acetone, methyl alcohol, alcohol, ethylene glycol, formamide, acetonitrile, acetic acid, Chloroform, Methylene chloride, and Bromoform are measured in the experiment.(2) The depolarization ratio of Raman shift in the measured spectrum are

主要的结果有：得到了丙酮分子9条喇曼谱线、甲醇分子5条喇曼谱线、乙醇分子9条喇曼谱线、乙二醇分子7条喇曼谱线、甲酰胺分子8条喇曼谱线、乙腈分子8条喇曼谱线、乙酸分子8条喇曼谱线

Methods Paracetamol was analyzed with HPLC,ODSC18 was packed in the analytical column,and phenacetin as internal standard.the mobile phase consisted of methanolwater(70:30)and the flow rate was 1.0 ml/min,The UV detection wave length was 257 nm.

采用ODSC 18色谱柱，内标为非那西丁，流动相为甲醇水(70：30，v/v)，流速1.0 ml/min，检测波长257 nm，测定泰诺片中对乙酰氨基酚的含量。

Computationalresults indicate that the no-planar trans-benzanilide is the most stable structure. The spectra indicate that the Franck Condon region photodissociation dynamics have multidimensional character withnine activemodes. The intensity of υ24 mode in methanol is much stronger than that in acetonitrile. Compared with fatty amides and benzamide, phenyl substitution for H atom on-NH2 group makes C=O solvent effects disappear.

结果表明，苯甲酰苯胺的非平面反式结构为最稳定结构；在Frank-Condon区域内，苯甲酰苯胺主要由9个活性振动模组成；其中ν24（苯环上C＝C不对称伸缩振动和CCH的面内弯曲振动，NH面内弯曲振动）振动模在甲醇溶剂中的强度远远大于其在乙腈的强度；与脂肪酰胺类化合物和苯甲酰胺的研究结果比较发现，苯基取代－NH2上的H原子使得C＝O不再具有明显的溶剂效应。

Study on an efficient process for the preparation of trifloxystrobin starting from 2-methylacetophenone bypartial oxidation,esterification,reaction with methoxyamine,bromization and condensation with 3'- acetophenone oxime.

以邻甲基苯乙酮为原料，经过高锰酸钾的碱性氧化，甲醇酯化，再与甲氧基胺盐酸盐肟化后，用N-溴丁二酰亚胺溴化，最后和间三氟甲基苯乙酮肟缩合得到目标产物肟菌酯。

Acetylpyruvic acid methyl ester can be synthesized by the condensation of dimethyl oxalate and acetone in the presence of sodium methoxide.

叙述了在催化剂甲醇钠的存在下，以草酸二甲酯和丙酮为原料合成乙酰丙酮酸甲酯的工艺。

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ，N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

The solvents commonly used in the solvothermal synthesis include alcohols (such as methanol, ethanol, isopropanol, alcohol, ethylene glycol, glycerine, etc.), amines (such as hexamethylenediamine, dimethylformamide, triethanolamine), Acetonitrile and Propionitrile, the differences of functional groups, varieties of kinds together with a wide differences of polarity, dielectric constant and boiling point of organic solvents greatly increase the diversities of the product.

溶剂热合成常用的溶剂有醇类(如甲醇、乙醇、异丙醇、正丁醇、乙二醇、甘油等)，胺类(如己二胺、二甲基甲酰胺、乙醇胺)，乙腈和丙腈等，有机溶剂由于带有不同的官能团，种类繁多，具有不同的极性、介电常数、沸点等，大大增加了合成产物的多样性。

Result: The anticancer active component includes: taxol 9.45%、cephalomanine: 9.63%、10- deacetylbaccatinⅢ: 22.64%、total flavonoids: 19.15%. 3. The preparation of Seiadopitysin control Methods: Take dry Ginkgo leaves and extracted three times by sonication with 95% EtOH, solutions were concentrated under vacuum, after defatting by petroleum benzin, the sample was extracted with EtOAc and the solutions were concentrated under vacuum.

金松双黄酮对照品的制备方法：取干燥银杏叶以95％乙醇超声提取3次，提取液合并，减压浓缩，石油醚脱脂后，用乙酸乙酯萃取，萃取液减压浓缩，经硅胶柱(6cm×80cm)层析，石油醚-乙酸乙酯(9∶1～5∶5)梯度洗脱，产物用甲醇多次冲淋，再以二甲基甲酰氨溶解，反复重结晶，得黄色粉末结晶。

The invention is characterized in that the carrier is produced through the reaction between halogen acetylized crosslinked polystyrene resin and hydroxybenzyl alcohol.

本发明的特征是：该载体由卤乙酰化聚苯乙烯树脂与对羟基苯甲醇反应制得。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。