乙酰乙酸乙酯

Two compounds were isolated from ethyl acetate extract of the fermentation of fungus 07-11,which obtained from the soil of Yunnan Province. They were identified as N-(4-hydroxy-2-methoxyphenyl)acetamide (1) and ergosta-7,22-diene-3,6-dione (2) respectively on the basis of spectral analyses and physical and chemical identifications.

从云南土壤真菌07-11号菌株的发酵液乙酸乙酯萃取物中分离得到2个化合物，通过理化鉴别和光谱测定，鉴定两化合物分别为N-(4-羟基-2-甲氧苯基)乙酰胺(1)和麦角甾7，22-二烯-3，6-二酮(2)。

Seven compounds have been isolated from hard coral Acropora pulchra. These compounds are:pentadecoic acid, heptadecyl ester;(2)n-cetanol;(3)batyl alcohol;(4) N- [ 1 --2-hydroxyl--3,7-heptad-ecadienal] -hexadecanamide;(5)1 -0-hexanoyl-glycerol ester;(6)thymine;(7)uracil. Their structures were determined by IR, MS, HNMR, 13CNMR analysis.

从北海佳丽鹿角珊瑚Acropora pulchra乙醇提取液的乙酸乙酯部分分离出七个化合物，经IR、MS、~1HNMR、~(13)CNMR等波谱方法鉴定，其结构分别为：(1)十五酸十七酯，(2)正十六碳醇，(3)鲨肝醇，(4)N-1-羟基甲基-2-羟基—-3，7-十七碳二烯基十六酸酰胺，(5)1-正十六酸甘油酯，(6)胸腺嘧啶，(7)尿嘧啶。

From Cacalia deltophylla (collected from Luqu County, Gansu Province), 22 compounds were isolated, of which 15 compounds have been identified. Among them, two compounds are new. They are named as 3-methyl-4-hydro-8-acetyl-furanonaphth-9-one and 1hydroxy-2-methoxy-3-acetyl-4, 8-dimethyl-5, 8-dihydro-naphthalene.

从采自甘肃省碌曲县的三角叶蟹甲草全草的甲醇提取物的石油醚部分和乙酸乙酯部分中，采用同样方法分离得到22个化合物，鉴定了其中的15个化合物，其中有2个为新化合物，分别命名为3-甲基-4-氢-8-乙酰基-呋喃萘-9-酮（2）和1-羟基-2-甲氧基-3-乙酰基-4，8-二甲基-5，8-二氢-萘（3）。

Trans-3-phenylglycidate ethyl ester was prepared from benzaldehyde and ethyl chloroacetate through Darzens condensation reaction.

以苯甲醛和氯乙酸乙酯为原料，经Darzens 缩合反应合成了反式-3-苯基缩水甘油酸乙酯，然后在25℃以氨水开环得赤型-3-苯基异丝氨酰胺。

Chapter 3: Synthesis of 2-aroyl-l,3,5-triaryl-4-carbethoxy-4-cyanocyclohexanols from chalcones with ethyl cyanoacetate is carried out in excellent yields with KF/basic alumina as catalyst under ultrasound irradiation.

第三章：研究了超声辐射下，以碱性氧化铝固载氟化钾为催化剂，利用查耳酮和氰乙酸乙酯合成2-芳酰基-1，3，5-三芳基-4-乙酯基-4-氰基环己醇。

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果：从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物，分别为绿原酸甲酯，5-O-咖啡酰基－奎宁酸丁酯，奎宁酸丁酯，5-羟甲基－2-糠醛，三十烷酸，-表儿茶素，7，8-二羟基香豆素，3，4-二羟基苯甲酸乙酯，原儿茶酸。

The solubility of the novel polyamides are greatly improved compared with the conventional aramids, especially the polyamide with dendritic blocks of the second genernation as side chains are soluble in most of the common organic solvents such as ether, ethyl acetate, chloroform, acetone, tetrahydrafuran etc.

树状片段的引入大大地改善了聚酰胺的溶解性，特别是以第二代树状片段为侧基的聚酰胺的溶解性得到了很大的改进，可以溶于大部分常见的有机溶剂，如乙醚、乙酸乙酯、氯仿、丙酮、四氢呋喃等。

In view of the existence of the above shortcomings of traditional methods, using acetyl chloride instead of acetic acid as a raw material, do not use any catalyst, not heating, room temperature reaction synthesis of ethyl acetate.

鉴于传统方法存在以上缺点，采用乙酰氯代替乙酸作为原料，不使用任何催化剂，不加热，常温反应来合成乙酸乙酯。

Treatment of sucrose alkyl 4,6-orthoacetate hexaacetates I with water or alcohol in the presence of an acid catalyst afforded derivatives of sucrose acetates by selectively blocking specific hydroxyl group in sucrose and acetyl migration.

4，6-原乙酸蔗糖六乙酸酯在酸催化下水解和醇解，选择性地保护了蔗糖分子中的某些羟基，并通过乙酰基由C~4→C~6迁移的异构化反应合成了一系列蔗糖乙酸酯。

In this thesis, the design, synthesis and application of substituted 1,8-naphthalimides and napthopyrones conjugated with uridine, substituted 1,3,5-triazine, 1,2-dibromoethane, ethyl bromoacetate have been studied.

本论文研究了取代l，8-萘酰亚胺和萘并吡喃酮与尿苷、取代均三嗪、二溴乙烷、溴乙酸乙酯偶合和双l，8-萘酰亚胺之间偶合的设计、合成及应用。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。