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乙酰基

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A novel method to prepare polyrotaxane in solution by α-cyclodextrins and dumbbell-like poly derivative with reversible acylhydrazone bond and big end stopper (2',4-dinitrophenyl) is described.

合成了具有可逆酰腙键的2,4-二硝基苯甲醛封端的哑铃型聚乙二醇衍生物。

The result of the experiment showed that the qualitative medium - speed filter paper can be used as the material of the nitrite - detecting paper: color developing reagent A containing 4 - aminobenzene sulfonamide and N - 1 naphthyl ethylenediamine hydrochloride, and mixtures of 1 : 1 naphthylamine solution and sulfanilic acid solution as color developing reagent.

实验结果表明:定性中速滤纸可以作为亚硝酸根试纸的材料;含有4-氨基苯磺酰胺和N-1-萘基乙二胺盐酸盐的显色剂A及含有1:1的α-萘胺溶液和对氨基苯磺酸溶液的显色剂B,按1:1混合后可以作为显色剂;通过应用实验表明,亚硝酸根试纸具有体积小、便于携带、检测方便、成本低廉等特点。

Poly(N-isopropylacrylamide-co-2-hydroxyethyl methacrylate)/clay hydrogel was copolymerized with NIPA and HEMA cross-linked by clay to form a new kind of nanocomposite hydrogel P(NIPA-co-HEMA)/clay was obtained.

以无机粘土为交联剂制备了具有温度、pH双重敏感性的聚(N-异丙基丙烯酰胺-co-甲基丙烯酸-β-羟乙酯)/粘土纳米复合水凝胶P(NIPA-co-HEMA/clay,并用红外和X衍射对其结构和形态进行了表征。

With the occurrence of H2/Pd-C and ethyl formic ester,the reduction of the nitro group and the formylation of the amino group could be finished in one step.

但是在甲酸乙酯存在下,用H2/Pd-C对Ⅶ的硝基进行还原,得到的Ⅷ中的氨基可当即被甲酰化,使由Ⅶ到Ⅳ的两步反应一步完成。

The title anti-fogging coating was prepared from film-forming substance such as UV curing of n-butyl methacrylate,β-hydroxy ethyl acrylate,acrylamide and sodium propenyl alkyl ether hydroxyl sulfonate,and proper solvents, crosslinker s,photoinitiators and additives.

以光敏丙烯酸酯低聚物、甲基丙烯酸丁酯、丙烯酸-β-羟乙酯、丙烯酰胺及丙烯基烷醚羟磺酸钠为主要成膜物质,再配以适量的溶剂、交联剂、光敏剂及各种助剂制成UV固化防雾涂料。

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下:首先,以磺胺异噁唑和磺胺二甲嘧啶为模板,分别以4-乙烯基吡啶,甲基丙烯酸,丙烯酰胺为功能单体,以二甲基丙烯酸乙二醇酯为交联剂,偶氮二异丁腈为引发剂,采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

N-(1-Naphthyl)ethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-(1-萘基)乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

N-1-Naphthylethylenediamine dihydrochloride solution was injected into the mixed flow of the water sample and sulfanilamide solution. Red dye formed by the reactions was spectrophotometrically detected at lλmax 540 nm.

将N-1-萘基乙二胺二盐酸盐溶液注入到水样和对氨基苯磺酰胺溶液的混合流,在lλmax 540nm处对反应形成的红色染料进行分光光度检测。

Dendrimers with stearyl groups on the periphery are synthesized by amidation using dendrihmers with NH2 on the periphery and stearyl chloride as raw materials.

以乙二胺和丙烯酸甲酯为原料,甲醇为溶剂,通过Michael加成及酰胺化反应,合成端基为胺基的树枝状大分子。

Ethambutol is a first-line drug used for antituberculosis therapy. It is often used in combination with isoniazid, rifampin, pyrazinamide, and streptomycin. The action of EMB in antituberculosis mechanism is the destruction of cell wall of tubercle bacilli via binding the target molecule -- arabinosyl transferases. These enzymes are involved in the polymerization of the cell wall arabinan. Inhibition of arabinan synthesis by EMB results in the accumulation of mycolic acids, leading to cell death.The EMB-resistance of MTB is involved with the mutation of emb operon or the over expression of emb operon.

乙胺丁醇是和异烟肼、利福平、链霉素、吡嗪酰胺联合治疗结核病的一线抗结核药物,EMB对结核分枝杆菌的作用机制与分枝杆菌胞壁结构破坏有关,主要作用于靶分子阿拉伯糖基转移酶,抑制了阿拉伯糖基聚合入阿拉伯半乳聚糖,从而影响细胞壁分枝菌酸-阿拉伯半乳聚糖-肽聚糖复合物的形成,导致菌细胞的死亡。

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