乙酰乙酸酯

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。

In this paper the study on optimizing the esterification of cellulose and some character of CAB(the degree of substitution of cellulose, solubility, the thermal properties and molecular weight) was discussed. The mechanism of the esterification of cellulose in butyric acid/ acetic acid/ butyric anhydride which comprises the creation of the acetic butyric anhydride, acetyl cation and butyryl cation was investigated by the study of the effect of the content of the organic acid and anhydride on the degree of acetyl and butyryl substitution of cellulose.

最后本文根据纤维素在丁酸/乙酸/丁酸酐中的酯化反应中有机酸以及酸酐的添加量对最后产物纤维素醋酸丁酸酯中乙酯或者丁酯取代度的影响，提出纤维素在丁酸/乙酸/丁酸酐中的酯化反应经历一个混和酸酐以及乙酰碳正离子、丁酰碳正离子的生成过程。

AIM: To investigate the effect of PD98059, a specific repressor of extracellular signal regulated kinase1/2 (ERK1/2), on the proliferation of the murine lymphocytes. METHODS: Lymphocytes were isolated from lymphoid nodes of BALB/c mouse. After stained with carboxy fluorescein diacetate, succinimidyl ester, the cells were stimulated with polyclonal activators, concanavalin and phorbol 12,13 dibutyrate plus ionomycin.

分离小鼠淋巴结细胞，藉羧基荧光素乙酰乙酸染色，用多克隆刺激剂刀豆A蛋白或者佛波醇酯加离子霉素刺激，以流式细胞术分析PD98059对淋巴细胞增殖的影响；利用碘化丙锭染色分析PD98059对细胞周期的影响。

The synthesis of sucrose ester containing ethanoyl and oleoyl was performed by transesterification between sucrose octaacetate and ethyi oleate in organic solvents, using lipases Novo435 as the catalyst.

在有机溶剂中，以脂肪酶Novo435为催化剂，蔗糖八乙酸酯与油酸乙酯通过转酯化反应合成了同时含有油酸酰基和乙酸酰基的混合型蔗糖酯，当蔗糖八乙酸酯与油酸乙酯的物质的量之比为1：1时，油酸乙酯的转化率达95％。

Cefixime open side chain acid was prepared by oximation,etherification,chlorination,ester decomposition using t-butyl acetoacetate as starting material.

以乙酰乙酸叔丁酯为原料，经过肟化、醚化、氯代酯解反应合成了头孢克肟开环侧链酸。

Alumina sols of different content were prepared by using Al3 as precusor, water as solvent, nitric acid as peptizer, ethylacetoacetate and polyvinylpyrrolidone as modified menstruum. We used dip-coating method and spin-coating method prepared of alumina films on the plane glass and used dip-coating method and rising liquid method inside the wall of the fiber.

以仲丁醇铝为前驱物、水为溶剂、硝酸为胶溶剂、同时加入乙酰乙酸乙酯和聚乙烯吡咯烷酮作为改性剂制备了不同浓度的氧化铝溶胶用提拉法和旋覆法在平板玻璃上镀膜，同时用提拉法和液面上升法在石英毛细管内壁上镀膜。

This reflected that EMP and HMP pathways and the tricarboxylic acid cycle were very important to the bioreduction.

表明糖酵解途径、磷酸戊糖途径和三羧酸循环的顺利进行对于面包酵母在有机介质中催化4-氯乙酰乙酸乙酯还原反应都是十分重要的。

Four substances including 2-methyl ethyl acetoacetate and barley straw extract distilled from bulrush as well as cetyl trimethyl ammonium bromide and isothiazo lintone were used for the comparison experiment in inhibiting the growth of Microcystis aeruginosa in various phases. Result showed that inputting chemicals in the lag phase has better effect than in the log phase, and adding in lag phase can effectively inhibit the algae growth. Although feeding allelopathic substance at log phase can lead to certain restraining effect, it cannot result in the effective inhibition of algae growth, which can be well achieved by feeding CTAB and isothiazo lintone below 10mgl/L during log phase.

研究用从芦苇中提取的2-甲基乙酰乙酸乙酯和大麦秸浸出液两种化感物质以及十六烷基溴化钱和异噻唑啉酮等四种药剂对不同生长期的铜绿微囊藻进行了对比抑制试验，结果显示在铜绿微囊藻生长的迟缓期投加试验药剂效果比在对数期投加效果都好，在迟缓期投加四种药剂，都有很好的抑藻效果；在铜绿微囊藻生长的对数期投加化感物质，虽然有一定的抑藻率，但效果较差，而在藻对数期投加10mg/L以下的CTAB和异噻唑啉酮能达到很好的水华抑制效果。

7-Hydroxy-4-methylcoumarin was synthesized from ethyl acetoacetate and m-dihydroxybenzene by the Pechmann condensation using phenyl sulfonic acid as catalyst under solvent-free conditions.

摘 要：以苯磺酸作催化剂，乙酰乙酸乙酯和间苯二酚为原料，通过Pechmann缩合反应合成7-羟基-4-甲基香豆素。

Synthesis 3,5-dihydroxytoluene by ethyl acetoacetate and diketene as material(yield 6%),by 3-methyl-4-chlorophenol and KOH as material(yield 30-40%)respectively,It was solved for product separation and purify.

分别以乙酰乙酸乙酯与双乙烯酮为原料(收率6%)、3-甲基-4-氯苯酚与氢氧化钾为原料(收率30-40%)合成了3，5-二羟基甲苯，解决了产品分离纯化问题。3-甲基-4-氯苯酚路线进行了中试，中试收率为20%。

The objective is to subjugate and discourage the people, because that allows the elite to continue to rule unopposed.

其目的是压制和打击人民的积极性，因为这可以让实权派继续统治不会沦为反对派。

GOD,this is the second time you vanquished me!

天啊，这是第二次你打败了我！