乙酰氯

Methods The propylbridged biferrocenyl substituted pyridazinone was synthesized by the reaction of propylbridged biferrocene with ethyl succinyl chloride, and then condensed with hydrazine hydrate.

双二茂铁丙烷先与丁二酸单乙酯酰氯发生酰化反应，生成的1，4酮酸酯再与水合肼缩合得到含有双二茂铁丙烷的哒嗪酮衍生物。

P28 紫色 Formation of a peptide bond 肽键形成–4侧链具有的反应–形成二硫键-其它反应 Tyr,His,Arg Review Isoelectric Point Titration滴定 of an amino acid 滴定 Gly幻灯片 18 His Lys Glu Reaction of amino acids Section 4 Protein isolation and purification 蛋白质分离及提纯 Working With Proteins Experimental techniques for protein analysis and characterization Purification steps A cell contains many types of proteins In the lab we want to isolate a single protein for experiments Purification steps We first grow cells or isolate tissues that contain the protein of interest We break open the cells to produce a crude extract Use centrifugation离心 to separate soluble from insoluble material We fractionate 分离 the protein mixture based on properties of such as size, charge affinity or solubility.

丹磺酰氯与氨基酸反应生成荧光性质强和稳定的磺胺衍生物，用于多肽链NH 用于多肽链 3末端氨基酸的标记烃基化反应(1) 2，4-二硝基氟苯2，4-dinitrofluorobenzene，二硝基氟苯(二硝基氟苯 DNFB也叫做试剂。DNFB在弱碱性溶液也叫做Sanger试剂试剂中与氨基酸发生取代反应，生成黄色化合物二硝基二硝基苯基氨基酸(dinitro phenyl amino acid， DNP氨基酸氨基酸)苯基氨基酸氨基酸(2)苯异硫氰酸酯(phenylisothiocyanate， PITC)在弱碱性条件下，与氨基酸反应在弱碱性条件下，生成苯乙内酰硫脲 PTH衍生物，(phenylthiohydantoin， PTH)衍生物，即PTH-氨基酸，此反应又称之Edman反应，该反应是蛋白质或多肽氨基酸序列测定常用的反应。

Enzymatic synthesis of cefaclor from 7\|aminodesacetoxymethyl\|3\|chlorocephalosporanic acid (7\|ACCA) and phenylglycine derivatives using penicillin G acylase was studied.

以7-氨基去乙酰氧甲基-3-氯头孢烷酸(7-ACCA)和苯甘氨酸衍生物为底物，利用青霉素酰化酶酶促合成头孢克罗。

It's soil, however, after its problems, the crop was phytotoxicity very concern, according to chlorine sulfonylurea herbicide easily after long after stubbly maize produced in the problem, residual phytotoxicity chose herbicides security agents Ⅰ compounds, N - methylene chloride acetyl groups - 5-2 - diethyl - propyl arene pbo.

它的土壤残留问题及其对后茬作物的药害影响，一直是人们极为关注的问题，故本文针对除草剂氯磺隆使用后易对后茬玉米产生残留药害的问题，选择了除草剂安全剂化合物Ⅰ：N-二氯乙酰基-5-乙基-2-丙基-1，3-恶唑烷。

In this research, liposoluble chlorogenic laurate was synthesized by acylation with lauroyl chloride in the presence of triethylamine in non-water phase.

本研究对CGA进行了分子修饰，即在非水相中，以三乙胺为催化剂，对其进行月桂酰氯酰化，制备了脂溶性的绿原酸月桂酸酯。

Subsequently,enol methylation of P in basic condition completed the synthesis of malyngamide O.Applied this route to the synthesis of malyngamides Q and R,the chiral unsaturated acid was connected with the vinyl chloride part by amidation,then the resulting product was converted into the corresponding aldehyde,followed by aldol condensation of the aldehyde with the chlorotitanium enolate of pyrrolidone to complete the skeleton of malyngamides Q and R,then the synthesis of them was completed via enol methylation in acid condition.

该合成路线拓展应用到malyngamides Q和R的合成时，首先用酰胺键将手性不饱和脂肪酸和烯氯片段连接，再转化成相应的醛，与乙酰基吡咯酮进行TiCl_4催化的aldol反应即得到malyngamides Q和R的骨架结构，再经过酸催化的烯醇甲基化反应完成了Q和R的全合成。

Taking the method of the indoor bioassay to study the herbicide antidote dichloro-N-acetyl-2-methyl-1-oxa-4-aza-Lo\nonane to reduce herbicide acetochlor on the stubble after the rice crop residues injury.

采用室内生物活性测定的方法，研究了除草剂解毒剂N-二氯乙酰基－2-甲基－1-氧杂－4-氮杂－螺[4.4]壬烷减轻除草剂乙草胺对后茬作物水稻的残留药害。

Two novel pyrazolone derivatives 2-ethylamino-6H-5-(1-phenyl-3-methyl/phenyl-5-pyrazolone-4-ylene)-1,3,4-thiadiazine (PMCP-ETSC/DPCP-ETSC) containing NNS six-membered heterocycles were synthesized by the condensation reaction of 1-phenyl-3-methyl/phenyl-4-chloroacetyl-pyrazolone-5 with 4-ethyithiosemicarbazide. The title compounds were characterized by elemental analysis, IR, 1H NMR, 13C NMR and single-crystal X-ray diffraction.

利用1-苯基－3-甲基／苯基－4-氯乙酰基－吡唑啉酮－5与4-乙基氨基硫脲发生缩合反应，生成了2个新的双杂环化合物2-乙氨基－6H-5-（1-苯基－3-甲基／苯基－5-吡唑啉酮－4-基）－1，3，4-噻二嗪(PMCP-ETSC/DPCP-ETSC)，并对其进行元素分析、红外光谱、核磁共振表征和晶体结构分析。

This reflected that EMP and HMP pathways and the tricarboxylic acid cycle were very important to the bioreduction.

表明糖酵解途径、磷酸戊糖途径和三羧酸循环的顺利进行对于面包酵母在有机介质中催化4-氯乙酰乙酸乙酯还原反应都是十分重要的。

The experimental condition of acetylating method for determining priminary alcohol and secondary alcohol catalyzed by perchloric acid in the medium of analytically pure ethylacetate is proposed.

提出了以高氯酸为催化剂，分析纯乙酸乙酯为介质，乙酰化法测定伯、仲醇的实验条件，实现了对经典方法的改进，简化了操作程

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。