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乙酰乙酸

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With 1,4-bezenoquinone and ethyl acetoacetate as the starting materials, it had been prepared in a novel six-step procedure in overall yield of 34.6%.

以1,4-苯醌和乙酰乙酸乙酯为起始原料,经新的六步反应过程,合成阿比朵尔,总收率为34.6%。

KF/NaZnPO4 was used as the catalyst for Michael addition reaction of ethyl acetoacetate and acrylonitrile.

以磷酸锌钠负载KF为催化剂,催化乙酰乙酸乙酯与丙烯腈进行Michael 加成反应。

Various reaction parameters such as ratio of ethyl acetoacetate to ethylene glycol,catalyst amount,reaction time and water-carrying reagent amount were studied.

讨论了酯醇比、催化剂用量、反应时间、带水剂用量对酯化率的影响。最佳反应条件为:n:n=1:1.8,催化剂用量为乙酰乙酸乙酯质量的2%,带水剂用量为20mL,反应时间3h。

A series of methyl 2,7,7-trimethyl-5-oxo-4-aryl1,4,5,6,7,8- hexahydroquinoline -3-carboxylate were synthesized by the reaction of aromatic aldehydes,dimedone and methyl acetoacetate using ammonium acetate as catalyst in glycol under microwave irradiation with 82%~98% yields in 4~6 min.

微波辐射下以芳醛、达咪酮、乙酰乙酸甲酯为原料,乙二醇为溶剂,醋酸铵为催化剂合成了一系列2,7,7-三甲基-5-氧代-4-芳基-1,4,5,6,7,8-六氢喹啉-3-羧酸甲酯化合物,反应时间4~6 min,产率82%~98%。

_6P_2W_(17)VO_(62) catalyst was prepared and characterized by FTIR,and synthesis of fraistone over as-synthesized catalyst from ethyl acetoacetate and 1,2-propylene glycol was investigated.

制备了Dawson型磷钨钒酸铵催化剂,用FT-IR分析方法对催化剂进行了结构表征,并以乙酰乙酸乙酯与1,2-丙二醇为原料催化合成了苹果酯-B。

The synthesis of celery ketone from butyl aldehyde and ethyl acetoacetate was improved with higher yield by using solid superbase(K2O/γ-Al2O3) for the first time.

在正丁醛和乙酰乙酸乙酯为原料合成芹菜酮的合成过程中,对其催化方法进行改进。

The influence of reed produced allelopathy material eathyl-2-methyl acetoacetate on respiration action, photosynthesis action and antioxidant enzymes system of Microcystis aeroginosa were studied.

研究了芦苇产生的化感物质2-甲基乙酰乙酸乙酯对铜绿微囊藻呼吸作用、光合作用和抗氧化酶体系的影响。

Supported 12-Phosphotungstic Acid and Its Salts as Catalysts for the Synthesis of Fructone and Fructone-B;2. Their catalytic activities were measured by synthesis of fructone-B from ethyl acetoacetate and 1,2-propanediol.

制备了一系列以脱铝超稳Y沸石为载体的磷钨酸及其铯盐催化剂,考察了催化剂在以乙酰乙酸乙酯和1,2-丙二醇为原料催化合成草莓酯反应过程中的性能。

The method was proved to be simple,rapid,practical and highly sensitive.It is an efficient method for the quality control of acetoacetic ester.

本法简便,快速、实用,灵敏度高,可有效地用于乙酰乙酸乙酯的质量控制。

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.

摘要] 目的:用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。

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