乙酰化

For the synthesis of NHC precursors, there are also several routes: condensation of glyoxal, amines and paraformaldehyde; alkylation of imidazole or monosubstituted imidazole with alkyl halide; annulation of ortho esters and 1,2-diamines; ring closure of hydrazines or amides with acetic anhydride; reduction of thiones with Na/K in THF.

关于N-杂环卡宾前体的合成途径主要有：乙二醛、伯胺和多聚甲醛的缩合反应；卤代烷与咪唑及其取代咪唑的烷基化反应；原甲酸酯与1，2-二胺的成环反应；肼或酰胺与酸酐的环化反应；用Na/K对环硫脲化合物的还原反应。

The composing of CPA is: 25% DMSO,17% formamide, 10% propane-1, 2-diol and 6% PEG.

联合玻璃化保护剂的组成为：25％DMSO、17％甲酰胺、10％1，2-丙二醇和6％聚乙二醇。

Past the kitchen, toilet use antibacterial, cleaning agents, basically trimer cyanuric chloride Department of halogenated compounds, the main components and to hydantoin as an active ingredient of two products.

以往厨房、厕所使用的抗菌、洗净剂，基本上是以氯化三聚异氰系化合物为主成分和以卤化乙内酰脲为有效成分的两种制品。

Monochloroethylene carbonate is prepared by chlorination of ethylene carbonate with sulfuryl chioride ,a solution of monochloroethylene carbonate in ethylene carbonate is reacted with triethylamine to give vinylene carbonate.A parameter design method was applied to select the optimum synthesis conditions.63.3％ and 78％ yields superior to the conventional for monochloroethylene carbonate and vinylene carbonate were obtained respectively,and the process was also simplified .

以碳酸乙烯酯为原料，用磺酰氯作为氯化剂生成一氯代碳酸乙烯酯，三乙胺为脱卤化剂在碳酸乙烯酯溶剂中合成碳酸亚乙烯酯，对一氯代碳酸乙烯酯和碳酸亚乙烯酯制备的工艺参数进行优化，收率分别达到63.3％和78％，均超过了传统方法，且简化了工艺，缩短了反应时间，易于工业化生产。

The enzymatic resolution of 1-phenylethylamine by amidation reaction in organic medium was studied.

在有机相中，对酶催化条件下的1-苯基乙胺酰胺化反应进行了研究。

In this chapter, the folate-EDA was covalently connected with heparin- campotothecin by carbodiimide activation to get a folate-heparin-campotothecin conjugate.

以乙二胺作为连接臂，通过酰胺键将氨基化的叶酸与肝素-喜树碱复合物连接起来，制备了一种叶酸偶联的肝素-喜树碱复合物。

The synthesis of the intermediate amidetriazinone was a crucial step in the synthesis of triazinone. Ethyl acetate was used as the initial material then was carried out for five steps hydrazine hydrate, triphosgene, chloroacetone, hydrazine hydrate respectively with the yield of 59.8%.

三嗪酮类化合物的合成关键是中间体氨基三嗪酮，本文以乙酸乙酯为起始原料，经过酯的肼解、成环反应、胺的烷基化、酮和肼的缩合、酰胺的水解五步反应合成中间体氨基三嗪酮，其收率达59.8%。

The new surfactant was synthesized from the main starting materials such as lauric acid, p-cresol, chlorosulphonic acid and ethylene diamine, by 5 classic reactions which are acyl chlorination, esterification, Fries rearrangement, sulfonation and condensation, with total yield of 58%.

作者以十二酸、对甲酚、氯磺酸、乙二胺等为主要原料，共采取了酰氯化、酯化、Fries重排、磺化和缩合等5步经典的单元反应，合成了该表面活性剂，总收率为58％，并探讨了各步反应的条件对收率的影响。

A series of ABEPS were synthesized from long chain fatty acids, benzene, polyglycol and 1, 3-propane sultone by the procedure of Friedel-Crafts acylation, Huang-Minlon reduction, Williamson and sulfonation reaction, and these compounds had never been reported in the past time.

以长链羧酸、苯、多缩乙二醇和丙烷磺内酯为初始原料，依次经Friedel-Crafts酰基化反应、Huang-Minlon还原、Blank反应、Williamson成醚以及磺化反应等过程，合成了系列未见报道的ABEPS。

Occasionally, we observed the four-component iodoamination of 1, 2-allenyl selenides with I〓 in MeCN at room temperature.

我们还发现1，2-联烯基硒醚在无水乙腈中可以与碘发生碘胺化反应生成酰胺，在此反应中溶剂乙腈参与了反应。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。