乙酰丙

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下：首先，以磺胺异噁唑和磺胺二甲嘧啶为模板，分别以4-乙烯基吡啶，甲基丙烯酸，丙烯酰胺为功能单体，以二甲基丙烯酸乙二醇酯为交联剂，偶氮二异丁腈为引发剂，采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

Ingredients: water,decyl glucoside,glycerin,sodium cocoamphodiacetate,sodium pca,polysorbate-20,cocamidopropyl betaine,carya illinoensis powder,panthenol,carbomer,aloe barbadensis leaf juice,lavandula angustifolia oil,perfume,tetrasodium edta,lactic acid.

主要成份：去离子水，葵基葡聚糖，甘油，椰油两性二醋酸二钠，吡咯烷酮羧酸钠，聚山梨醇酯-20 ，椰油酰胺丙基甜菜碱，核桃粉，泛醇，卡波姆，芦荟叶萃取物，薰衣草精油，香精，乙二胺四乙酸四钠，乳酸。

Dipropyl ether will be recovered in the distillate using 1-pentanol.

使用1-戊醇。N.N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收。

The formation of charge transfer complex was studied in the first part. The second part includes the synthesis and characterization of the acrylated unsaturated polyester and the kinetic studies on the Ar-UPE/ triethylene divinyl ether (DVE-3) photocuring system, the rheology and properties of film after photocuring. The third part includes the synthesis and characterization of the urethane modified unsaturated polyester and the kinetic studies on the PU-UPE/DVE-3 photocuring system, the rheology and properties of film after photocuring. The fourth part includes the synthesis and characterization of the vinyl ether end capped polyurethane and the kinetic studies on the VE-PU/DVE3 photocuring system, the rheology and properties of film after photocuring.

整个研究工作分为四个部分：一是电荷转移复合物的研究；二是丙烯酰氧基化不饱和聚酯的合成，表征，Ar-UPE/二缩乙二醇二乙烯基醚（DVE-3）体系光固化动力学研究以及Ar-UPE/DVE-3体系流变性能和光固化后涂膜综合性能的研究；三是氨酯改性的不饱和聚酯的合成，表征，PU-UPE/DVE-3体系光固化动力学研究以及该体系光固化后涂膜综合性能的研究；四是乙烯基醚封端的聚氨酯的合成，表征，VE-PU/马来酸二甲酯体系光固化动力学研究以及VE-PU/DMA体系流变性能和光固化后涂膜综合性能的研究。

A SPE procedure was suggested for extracting and concentrating fisetin by using different volume fractions of ethanol in aqueous solution as the loading conditions.

分别以中药黄栌的主要成分非瑟酮为印迹分子、丙烯酰胺为功能单体及乙二醇二甲基丙烯酸酯为交联剂，通过封管聚合法合成了分子印迹聚合物；将其装于自制的固相萃取柱中，研究了以不同体积比的乙醇-水溶液为溶剂时非瑟酮在柱上的保留行为；通过优化清洗及洗脱条件，使非瑟酮与它的结构相似物槲皮素在柱上得到了很好的分离。

A key intermediate of abacavir, named N-(2-amino-4,6-dichloro-5-pyrimidinyl) formamide was synthesized from diethyl malonate and guanidine hydrochloride. This method suits to industry for large scale. The materials are easy to get and very cheap.

2-氨基-4，6-二氯-5-甲酰氨基嘧啶是合成阿巴卡韦的关键中间体，本文拟以丙二酸二乙酯和盐酸胍为起始原料合成这一关键中间体，具有原料来源广，适合大规模生产等优点。

We researched the high molecular polyether,polyamide hot melt adhesive, 2-phenoxy ethanol phenyl cellosolve,propylene glycol phenylate,etc,which have passed appraisal of the provincial science and technology achievement.the company gains higher economy profit after putting into production.

公司设有专业科研机构从事新产品的开发研制工作。先后研制开发成高分子聚醚，聚酰胺热熔胶，乙二醇苯醚，丙二醇苯醚等十多项新产品，均通过省级科技成果鉴定。

Selecting acrylic acid、acrylamide and 2 propenoic acid 2 hydroxyethyl ester as the monomers of copolymerization,a water absorbent resin used for condensing protein solution has been synthesized by means of water solution polymerization.

以丙烯酸、丙烯酰胺及丙烯酸羟乙酯等为单体合成了浓缩蛋白质溶液用吸水树脂，其最大浓缩倍率可达 4。

In chapter four, molecular imprinting polymers against amino acid derivatives utilizing 2-VP+AM as combined functional monomer and trimethylolpropane trimethacrylate as tribasic cross-linker were prepared and result was compared with those with the same amino acid derivative as the imprinted molecules utilizing ethyleneglycol dimethacrylate as dibasic cross-linker. It was found that cross-link intensity of the molecular imprinting polymer is higher when TRIM was utilized and baseline separation for the imprinted molecule could be achieved. When TRIM was utilized as cross-linker more molecule is imprinted during the polymerization.

第四章采用2-乙烯基吡啶+丙烯酰胺复合功能单体，考察了三元交联剂三甲氧基丙烷三甲基丙烯酸酯烙印氨基酸衍生物的情况，并与二元交联剂乙二醇二甲基丙烯酸酯烙印相同氨基酸衍生物的情况进行了对比，发现三甲氧基丙烷三甲基丙烯酸酯交联剂在较小的用量下就可使分子烙印聚合物达到足够的交联度，实现烙印分子的基线分离。

In this thesis, a novel polymerizable cation amphiphilic compound, 4-2-(acryloyloxy ethoxy benzyl tri-ethyl ammonium bromide, was synthesized.

本论文合成了一种新型可聚合两亲化合物4-2-(丙烯酰氧基乙氧基苯亚甲基三乙基溴化铵。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。