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This result indicated that the best way to purify soybean agglutinin was GalNac-epoxy-Sepharose 6B.

这一结果表明大豆凝集素最理想的纯化方法是N-乙酰基-D-半乳糖胺-expoxy-sepharose 6B亲和层析体系。

Alkalimetry is standard method of determining degree of deacetylation of chitosan generally applied in aquaculture and other industry.

碱量法是水产行业测定壳聚糖脱乙酰度的标准方法,应用广泛。

In this paper, we have studied different types of indicators which can be used in alkalimetry, the results suggested that helianthine-triphenylrosaniline (1:1) mixed indicator can instruct color changes of titration end significantly, the accuracy and reproducible are good.

研究了用于碱量法测定的不同种类指示剂,结果表明:甲基橙-亚甲基蓝(1:1)混合指示剂终点颜色变化明显,准确性和重现性好,可以作为测定壳聚糖不同脱乙酰度的通用指示剂,解决了目前碱量法存在的通用性和毒害问题。

In this dissertation, the stable radical cation salts ofphenothiazine and 10 - alkylphenothiazine alky=〓(〓 hexachloroantimonate,perchlorate and iodide were prepared by one- electron oxidationwith 2,2,6,6-tetramethyl - 4 -acetyloxypiperidine oxoammoniumhexachloroantimonate, perchloric acid/hydrogen peroxide andmolecular iodine respectively, and they were characteried by UV -Vis spectroscopy and ESR spectroscopy.

本文的主要内容有:吩噻嗪和10-烃基吩噻嗪分别被碘、高氯酸/过氧化氢,2,2,6,6-四甲基-4-乙酰氧基哌啶氧铵六氯锑酸盐氧化为相应的正离子自由基碘盐、高氯酸盐、六氯锑酸盐,并用UV-Vis光谱和ESR波谱进行了鉴定和研究。

After acetylation of cellulose, the allomorph of CTA changed and the crystallinity decreased; however, amorphism is dominant in CDA obtained by hydrolysis from CTA and spinning resulted in the reduction of crystallinity in CDA.

纤维素乙酰化后形成CTA,其晶型发生变化,结晶度降低;而CTA水解后得到的CDA,无定形占明显优势,纺丝过程中的取向又会进一步降低CDA的结晶度。

Hyaluronic acid is a linear polysaccharide chain composed of alternating β-1,4-glucuronic acid and β-1,3-N-acetylglucosamine moieties.

透明质酸(Hyaluronan, HA)是由葡萄糖醛酸和N-乙酰氨基葡萄糖为双糖单位交替连接而成的粘多糖物质。

In the part of producing TONALIDE, through single-factor-experiments , the highest yield of reaction condition was confirmed as: reaction time about 4 hours; reaction temperature about 20 ; the quantity of chlori-acytyl about 10g; the quantity of aluminum chloride 13-15g and the yield of reaction was as high as 90%.

在TONALIDE的合成部分,通过单因素试验,找到了反应收率最高的反应条件为:反应时间4小时左右;反应温度20℃左右;乙酰氯的用量10g左右;反应中的三氯化铝的用量13~15g,此时反应收率可达90%。

Amino desacetoxycephalosporanic acid (7 - ADCA) is an ampholyte.

7-氨基去乙酰氧基头孢霉烷酸是两性化合物,从等电点两侧改变溶液的 p H值都可以产生过饱和度并结晶得到晶体产品,本文对 7-ADCA两种方法结晶的初级成核过程进行了研究。

The yield of the 3, 4-dihydropyrimidine-2(1H)-one was up to 95.4% under mole ratio of anisaldehyde, methyl acetoactate and urea is 1:2:5, ion-exchange membrane is 3 g, ethyl alcohol as solvent and refluxing for 2 h.

当对羟基苯甲醛、乙酰乙酸甲酯与脲的摩尔比为1:2:5,乙醇作溶剂,3 g离子交换膜,回流2 h,产物收率达95.4%。

Methoxycarbonyl-4-(4-methoxyphenyl )-6-methyl-3, 4-dihydropyrimidine-2(1H)-one was synthesized from anisaldehyde, methyl acetoactate and urea in presence of HF-1O1 strong acidic ion-exchange membrane.

在HF-101强酸性离子交换膜的存在下,由对羟基苯甲醛、乙酰乙酸甲酯与脲一步合成了5-甲氧羰基-4-(4-甲氧苯基)-6-甲基-3,4-二氢嘧啶-2(1H)-酮。

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