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The optimal carrier gas velocity of prepared SE-30 series capillary chromatographic columns was studied and used to separate isomeric compounds. The efficiency of SE-30 capillary chromatographic columns has been studied with different diameters, film thicknesses and oven temperatures, using n-do-decane, phenol, aminobenzene, and butyl acetate as test samples.

研究自制的SE-30系列毛细管气相色谱柱的载气最佳线速度,并应用于同分异构体的色谱分离分别用十二烷、苯酚、苯胺、醋酸丁酯作试祥在不同载气线速条件下对不同口径、不同膜厚、不同柱温的SE-30毛细管色谱柱的柱效进行考察,并在最佳线速度条件下分离异戊醇、硝基氯苯、硝基甲苯及二乙苯同分异构体体系。

Methods: A model to evaluate lymphocyte proliferation stimulated with a polyclonal activator, concanavalin A, was established by vital dye carboxyl fluorescin diacetate succinmidyl ester labeling technique. Effects of the different doses of anisomycin on the lymphocyte proliferation were estimated by flow cytometry and MTT methods. The propidium iodide labeling technique was applied to assay the effect of the different doses of anisomycin on changes of the lymphocyte cell-cycle stimulated by ConA or by phorbol ester plus Ionomycin. The percentage of the expression level of CD69 and CD25 on the activated lymphocytes was evaluated by fluorescin-conjugated monoclonal antibody double labeling technique.

以活体染料羧基荧光素乙酰乙酸琥珀酰亚胺酯染色,建立在多克隆刺激剂刀豆蛋白A刺激下评价小鼠淋巴细胞增殖的模型,通过流式细胞术和MTT法分析茴香霉素在不同剂量下对淋巴细胞增殖的作用;采用碘化丙锭染色分析茴香霉素对ConA或佛波醇酯加离子霉素刺激的小鼠淋巴细胞周期变化的作用;利用荧光标记的单克隆抗体双染技术和流式细胞术观察茴香霉素对小鼠CD3~+T细胞早期及中期活化标志分子CD69和CD25表达的影响。

Specific drug–polymer interactions are engineered by optimizing the lactide to glycolide ratio and including specific polymer end groups.

通过优化丙交酯与乙交酯比例及加入特殊的聚合物末端基来获得特殊的药物-聚合物间相互作用。

Then two star-shaped oligomers with designed molecular weights 5000 g mol-1 and 10000 g mol-1, respectively, were synthesized from D, L-lactide and glycolide as raw materials and pentaerythritol as initiator under catalysis of dibutyltin oxide.

以合成的丙交酯和乙交酯为原料,季戊四醇为引发剂,氧化二丁基锡为催化剂合成出设计分子量为5000和10000两种预聚物。

Such structural complexity is further enhanced by O-acetylation, esterification, lactonization, as well as other forms of substitutions, reflecting significance of carbohydrates in cell recognition.

细胞表面上糖缀合物的糖链经常以多/寡聚体形式存在,并且结构复杂,常常大量表达唾液酸、糖醛酸、硫酸化糖基等酸性糖,并发生O-乙酰化、酯化和内酯化等修饰。

The amphiphilic copolymer poly (MAA-SMA-PEGMA) was synthesized by the conventional free-radical copolymerization of methacrylic acid, stearyl acryate and poly methacrylate monomers.

利用功能性单体甲基丙烯酸、甲基丙烯酸十八烷基酯和聚乙二醇甲基丙烯酸酯通过常规自由基无规共聚反应,合成了两亲性共聚物Poly(MAA-SMA-PEGMA)。

Compounds were identified by NMR etc, and they are veraflorizine 1, ebeinone 2, verticinone 3, isoverticine 4, trilinolein 5, phenanthrene 6, 2,5-dimethoxy-1,4-benzoquinone 7, tetradecane 8. All of them were isolated from this plant for the first time.

从安徽舒城县产舒城贝母的干燥鳞茎中分离得到了14个单体化合物,应用核磁共振等手段鉴定了8个化合物的结构,其中4个化合物为异甾体生物碱,4个为非生物碱,分别为:veraflorizine 1、鄂贝乙素2、浙贝乙素3、异浙贝甲素4、三亚麻油酸甘油酯5、菲6、2,5—二甲氧基苯醌(2,5-dimethoxy-1,4-benzoquinone)7和正十四烷8,这些化合物均为首次从该植物中分离得到。

The optimal conditions determineded by experiments were as follow: chloracetic acid : sodium carbonate : isopropyl xanthate : ethylamine=l : 0.58 : 1 : 1.05, water usage is 30 ml/O.lmol chloracetic acid, esterification temperature was 80癈, esterification time was 2h, ammonolysis temperature was 70 C, ammonolysis time was Ih.

实验得出最佳工艺条件为:一氯乙酸:碳酸钠:异丙基黄药:乙胺=1:0.58:1:1.05,水用量为30 ml/0.1mol一氯乙酸,酯化温度80℃,酯化时间2小时,氨解温度70℃,氨解时间1小时。

Properties of frontier orbital of xanthogen formates and ethoxycarbonyl thionocarbamates, including HOMO energy, shape of HOMO and atomic HOMO density, were calculated with quantum chemistry programs GW03 and FUJISTU CAChe. According to the results, the relationship between selectivity of such two kinds of collectors and their quantum chemical indices was investigated to discuss the feasibility of applying them in screening chalcopyrite collectors.

摘 要:利用量子化学软件GW03和FUJISTU CAChe计算黄原酸甲酸酯类、乙氧羰基硫氨酯类黄铜矿捕收剂的前线轨道的性质—HOMO能量、HOMO形状以及药剂组成原子的HOMO密度,并结合这两类药剂的浮选结果研究这些量化参数与药剂选择性之间的联系,探讨这些参数作为选择黄铜矿捕收剂判据的可行性。

In this study, Japanese cedar, Ma bamboo and Makino bamboo were liquefied in polyethylene glycol/glycerol co-solvent with H2SO4 or HCl as catalyst. The liquefied woody materials were blended with PMDI (4,4'-Diphenylmethane diisocyanate;MDI) to prepare the PU foams. The effects of preparation conditions of PU resin on the properties of PU foams were investigated.

中文摘要本研究将柳杉(Cryptomeria japonica; Japanese cedar)、麻竹(Dendrocalamus latiflorus; Ma bamboo)及桂竹(Phyllostachys makinoi; Makino bamboo)等木质材料以聚乙二醇及丙三醇之混合液为溶剂,H2SO4及HCl为催化剂进行液化处理,并将其液化木质材料与4,4'-二苯甲烷二异氰酸酯反应制造聚胺基甲酸酯发泡体,探讨PU树脂调配条件对PU发泡体性质之影响。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。