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乙酰乙酸酯

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Replacement of one benzimidazole fragment with benzothiazole or benzoxazole and optimization of the structure to create the new frame of the compounds were also carried out with the exception to find more potent compounds. The purpose of design and synthesis of these compounds is to investigate the QSAR of this class of compounds with the inhibition of HCV NS3/NS4A protease and eventually to develop more potent inhibitors.

本文首次采用了丙二酰胺与邻芳二胺在微波辐射下制备对称性双芳并唑甲烷化合物、用芳并唑-2-乙酸乙酯与邻芳二胺在微波辐射下制备非对称性双芳并唑甲烷化合物、用4-取代噻唑-2-乙酸乙酯与邻芳二胺在微波辐射下制备非对称性(4-取代-噻唑-2-基)(1H-芳并咪唑-2-基)甲烷化合物等合成路线,共合成了48个目标化合物,其中41个为新化合物,用~1HNMR,ESI-MS,FT-IR,元素分析对这些化合物进行了全面表征,确定了这些化合物的结构,并对部分化合物进行了~(13)CNMR分析。

Ethyl phenoxyacetate has been synthesised by the reaction of phenol with ethyl chloroacetate under the condition of solid-liquid phase transfer catalysis using PEG-400 as the catalyst.

于固一液相转移催化条件下,以PEG-400为催化剂,通过苯酚与氯乙酸乙酯反应合成了苯氧基乙酸乙酯。与85%的水合肼作用得到相应的酰肼。

Trans-3-phenylglycidate ethyl ester was prepared from benzaldehyde and ethyl chloroacetate through Darzens condensation reaction.

以苯甲醛和氯乙酸乙酯为原料,经Darzens 缩合反应合成了反式-3-苯基缩水甘油酸乙酯,然后在25℃以氨水开环得赤型-3-苯基异丝氨酰胺。

In order to investigate the mechanism for this reac-tion, methyl α-bromoacetate or ethyl α-bromoacetate as starting material was added to the solution of phenyl selenoamide in ethanol in 1∶1 or 2∶1 molar ratio under the neutral condition at room temperature. The results indicated that the same product bis or bis diselenide was formed. Byproduct ethyl benzoate was also separated.

为了研究该反应机理,选择α-溴代乙酸甲酯或α-溴代乙酸乙酯在无催化剂、中性条件下,乙醇溶液中与苯基硒代酰胺室温下反应,投料比为1∶1和2∶1,结果也都生成了同一类产物二甲氧羰基甲基二硒醚或二乙氧羰基甲基二硒醚,同时还分离得到了相应的副产物苯甲酸乙酯。

In order to investigate the mechanism for this reaction, methyl α-bromoacetate or ethyl α-bromoacetate as starting material was added to the solution of phenyl selenoamide in ethanol in 1:1 or 2:1 molar ratio under the neutral condition at room temperature. The results indicated that the same product bis or bis diselenide was formed. Byproduct ethyl benzoate was also separated.

为了研究该反应机理,选择α-溴代乙酸甲酯或α-溴代乙酸乙酯在无催化剂、中性条件下,乙醇溶液中与苯基硒代酰胺室温下反应,投料比为1:1和2:1,结果也都生成了同一类产物二甲氧羰基甲基二硒醚或二乙氧羰基甲基二硒醚,同时还分离得到了相应的副产物苯甲酸乙酯。

Water, Sodium Laureth Sulfate, Cocamidopropyl Betaine, Cocamide MEA, Disodium Cocamphodiacetate, Sodium Lauryl Sulfate, PEG 40 Hydrogenated Castor Oil, Perfume, Sodium Chloride, Propylene Glycol, Quaternium 80, Methylparaben, Polyquaternium 10, Hydroxypropyl Guar Hydroxpropyltrimonium Chloride, Citric Acid, Diazolidinyl Urea, Tetrasodium EDTA, Polyquaternium 7, Propylparaben, Sodium Hydroxide, Panthenol, Persea Gratissima Oil, Penta Sodium Pentetate, Hedera Helix Extract, Bambusa Vulgaris Extract

水,月桂醇聚醚硫酸酯钠,椰油酰胺丙基甜菜碱,椰油酰胺MEA,椰油酰两性基二乙酸二钠,月桂醇硫酸酯钠,PEG 40 氢化篦麻油,香料,氯化钠,丙二醇,季铵盐-80,苯甲酸甲脂,聚季铵盐-10,羟丙基瓜尔胶羟丙基三甲基氯化铵,柠檬酸,重氮烷基咪唑脲,乙二氨四醋酸四钠,聚季铵盐-7,对羟基苯甲酸丙酯,氢氧化钠,泛酰醇,酪梨油,喷替酸五钠,常春藤萃取物,银竹萃取物。

Ingredients: Water,Lauric Acid,Myristic Acid,Stearic Acid,Propylene Glocol,Potassium Hydroxide,Cocamidopropyl Betaine,Starch Hydroxypropyltrimnium Chloride,Sodium Laureth Sulfate,Glycol Distearate,Lavandula Angustifolia Oil,Creatine,Tetrasodium Edta,Perfume,Dmdm Hydantoin.

成分: 去离子水,月桂酸,肉豆蔻酸,硬脂酸,丙二醇,氢氧化钾,椰油酰胺丙基甜菜碱,淀粉羟丙基三甲基氯化铵,月桂醇聚醚硫酸钠,乙二醇双硬脂酸酯,薰衣草精油,肌酸,乙二胺四乙酸四钠,香精,DMDM 乙内酰脲。

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果:从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物,分别为绿原酸甲酯,5-O-咖啡酰基-奎宁酸丁酯,奎宁酸丁酯,5-羟甲基-2-糠醛,三十烷酸,-表儿茶素,7,8-二羟基香豆素,3,4-二羟基苯甲酸乙酯,原儿茶酸。

Result: The anticancer active component includes: taxol 9.45%、cephalomanine: 9.63%、10- deacetylbaccatinⅢ: 22.64%、total flavonoids: 19.15%. 3. The preparation of Seiadopitysin control Methods: Take dry Ginkgo leaves and extracted three times by sonication with 95% EtOH, solutions were concentrated under vacuum, after defatting by petroleum benzin, the sample was extracted with EtOAc and the solutions were concentrated under vacuum.

金松双黄酮对照品的制备方法:取干燥银杏叶以95%乙醇超声提取3次,提取液合并,减压浓缩,石油醚脱脂后,用乙酸乙酯萃取,萃取液减压浓缩,经硅胶柱(6cm×80cm)层析,石油醚-乙酸乙酯(9∶1~5∶5)梯度洗脱,产物用甲醇多次冲淋,再以二甲基甲酰氨溶解,反复重结晶,得黄色粉末结晶。

The extracts from evening primrose flower could significantly enhance the cellular immune function in immunosuppressed mice. Effects of ethylacetate extract was better than those of water extract.

月见草花乙酸乙酯提取物和水提取物均可明显增强环磷酰胺免疫抑制小鼠的细胞免疫功能,其中乙酸乙酯提取物的作用优于水提取物。

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The objective is to subjugate and discourage the people, because that allows the elite to continue to rule unopposed.

其目的是压制和打击人民的积极性,因为这可以让实权派继续统治不会沦为反对派。

GOD,this is the second time you vanquished me!

天啊,这是第二次你打败了我!

So a kind of strong antagonism permeated in the relations of two countries.

所以两国这一时期的政治关系始终弥漫着一种强烈的对抗情绪。