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Methods The propylbridged biferrocenyl substituted pyridazinone was synthesized by the reaction of propylbridged biferrocene with ethyl succinyl chloride, and then condensed with hydrazine hydrate.

双二茂铁丙烷先与丁二酸单乙酯酰氯发生酰化反应,生成的1,4酮酸酯再与水合肼缩合得到含有双二茂铁丙烷的哒嗪酮衍生物。

Highly selective acylation at C-5 of indole was realized and a new method was established in the synthesis of TIMs.

采用三氟乙酰基作为吲哚C-3的保护基团,在路易酸催化下使吲哚的酰化反应高选择性地发生在5-位。

In this research, liposoluble chlorogenic laurate was synthesized by acylation with lauroyl chloride in the presence of triethylamine in non-water phase.

本研究对CGA进行了分子修饰,即在非水相中,以三乙胺为催化剂,对其进行月桂酰氯酰化,制备了脂溶性的绿原酸月桂酸酯。

Various reaction parameters such as ratio of ethyl acetoacetate to ethylene glycol,catalyst amount,reaction time and water-carrying reagent amount were studied.

讨论了酯醇比、催化剂用量、反应时间、带水剂用量对酯化率的影响。最佳反应条件为:n:n=1:1.8,催化剂用量为乙酰乙酸乙酯质量的2%,带水剂用量为20mL,反应时间3h。

School "of acetaminophen refined the process of acylation of the multimedia simulation design" system.

学院《对乙酰氨基酚的酰化精制过程的多媒体仿真设计》系统开发。

A series of 2-acetylformanilides were prepared,followed by thiolation with Lowesson reagent to afford 2-acetylthioformanilides,which further reacted with Mn3·2H2O in glacial acetic acid under microwave irradiation to afford 2-acetyl benzothiazole s.

合成了一系列的硫代酰胺,研究了它们在微波辐射醋酸锰作用下发生氧化自由基环化反应,成功地合成了一系列2-乙酰基苯并噻唑衍生物,其结构经红外光谱、核磁共振谱和质谱得到了证实

When bromine was used to bromization reaction with 4-acetyl-guaiacol,the product bromide incompletely or super bromide partial,and the selectivity was poor.

使用单质溴与4-乙酰基愈创木酚进行溴化反应时,产物溴化不完全,或者局部过量的溴化,且选择性较差。

Fibrous hydrous zirconia, spinnable hydrous zirconia chelated by acetylacctone and modifiedhydrous zirconia were synthesized from zirconium oxychlorid(ZrOCl_2·8H_2O) and then applied toprepare ZrO_2/PVA electrospinning hybrid fibers, ZrO_2/PVA continuous hybrid fiber and ZrO_2/PVPhybrid microsphere respectively. The chemical structure, properties, microstructure and formationmechanism of the corresponding materials were investigated.

论文以无机盐ZrOCl_2·8H_2O为原料,合成出纤维状的ZrO_2水合物、乙酰丙酮配位的可纺性ZrO_2水合物和正丁醇改性的ZrO_2水合物,分别与PVA和PVP杂化复合,制备出ZrO_2/PVA杂化电纺纤维、ZrO_2/PVP杂化连续纤维和ZrO_2/PVP杂化微球,并对相关材料的组成、结构、性能及形成机理等进行了深入分析和研究。

A series of polys based on pyromellitic dianhydride, biphenylyl tetracarboxylic dianhydride, thiodiphthalic dianhydride bis benzene dianhydride and oxydiphthalic dianhydride were prepared in different solvents.

以所合成的AB_2单体为原料,合成了一系粘度较低、溶解性良好,带端酚羟基、苯甲酰基、乙酰基、氰代苯基和苯酰苯亚胺基的芳香族超支化聚酰亚胺,通过核磁波谱、红外光谱分析和元素分析对其结构进行确证。

Four substances including 2-methyl ethyl acetoacetate and barley straw extract distilled from bulrush as well as cetyl trimethyl ammonium bromide and isothiazo lintone were used for the comparison experiment in inhibiting the growth of Microcystis aeruginosa in various phases. Result showed that inputting chemicals in the lag phase has better effect than in the log phase, and adding in lag phase can effectively inhibit the algae growth. Although feeding allelopathic substance at log phase can lead to certain restraining effect, it cannot result in the effective inhibition of algae growth, which can be well achieved by feeding CTAB and isothiazo lintone below 10mgl/L during log phase.

研究用从芦苇中提取的2-甲基乙酰乙酸乙酯和大麦秸浸出液两种化感物质以及十六烷基溴化钱和异噻唑啉酮等四种药剂对不同生长期的铜绿微囊藻进行了对比抑制试验,结果显示在铜绿微囊藻生长的迟缓期投加试验药剂效果比在对数期投加效果都好,在迟缓期投加四种药剂,都有很好的抑藻效果;在铜绿微囊藻生长的对数期投加化感物质,虽然有一定的抑藻率,但效果较差,而在藻对数期投加10mg/L以下的CTAB和异噻唑啉酮能达到很好的水华抑制效果。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。